洛伐他丁的电化学行为研究

用线性扫描极谱法考察了洛伐他丁的极谱行为,旨在建立一种简单、快捷和灵敏的测定洛伐他丁含量的分析方法。实验采用三电极系统（滴汞电极为工作电极,Pt电极为对电极,饱和甘汞电极为参比电极）,以1∶1的0.8 mol/L NH4Cl和0.8 mol/L NH3.H2O混合溶液为底液,发现洛伐他丁在-1.62 V左右有一个灵敏的二阶导数极谱峰,其峰高与洛伐他丁溶液在0.50~7.00μg/mL范围内呈线性关系。洛伐他丁的加标样品回收率在98.0%~104.2%之间,最小检测限为0.370μg/mL。同时考察了表面活性剂和共存的金属离子Al3＋、Cu2＋、Fe3＋、pb2＋对洛伐他丁极谱波的影响。利用建立的洛伐他丁含量的极谱分析方法对样品中洛伐他丁含量进行了测定,结果表明所建立的洛伐他丁极谱分析方法快速、准确,具有一定实用价值。     

汶川地震区震后泥石流活动特征与防治对策

2008年5月12日的汶川Ms8.0地震对地表产生强烈扰动,使得泥石流形成条件发生剧烈变化,影响到震后泥石流的活动特征和减灾对策.作者在调查数据的基础上,从固体松散物质条件、微地貌条件和水文条件的变化3个方面,分析了汶川地震区震后泥石流形成条件的变化,认为:汶川地震灾区崩塌、滑坡等产生的松散固体物质达28×108 m3,为该区泥石流长期活动提供了丰富的物质基础;流域微地貌突变特别是严重的沟道堵塞,有利于泥石流规模的增大;强烈地表扰动和毁灭性、大面积毁坏植被,改变了地表水入渗、产流和汇流条件,利于侵蚀和洪峰形成.这些流域状态的巨变,构成了有利于泥石流形成的条件组合.从而,导敛震后泥石流活动强度急剧增大,使得泥石流成为对地震区影响最为严重的灾害.震后泥石流活动的主要特点有:泥石流沟谷数量增加,大量震前被判定为非泥石流沟的流域暴发了泥石流;激发泥右流的临界雨量明显降低泥石流暴发表现出明显的高频性与群发性;泥石流的容重约提高10%～30%,原来定性为稀性或过渡性的泥石流沟转化为过渡性或粘性泥石流沟;泥石流流量普遍增大,大致可增加约50%～100%,现有规范中泥石流流量计算方法的结果偏小,需要修正.震后泥石流演变趋势为:活动强度由急剧增强的突变转为逐步减弱,期间活跃期与平静期交替出现,第1个泥石流活跃期可能会持续约15年左右;泥石流形成将由降雨控制型逐步转为松散土体控制型;一些松散土体丰富且尚未发生泥石流的面积大于5 km2流域,将是未来暴发大规模泥石流的风险源.针对震后泥石流的活动特征、演化趋势和震区泥石流防治中存在的问题,提出:判识潜在泥石流灾害,增强减灾措施的针对性;进行泥石流灾害风险分析,加强风险管理;改进泥石流规模计算方法,适应震区超常规模泥石流防治需求;重新确定泥石流预警报的临界雨量指标,加强监测预警系统建设等灾害防治对策.     

Performance study of combined test rig for metro train traction

This paper deals with a combined test rig for a traction system in the laboratory environment. An experimental system was designed and implemented to verify the performance of the traction system for a metro train. For a highly accurate control of the system, a hybrid control algorithm combining vector control and slip frequency control was applied to control the traction inverter. The design method of the flywheels, which represent the equivalent model of the train moment inertia, was elaborated. A train runtime diagnosis system was completed by adopting the multifunction vehicle bus (MVB) protocol. The dynamic performance of the metro power traction system was emulated under the control of the train runtime diagnosis system. Using the combined test rig, the performances of the traction system in traction, braking, temperature rise, etc., were verified through traction and breaking experiments.

     

瓮福磷矿选矿厂精矿仓设计

瓮福磷矿选矿厂精矿仓首次采用网架式地面矿仓，造价低，空间利用率高，设备运行平稳可靠，操作灵活方便，工作环境好。超长梭式胶带布料机的设计也是成功的。     

基于Logistic回归惩罚函数的遗传位点分析

探讨将基于惩罚函数的变量选择方法应用到遗传位点分析.以2016年9月16日的全国研究生数学建模竞赛B题的数据为例,首先对每个位点的碱基对(A、T、C、G)编码方式数值化处理,最后用数值化后的数据进行建模,并将单变量选择Logistic SCAD、组变量选择Logistic Group SCAD模型和双层变量选择Logistic cMCP模型定位到与遗传性疾病显著相关的遗传位点,分别与出题者提供的标准答案进行对比,结果显示双层变量选择Logistic cMCP模型能够准确的定位到与遗传性疾病显著相关的遗传位点.因此将其运用到具有遗传性疾病和性状的遗传位点分析是值得研究的.     

基于渐开线齿轮范成仪的改进设计

根据渐开线廓范成仪的功能和原理,把老式范成仪的手动操作改为电子控制自动操作,使操作精确方便,经实际使用效果很好,为制造自动式渐线线齿轮范成仪提供参考.     

基于RFID的监狱智能定位系统的设计与实现

为解决在押犯人管理困难的问题,该文介绍了一种基于射频识别技术的CC1110 RSSI定位系统。系统主要由腕带标签、读卡器、无线中继和服务器组成。标签主要负责对读卡器发送相关信息,读卡器负责接收标签的数据并转发给无线中继,中继通过以太网把读卡器传送过来的数据发送给服务器,服务器负责对数据的处理、分析并进行相关管理操作。该系统结构简单、硬件成本较低、易部署、适应性较强。实际测试表明,该系统能够用于监狱在押人员的定位,降低非视距误差。     

Enhanced luminescence and thermal stability of (Sr,Ca)AlSiN3:Eu2+ via superficial organic carbon modification

The Eu²⁺-activated nitride phosphors have been widely used in solid-state lighting, but the applications in high-power white-light-emitting diodes (wLEDs) field require higher thermal stability of luminescent materials. The oxidation of Eu²⁺ and the damage of nitride host in the Eu²⁺-activated nitride phosphors are the two crucial reasons for the luminescence loss while operating. A superficial organic carbon modification is performed on the red-emitting (Sr,Ca)AlSiN₃:Eu²⁺ phosphor via the incorporation of organic carbon by solution mixing and thermal post-treatment under the N₂-H₂ atmosphere. After the superficial organic carbon modification, the oxidation of Eu²⁺ and the formation of impurity phases on the phosphor surface are effectively reduced. When the superficial organic carbon modified sample was treated in the 2 wt.% sucrose solutions, the relative brightness is strengthened by 2.15%, the thermal quenching characteristic is improved by 8.9% at 300℃, and the aging test results show an excellent thermal stability. All above indicate that the superficial organic carbon modification is a promising technique to enhance the thermal stability of analogous Eu²⁺-activated nirtide phosphors.     

钢的回火过程中应力演化的数值模拟

本文提出了一种模拟钢的回火过程中应力演化的数学模型。其中着重进行了蠕变方面的试验研究。在淬火过程数值模拟基础上，用据此模型开发的有限元软件对２６Ｃｒ２Ｎｉ４ＭｏＶ钢圆筒形试件的回火过程进行了计算。结果表明，由本模型预测的回火效果与实测吻合较好。此外还计算分析了回火规范对残余应力的影响，进一步验证了模型的有效性。     

Temperature Dependence of the Magnetocrystalline Anisotropy in Nd_2Co_(14)B Compound

Easy and hard magnetization curves of Nd_2Co_(14)B compound have been measured withextracting-sample-magnetometer(μ_0H_(max)=6T)at 10～300 K.Magnetic anisotropy constants K_1 and K_2have been determined by fitting the hard magnetization curves,in which only K_1 ,K_2 and misalignment anglehave been taken as fitting parameters.The values of K_1 and K_2 at 4.2 K were derived by extrapolation.Anisotropy coefficients,x_2~° and x_4~°were derived from the anisotropy constants.The anisotropy constant K_2increases rapidly with increasing temperature when TT_(sr).The temperature depen-dence of the magnetic anisotropy coefficient x_2~° was fitted with the formula.The anisotropy coefficients x_2~°can be well described by the tenth-power law from 4.2 K to T_(sr)and by the sixth-power law from T_(sr_ to 300 K.