邻—(4—乙基苯甲酰基)苯甲酸的研究

本文阐述了通过Friedel-Crafts反应合成邻-(4-乙基苯甲酰基)苯甲酸的方法.研究了影响产物质量的因素,提出了适宜的工艺条件.     

大规模数据库中的知识获取

一、前言数据是知识的潭泉,拥有大量的数据与拥有许多有用的知识完全是两回事.为了有效地利用大量的公共数据,必须更好地理解这些数据,并从其中快速、准确地发现知识.这里所说的知识是指大量数据中存在的规律性(r egularity)或不同属性值之间所存在的[I F THEN〕规则.将所获取的知识附加于仅由事实数据(fact data)构成的传统数据库上,既可强化数据库的查询能力,又可给数据库提供推理能力,     

Trends and variations in neonatal length of in-hospital stay in Canada

The objectives of this study were to evaluate the possible mechanisms involved in prolongation of bleeding time in pre-eclamptic patients receiving a magnesium sulfate infusion to prevent convulsions. Eighteen pre-eclamptic patients near term or at term (4 cases 33 to 35 weeks; the remainder > 36 weeks) were studied. Fifteen of them received magnesium sulfate infusion; 3 did not and served as controls. Bleeding time (modified Ivy method with Surgicutt), platelet count, platelet aggregation pattern, as well as serum arachidonic acid metabolites [thromboxane B2 (TxB2) and 6-Keto-prostaglandin F1 alpha (6-Keto-PGF1 alpha)] werde done on admission to the labor floor (before magnesium infusion) and repeated at discontinuation of the infusion, 12-24 hours postpartum; the controls received the second test 24 hours postpartum. Thirteen of 15 patients receiving magnesium sulfate had an increase in bleeding time from an average of 6 minutes 31 seconds to 11 minutes 56 seconds, an 82% rise (p < 0.004). In 2 there was a decrease. Among the 3 controls the averages were 6 minutes 38 seconds and 6 minutes 3 seconds. The total magnesium given ranged from 52.5 to 145 grams. Platelet counts averaged 251,000/mm3 (range 145,000-519,000). Platelet aggregation pattern done in 11 patients and was normal and unchanged after magnesium in 10 of the patients with increased bleeding time and one control. TxB2 and 6-Keto-PGF1 alpha levels did not change significantly either after magnesium administration (688 and 135 pgm/ml, to 654 and 117) or in controls (695 and 230 pgm/ml, to 445 and 225). Likewise, the ratio of these 2 substances did not change in either group (6.3 to 6.6, and 4.2 to 2.2). There was no correlation between duration of infusion or total magnesium given and directions of small changes observed. This study confirms a prior preliminary observation that magnesium sulfate infusion, as currently used to prevent eclamptic convulsions, induces a significant prolongation of bleeding time. This effect is mediated neither by changes in platelets count or aggregation pattern, nor by changing the level or ratios of serum arachidonic acid metabolites (TxB2 and 6-Keto-PGF1 alpha). Further studies are needed to clarify the mechanism of this clinically important observation of increased bleeding following magnesium sulfate infusion.     

提高柴油机缸盖内腔铸造质量的工艺措施

缸盖是柴油机上的重要零件之一。铸造毛坯不可避免地存在劈缝、内腔粘砂、粗糙、局部不通等内腔质量问题 ,从而影响缸盖串水冷却效果。本文介绍了一些工艺措施 ,较好地解决了这个问题。     

NGO-Ⅲ催化剂的异构化性能评价

直馏汽油非临氢高效异构化使用最新一代NGO－Ⅲ型催化剂，生产的产品汽油辛烷值、产品收率及催化剂稳定性等全面超过现用的工业催化剂，达到目前国内同类产品的领先水平。     

再谈石材幕墙干挂中存在的安全隐患

随着社会经济的发展，在建筑物装饰中，石材幕墙已占有相当大的比例，华丽的石材幕墙确实为装点城市增添了光彩。庞大的幕墙所用石材每块重达几十斤，并且是由一个个小小的、很不起眼的干挂件与结构体相连接，可见质量是何等的重要。　　但是，令人担忧的是，目前市场上的干挂件质量不容乐观。近几年，外交部大楼、首都机场候机楼等均发生过石板从天而降砸坏汽车和其他物品的事件。导致事件的原因是因挂件质量低劣、焊接头缝不饱满，且经过高温退火产生氧化而断裂所造成。去年中央电视台《焦点访谈》节目对江苏兴化生产的不锈钢产品质量…     

H.248协议在UMTS核心网中的应用

描述了H.248协议的连接模型和消息结构,分析了H.248协议在UMTS核心网中的实现方案,并给出了一个应用实例,最后探讨了实现中可能面对的问题和解决方案。     

二维谐振子与二维氢原子的能量及波函数

借助于ＳＵ(１,１)代数,找出了二维谐振子与二维氢原子的能量及波函数间的关系．     

CuO/ZnO甲醇合成催化剂的正电子湮没谱学研究

发展了用正电子湮没寿命参数测定用共沉淀方法制备的金属氧化物系固溶度的新方法。测量了一系列用共沉淀方法制备的不同CuO at％含量的CuO/ZnO甲醇合成催化剂粉末(压制成片)还原前后的正电子寿命谱。分析该种催化剂的固溶特性及其与正电子寿命参数的关系,得出还原后样品的固溶度为12CuOat％.支持了CuO/ZnO甲醇合成催化剂以Cu~+离子为活性中心的观点。     

Si衬底上Ta-N/Cu薄膜性能研究

对Si衬底上Ta-N/Cu薄膜进行了电学和热学分析，结果发现500℃以下薄膜电随几乎不变，600-690℃下的退火引起的电阻率降低是由于Ta-N电阻的热氧化和Cu熔化扩散引起的，而690℃以上的电阻率增加是由于Cu引线传输能力减弱所致，为0.18μm以下的超大规模集成电路中的Cu引线和电阻薄膜的制作提供了有益的借鉴。