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101.
Jing Lv Longhai Guo Chunjie Xie Weitong Xu Jun Ye Xiaoyu Li Teng Qiu Xinlin Tuo 《应用聚合物科学杂志》2021,138(44):51316
Being a new kind of nanomaterials, aromatic polyamide nanofibers (ANF) have been much highlighted in recent studies. We here demonstrate an isopropyl alcohol (IPA) accelerated chemical cleavage on poly (p-phenylene terephthalamide) chopped fibers, which provides an efficient preparation method of ANF. The comprehensive study on the processes accelerated by different alcohols revealed that the preparation time of ANF in the mixed medium of dimethyl sulfoxide (DMSO)-alcohol (20:1 in volume) was shorten to 45 min and 75 min for methanol (ethanol) and isopropanol, respectively. However, the nanofibers prepared in DMSO-IPA exhibited the minimum in axial and radial dimensions, providing the finest and most uniform diameter of 16 nm. The corresponding ANF films through vacuum assisted filtration also showed the highest tensile strength of 150 MPa, in comparison with those of the ANF films prepared using other alcohols, which were about 110 MPa. Furthermore, ANF/silicon hybrid films were prepared by the ionic ring-opening reaction followed by the alkoxysilane condensation and nanoparticle fabrication. By changing the organo functional groups in the alkoxysilane, the surface of the films were adjustable in a wide contact angle range from 56° (hydrophilic) to 150° (superhydrophobic), suggesting the amendable interfacial properties potential applicable to composite fabrication with most of the resin matrix. 相似文献
102.
激光熔覆含SiC金属陶瓷涂层显微组织特征 总被引:5,自引:4,他引:5
采用连续CO2激光器在钢表面进行熔覆含SiC金属陶瓷涂层。对不同工艺条件下激光熔属层组织结构、成分与硬度进行了研究,对试验结果和凝固过程进行了传热分析。 相似文献
103.
104.
用双层辉光等离子法在钛表面制备的Ti-Pd合金层性能研究 总被引:2,自引:0,他引:2
采用双层辉光等离子冶金技术在纯钛表面制备了Ti—Pd合金层。其深度大约为90μm,Pd含量呈梯度变化,并出现了TiPd3,TiPd2,Ti2Pd3,Ti3Pd5,TiPd,Ti4Pd等6种化合物相和Pd相。合金层在100℃的NaCl饱和溶液+HCl溶液以及40℃的8.6%H2SO4溶液中的耐缝隙腐蚀性能优于Ti0.2Pd合金;在室温80%H2SO4的溶液中,腐蚀速率仅为0.682mm/a,是Ti0.2Pd合金的18.2%:在室温30%HCl的溶液中,表面Ti—Pd的腐蚀速率仅为0.004mm/a,是Ti0.2Pd合金的12.5%。 相似文献
105.
提出了一种根据不同的冲裁工序,可在压力机上迅速更换凸、凹模的通用模架;介绍了这种模架的结构、基本工作过程及其主要优缺点,并对模架的主要零件的设计作了说明。 相似文献
106.
107.
Fan Jinglian Zhao Muyue Xu Guofu Central-South University of Technology Changsha China 《中国有色金属学会会刊》1993,(3)
The breakage mechanism of W-Ni-Fe alloy in the process of electro-heat upsetting studied both theoretically and experimetnally, and also the behaviors of crack formation and propagation were analysed. Alloy suffers from corrosion and thermal-mechanical fatigue mutual function. Simultaneously, the practical ways to improve the anvil life was discussed. 相似文献
108.
In this work, we have put forth two different protocols to address a concrete secure multi-party computational (MPC) problem related to a triangle, of which the coordinates of the three vertices are confidentially kept by the three participants, respectively. The three parties wish to collaboratively compute the area of this triangle while preserving their own coordinate privacy. As one of the merits, our protocols employ weaker assumptions of the existence of pseudorandom generators. In particular, unlike massive secure MPC protocols that rely a lot on oblivious transfer, ours utilize a new computing idea called “pseudorandom-then-rounding” method to avoid this burdensome obstacle. The two protocols are based on different theorems, while they both make use of the same underlying idea. At last, we provide a detailed proof for the first protocol by a series of security reductions of our newly defined games, which seems somewhat stronger than the previous simulation-based proofs and a proof sketch for the second one. Analysis and discussion about the reasons are provided as well to round off our work. 相似文献
109.
110.