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81.
An O?carboxymethylated chitosan (O? CMCh) water solution (I) and N,N‐dimethylacetamide (DMAc) emulsion (II) were blended with a cellulose LiCl/DMAc solution, and corresponding polyblends (Polyblends I and II) were obtained. The rheology of the three fluids, that is, the cellulose solution and Polyblends I and II, was investigated. The cellulose solution was characterized by a power‐law fluid. When an O‐CMCh water solution or DMAc emulsion was added to the cellulose solution, the power‐law curve was preserved. The power‐law indexes (n) of all three fluids increased along with the temperature. Polyblend I displays an n close to but a little higher than that of the cellulose solution, while Polyblend II shows a much higher power index than those of the other two fluids. The values of the apparent viscosity (ηa) for all the three fluids are close and decrease along with an increase in the temperature. Adding O‐CMCh microparticles into Polyblends I and II results in a decrease in the structural viscosity index (Δη) in comparison to that of the cellulose solution, and this effect is very obvious for Polyblend I. A cellulose solution's Δη declines with the augmentation of temperature, while the Δη's of both Polyblends I and II show minimum values at about 323 K. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 1719–1725, 2003 相似文献
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83.
在实验研究的基础上,采用分子模拟的方法,对在水解-水热体系中TiO2纳米颗粒晶相生成原理进行了系统的模拟计算和建模研究,文章介绍了分子模拟软件Hyperchem的计算方法,建立了钛离子水解过程和能量分布模型,利用模拟计算和模型,直观和定量分析了水解中间产物、水热晶化过程以及最终产物间的关系。研究了pH值对同质异构相成因的影响机理;静电场作用对同质异构相生成的影响。考察了水合络离子的连接方式,指出顶角连接与棱边连接保持到最终产物的结构中。从能量的角度揭示了同质异构TiO2晶型成因。 相似文献
84.
We present an interactive method for mesh segmentation that is inspired by the classical live‐wire interaction for image segmentation. The core contribution of the work is the definition and computation of wires on surfaces that are likely to lie at segment boundaries. We define wires as geodesics in a new tensor‐based anisotropic metric, which improves upon previous metrics in stability and feature‐awareness. We further introduce a simple but effective mesh embedding approach that allows geodesic paths in an anisotropic path to be computed efficiently using existing algorithms designed for Euclidean geodesics. Our tool is particularly suited for delineating segmentation boundaries that are aligned with features or curvature directions, and we demonstrate its use in creating artist‐guided segmentations. 相似文献
85.
Jiuxin Jiang Bo Zhu Peiling Wang Weiwu Chen Dongsheng Yan Hanrui Zhuang Yibing Cheng 《Journal of the American Ceramic Society》2005,88(4):950-953
The Pr α-sialon powders prepared by self-propagating high-temperature synthesis (SHS), consisting of 55 wt% Pr α-sialon and 45 wt% of β-sialon (abbreviated as α' and β'), were hot-pressed at 1800°C for 1 h. The results showed that Pr α' phase would transfer to β' with the appearance of JEM phase (Pr(Si6− z Al z )(N10− z O z )) after sintering, thus resulting in the increase of β' phase to 86 wt%. The addition of Y2 O3 into SHS-ed Pr α' powders as the starting materials restrains the transformation of α' to β' and prevents the formation of JEM phase as well. The nucleation mechanism of Pr α' grain during hot-pressing was investigated in terms of transmission electron microscope and energy-dispersive spectrometer analysis. Two nucleation modes of Pr α' grains were found, i.e., nucleating on the undissolved Pr α' grains and on the nuclei of (Pr, Y) α' grains precipitated from liquid phase. 相似文献
86.
Liang Xu Lei Su Hongjie Wang Min Niu Lei Zhuang Kang Peng Xingyu Fan Hongfei Gao De Lu 《Journal of the American Ceramic Society》2022,105(8):5490-5500
Pursuing novel thermal barrier–coating materials with lower thermal conductivity and high-temperature stability can simultaneously improve the working efficiency and service temperature of a gas turbine. In this study, a series of high-entropy RE2(Y0.2Yb0.2Nb0.2Ta0.2Ce0.2)2O7 (RE = La, Nd, Sm, Gd, Dy, and Er) oxides were prepared though solid-state reaction. Through tuning the rare-earth cations, an order–disorder transition occurs from certain partially ordered weberite structure (C2221) to disordered defective fluorite structure (Fm m). All the high-entropy RE2(Y0.2Yb0.2Nb0.2Ta0.2Ce0.2)2O7 oxides possess low thermal conductivity in the range of 0.91–1.34 W m−1 K−1 at room temperature, which can be attributed to increased lattice anharmonicity and disorder, resulting in additional phonon scattering. Herein, we proved that the incorporation of heterovalent cations at B-sites in high-entropy A2B2O7 crystals is an effective strategy to reduce the thermal conductivity without compromising the decrease of oxygen vacancy. Moreover, the high-entropy RE2(Y0.2Yb0.2Nb0.2Ta0.2Ce0.2)2O7 oxides show the relatively higher thermal expansion coefficients of 10.3–10.7 × 10−6°C−1 and excellent phase stability at elevated temperatures. 相似文献
87.
88.
本研究选择了改性聚酰亚胺、改性聚甲醛、改性尼龙三种材料应用于摩托车衬套制品,进行了对比试验,结果表明:采用改性聚酰亚胺的衬套具有强度高、耐磨损、尺寸稳定性好等特点,完全达到该产品设计的要求。 相似文献
89.
为了减小视频信号采集端的负担,提出一种基于压缩传感理论的视频压缩算法模型。该模型采用广义轮换矩阵获取视频帧的测量值,再结合视频压缩的运动补偿预测关键技术,消除视频帧间冗余。然后在并行贪婪追踪算法中引入前向预测技术作为重构算法,最终获取重构的压缩图像。实验对比了在不同算法下的重构图像和不同采样比下不同算法的重构PSNR值,然后利用所提方法得到视频序列的重构压缩图像。实验结果表明,该算法模型能较精确地获取压缩的视频图像,适合在视频压缩中应用。 相似文献
90.
粉煤灰填充PVC树脂的研究 总被引:3,自引:0,他引:3
采用WAXD、SEM和力学测试等方法对不同粒度和不同含量的粉煤灰(PFA)与聚氯乙烯(PVC)共混物的结构形态、力学性能进行了测定。结果表明,PFA粒度对PVC/PFA共混物的性能具有明显影响,当PFA粒度尺寸达到一定程度时,再降低PFA粒度尺寸对共混物的性能影响不大。随着PVC/PFA共混物中PFA含量的增加,拉伸强度和拉伸模量增大,但伸长率降低。 相似文献