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21.
Manipulation of molecular orientation alignment in MCTLCPs (main-chain thermotropic liquid crystalline polymers) by pure shear at nano scale has been investigated for the first time using molecular dynamics (MD) simulation. Results indicate that high planar shear induces long-range uniform orientation ordering (liquid crystalline phase) of initially randomly orientated molecules of MCTLCP fluid confined in a nanochannel, which is confirmed by analyzing the orientation order parameter and the snapshots of MCTLCP liquid in a nanochannel under different shear rates. Insights into the origin of the phase transition phenomena are given at molecular level through investigating the thermodynamic density distribution of MCTLCP molecules in the nanochannel, suggesting that the energy shift due to a radical jump of system density affects both the magnitude and the orientation of the molecular ordering. Simulation results also show that there is a critical shear rate for transforming isotropic phase into liquid crystalline phase. The critical shear rate is dependent on the temperature of the MCTLCP system. Findings in this paper may present useful information for processing TLCP molecules at nano scale and the understanding of nanoflow. 相似文献
22.
Lei Liu Ying Kong Hong Xu Jin P. Li Jin X. Dong Zhi Lin 《Microporous and mesoporous materials》2008,115(3):624-628
A three-dimensional zinc phosphate compound with DFT topology, designated as ZnPO4-EU1, has been synthesized by an ionothermal approach from the system HF-ZnO–P2O5-choline chloride-imidazolidone. Ethylenediamine, derived from decomposition of the imidazolidone component of the deep-eutectic solvent (DES) itself, is delivered to the synthesis and serves as an appropriate template for ZnPO4-EU1. Experiments in which the synthesis conditions were varied showed that ZnPO4-EU1 may be prepared over a wide molar ratio of P/Zn = 0.55–13.0. Powder X-ray diffraction patterns have been obtained at intervals to track the crystallization process of this material. The experimental data show that Zn3(PO4)2 · 4H2O (a dense phase) was first isolated from the DES after reaction for 1 h. Subsequently, the pure phase of ZnPO4-EU1 was obtained with increasing crystallization time from 12 h to 72 h. The experimental results show that the nucleation and crystallization take place with relatively low levels of solvent degradation, demonstrating that zinc phosphate with a three-dimensional framework can be synthesized by in situ generation of an appropriate template using an unstable DES at high temperatures (150–200 °C). 相似文献
23.
镁钴铝类水滑石催化合成安息香甲醚 总被引:1,自引:0,他引:1
采用共沉淀法制备了镁钴铝类水滑石化合物(MgCoAl-HTLcs),并用 X 射线衍射、扫描电子显微镜、NH_3程序升温脱附等方法对 MgCoAl-HTLcs 进行了表征,并以 MgCoAl-HTLcs 为催化剂催化苯甲醛与甲醇反应合成安息香甲醚,研究了n(Mg):n(Co):n(Al)、催化剂用量、原料配比、反应温度、反应时间对合成反应的影响。表征结果显示,MgCoAl-HTLcs 的晶相完整,表面主要为弱酸、弱碱性。催化合成安息香甲醚的适宜条件为:MgCoAl-HTLcs 催化剂用量0.10 g(约为原料总质量的0.23%),n(Mg):n(Co):n(Al)=0.4:1.6:1.0,V(苯甲醛):V(甲醇)=3:50,反应温度50℃,反应时间150 min。在此条件下,苯甲醛的平衡转化率达77.49%,安息香甲醚选择性接近100%。为洁净合成安息香甲醚开辟了一条新的途径。 相似文献
24.
B737机务CBT系统建设方案的探讨 总被引:3,自引:0,他引:3
张旭 《上海工程技术大学学报》2004,18(4):375-378
通过对AICC制订的CBT课件开发规范的探讨,阐述了CBT的基本概念和波音737飞机机务CBT的开发制作过程,以及利用Authorware开发软件制作多媒体课件的技术难点。 相似文献
25.
Zhiping Lin Xu L. Bose N.K. 《IEEE transactions on circuits and systems. I, Regular papers》2008,55(1):445-461
26.
Power distribution systems have been significantly affected by many outage-causing events. Good fault cause identification can help expedite the restoration procedure and improve the system reliability. However, the data imbalance issue in many real-world data sets often degrades the fault cause identification performance. In this paper, the E-algorithm, which is extended from the fuzzy classification algorithm by Ishibuchi to alleviate the effect of imbalanced data constitution, is applied to Duke Energy outage data for distribution fault cause identification. Three major outage causes (tree, animal, and lightning) are used as prototypes. The performance of E-algorithm on real-world imbalanced data is compared with artificial neural network. The results show that the E-algorithm can greatly improve the performance when the data are imbalanced 相似文献
27.
In this paper, we present a static load balancing method for mapping production rules in an expert system onto processors of a message-passing multicomputer. The method uses simulated annealing to achieve a nearly optimal allocation of production rules onto processor nodes. The approach balances the initial rule distribution to avoid higher communication demand among processor nodes at run time. A formal mapping model is developed and a new cost function is defined for the annealing process. New heuristic swap functions and cooling policies are provided to ensure the quality of the annealing process. A software load balancing package, SIMAL, was implemented on a SUN workstation to carry out the benchmark experiments. The overhead associated with this mapping method is O(m In m), where m is the number of rules in the production system. Two benchmark production systems, Toru-waltz and Tourney, are mapped onto a hypercube computer with 32 nodes. Experimental benchmark results verify the effectiveness of the rule mapping method. The method can be applied for distributed artificial intelligence processing or for the parallel execution of cooperating expert systems on a message-passing multicomputer. 相似文献
28.
Chuanju Xu 《Journal of scientific computing》2006,27(1-3):495-505
A stabilization method for the spectral element computation of incompressible flow problems is investigated. It is based on a filtering procedure which consists in filtering the velocity field by a spectral vanishing Helmholtz-type operator at each time step. Relationship between this filtering procedure and SVV-stabilization method, introduced recently in [JCP, 2004, 196(2), p680], is established. A number of numerical examples are presented to show the accuracy and stabilization capability of the method. 相似文献
29.
Fixed point theorem-based iterative learning control for LTV systems with input singularity 总被引:1,自引:0,他引:1
In this paper, we address a challenging and open problem: how to design a suitable iterative learning control (ILC) system in the presence of input singularity, which is incurred by the singularities of the system direct feed-through term. Considering two typical types of input singularities, we first revise the ILC operators accordingly by adding a forgetting factor and incorporating a time-varying learning gain, in the sequel guarantee ILC operators to be contractible. Next, using the Banach fixed-point theorem, we demonstrate that the output sequence can either enter and remains ultimately in a designated neighborhood of the target trajectory, or is bounded by a class K function. Finally, an illustrative example is presented. 相似文献
30.
本文通过对压电量测系统等效电路图的逐步简化,得出矩形脉冲信号的漏电方程;并对系统在各种情况下的时间常数,漏电相对误差进行了计算,最后就系统在校准和现场测试中经常碰到的几种情况,进行了定量估算,从而解决了压电量测系统在使用中的一些具体问题。 相似文献