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101.
Wei Fen Zhang Xi Guang Chen Pi Wu Li Cheng Sheng Liu Qiang Zhi He 《Drying Technology》2008,26(1):108-115
Three kinds of carboxymethyl chitosan/β-cyclodextrin microspheres loaded with theophylline were prepared by spray drying intended for pulmonary delivery. Mucociliotoxicity, permeation rate, and drug release characteristics of the product were investigated. The microspheres obtained by spray drying were found to be spherical with smooth or wrinkled surfaces. The mean particle size was between 3.39 and 6.06 µm. The microspheres demonstrated high product yield (43.7-50.2%), high drug loading (13.7-38.1%), and high encapsulation efficiency (86.9-92.8%). FT-IR indicated that there were interactions of theophylline with carboxymethyl chitosan matrix. Further studies on mucociliotoxicity and permeation confirmed that microspheres had better adaptability and high permeation rate. In vitro drug release from the microspheres was not related to the drug/polymer ratios. 相似文献
102.
Flammability ranking of foliage species by factor analysis of physical and chemical pyric properties
In this paper, factor analysis is introduced to evaluate the flammability of 55 foliage species that may be used in China for construction of the fuel break network of forest strips with lower flammability. Six pyric parameters, i.e. air dry moisture content, absolute dry moisture content, ignition point, ash content, caloric value and extractive content, are measured and used as variables for factor analysis. The covariance analysis shows that four principal factors can be extracted to reflect the flammability in different physical and chemical senses. In terms of the contributions of the four factors to the variances and the physical significance of the relevant parameters, the four factors are, respectively, termed as ‘flaming factor,’ ‘air dry factor,’ ‘ash factor’ and ‘absolute dry factor.’ The stability of the factor analysis method is examined by a different number of samples considered, and the variation degrees of the orderings indicate that the method has high reliability to measure the total flammability of foliage species. The results of the flammability evaluation are verified by comparison with the recommended tree species in the Chinese technology standard. Copyright © 2008 John Wiley & Sons, Ltd. 相似文献
103.
Hydrothermal Synthesis of Magnesium Aluminate Platelets 总被引:1,自引:0,他引:1
Zhi-Zhan Chen Er-Wei Shi Hua-Wei Zhang Yong Zhang Xiang-Biao Li Xue-Chao Liu Bing Xiao 《Journal of the American Ceramic Society》2006,89(12):3635-3637
Magnesium aluminate (MgAl2 O4 ) platelets were first synthesized by hydrothermal treatment of γ-AlO(OH) in a magnesium nitrate aqueous solution at 400°C. The platelets are 100–200 nm in width and 25 nm in thickness. The influence of temperature, the anions of the magnesium salt, the amount of magnesium salt, and precursor pH on the formation of such structure was investigated. The experimental results indicated that the anions of the magnesium salt and precursor pH could have a significant influence on the growth of MgAl2 O4 . MgAl2 O4 formation followed the in situ transformation mechanism, which was the reason why the MgAl2 O4 crystallites had a platelet morphology. 相似文献
104.
以三聚磷酸钠生产过程为例,论述了在以纯碱为原料的非强酸性水溶液体系中,由于反应不完全导致反应物中存在少量的碳酸盐,这部分碳酸盐干扰了用酸碱滴定法测量的中和度,并据此提出中和度分析改进方法.由此可以推广到其它以纯碱为原料的非强酸性水溶液体系中. 相似文献
105.
Summary Well-defined water-soluble poly(styrenesulfonate)-b-poly(ethylene glycol)-b- poly(styrenesulfonate) (PSS-b-PEG-b-PSS) triblock
copolymers with narrow molecular weight distribution (1.29 < Mw/Mn < 1.36) were synthesized in aqueous solution at 70 oC via reversible addition-fragmentation chain transfer (RAFT) polymerization. The complex formed by the PSS-b-PEG-b-PSS triblock
copolymer coordinated with aluminum ion was investigated with turbidimetry, dynamic light scattering (DSL), zeta-potential,
and transmission electron microscopy (TEM). The aggregation formation was based on the neutralization of the SO3- groups in the PSS blocks with Al3+ ions. The appearance, size and stability of the PSS-b-PEG-b-PSS/Al3+ aggregates were controlled by varying the PSS block length and degree of neutralization (DN). At DN = 0.33, where the PSS-b-PEG-b-PSS
copolymer was completely neutralized with Al3+, the aggregate size increased with increasing PSS block length. The transition from the shrinking coil of small size to the
interchain aggregates of large size was found at DN of about 0.33. 相似文献
106.
刘建平 《电信工程技术与标准化》2008,21(6):32-38
本文研究了ROADM的技术优势,主要结构类型,涉及的关键技术以及存在的问题,并分析了当前ROADM标准化进展情况与发展趋势,还介绍了当前设备现状和现网应用情况。 相似文献
107.
108.
本文介绍了用αβ谱仪系统同时测量αβ谱、实现Rn/Th子体补偿、确定超铀α核素气溶胶体积活度及人工放射性气溶胶总β体积活度的技术途径。利用RaA、RaC′a峰的二段时间计数可确定空气中RaA、RaB、RaC的气溶胶体积活度,相应的,也能给出RaB、RaC对总β计数的贡献。根据一般环境条件下的平衡比,用ThC′的。计数修正Th子体对αβ测量的影响。 ̄[239]pu或/和 ̄[241]Am人工核素的α计数,可通过两段时间分别扣除RaA、RaC′拖尾的方法确定;β计数分别扣除Rn/Th子体β贡献即可确定。在本文规定的测量条件下,对室内天然Rn子体水平在15Bq/m ̄3以下,超铀α核素气溶胶体积活度的测量下限可达到0.1Bq/m ̄3;即使在75Bq/m ̄3环境下,人工核素总β的测量下限也可达lBq/m ̄3以下。 相似文献
109.
AIM: To study the effect of the angiotensin-converting enzyme (ACE) inhibitors perindopril (Per) and enalaprilat (Ena) on the reactivity of the endothelium in normal rats. METHODS: Male rats were treated intragastrically with Per (2 mg.kg-1.d-1) or placebo (n = 18) for 6 wk. Aorta was isolated for experiment. Another set of isolated aortic rings with and without endothelium were incubated with Ena (0.1 mumol.L-1) for 30 min. Responses to acetylcholine, serotonin, phenylephrine, sodium nitroprusside (SN), and nitroglycerin (Nit) were observed. RESULTS: Endothelium-dependent relaxation to acetylcholine was augmented in aortic rings from rats treated with Per in comparison with control. The IC50 value (95% confidence limits) decreased from 3.8 (0.56-26.1) mumol.L-1 (control group) to 0.98 (0.28-3.41) mumol.L-1 (Per-treated group). The maximal relaxation was augmented from 62 +/- 9% to 78 +/- 10% (P < 0.01). However, the responses to the endothelium-independent vasodilators, SN and Nit, were similar. Serotonin- and phenylephrine-induced contractions were decreased, which were influenced by basal release of endothelium-derived relaxing factor (EDRF). EC50 values was 6.1 (2.6-14.4) nmol.L-1 vs 8.3 (3.6-18.8) nmol.L-1 in comparison with control group and Per-treated group. The maximal contraction was decreased from 2.42 +/- 0.29 g (control group) to 1.96 +/- 0.25 g (treated group) (P < 0.01). Similar results were found in incubation with Ena. CONCLUSION: Ena and Per enhanced the basic release of EDRF from vascular endothelium. 相似文献
110.
The effect of salt addition, in the form of a fluxing agent containing equivalent amounts of NaCl and KCl, on the microstructure and mechanical properties of 359/SiC/10p composite has been investigated. Both microstructure and properties are affected, with the removal of magnesium and strontium and the introduction of sodium and potassium being responsible for the degradation in properties. Thermodynamic calculations have been carried out to account for the effect of salt addition in terms of the surface adsorption of sodium and potassium impurities and the consequent changes in the surface-interface tension of their binary alloys. Mechanisms for the degradation of properties have been discussed. 相似文献