掺杂元素对Ni-Mn-Ga合金结构与性能的影响

Ni-Mn-Ga合金是一种新型的智能材料,兼具铁磁性和形状记忆效应的双重优点,以对磁场的快速响应和大的宏观可恢复应变的特点有望成为传感器和驱动器的候选材料.通过掺入金属元素可以弥补该合金马氏体相变温度低,脆性大的不足.综述了掺杂元素对合金结构、相变温度、力学性能、形状记忆效应的影响,并提出了需要深入研究的问题.     

基于路径仓的面向对象XML查询处理技术

XML正在迅速成为Internet上数据表示和交换的标准,存储与查询XML数据变得日益重要,如何快速、准确地查询面向对象的XML数据成为当前研究的热点,索引技术是提高查询效率的有效方法。该文基于路径仓索引模式,提出了一种面向对象的XML数据的查询处理技术。     

Synthesis of novel functional polyolefin containing carboxylic acid via Friedel-Crafts acylation reaction

The strong polar group, carboxylic acid, has triumphantly been introduced into ethylene and allylbenzene copolymers without obvious degradation or crosslinking via Friedel-Crafts (F-C) acylation reaction with glutaric anhydride (GA), succinic anhydride (SA) and phthalic anhydride (PA) in the presence of anhydrous aluminum chloride in carbon disulfide. Some important reaction parameters were examined in order to optimize the acylation process. In the optimum reaction conditions, almost all of the phenyls can be acylated with any anhydride. The microstructure of acylated copolymer was characterized by FT-IR, ¹H NMR and ¹H-¹H COSY. All the peaks of acylated copolymers can be accurately attributed, which indicates that all the acylation reactions occur only at the para-positions of the substituent of the aromatic rings. The thermal behavior was studied by differential scanning calorimetry (DSC), showing that the melting temperatures (T_ms) of acylated copolymers with GA firstly decrease slowly and then increase significantly with the increase of the amount of carboxyl acid groups.     

池州发电厂一期工程综合试桩成果评价

池州发电厂一期工程在试桩过程中,进行了多项目的综合性试验。通过试桩比较,确定一期工程基础采用钢筋混凝土预制桩。从而满足了设计、施工、管理、检测所需要的各种参数,保证工程地基处理质量。     

Preparation and characterization of mullite whisker reinforced ceramics made from coal fly ash

Ceramics with mullite whiskers were prepared from coal fly ash and Al₂O₃ raw materials, with AlF₃ used as an additive. The phase structures and microstructures of the ceramics were identified via X-ray diffraction and scanning electron microscopy, respectively. The results show that pickling of coal fly ash is an effective method for enhancing the flexural strength of ceramics. Sintering temperature and AlF₃ addition were also key factors influencing the creation of ideal ceramics. The ceramic made from pickled coal fly ash, 6?wt% AlF₃, and sintered at 1200?°C, exhibited the highest flexural strength of 59.1?MPa, and had a bulk density of 1.32?g/cm³ and porosity of 26.8%. The results show that ceramic materials made under these conditions are ideal candidates for manufacturing ceramic proppants for the exploitation of unconventional oil and gas resources.     

一种新型常温微量氯气吸附剂热动力学研究

用一次等量浸渍法制备氯气吸附剂。在反应温度为常温、空速小于或等于1 000 h-1、进口氯气体积分数小于或等于400×10-6、出口氯气体积分数小于或等于0.1×10-6的条件下,吸附氯容量大于或等于11%。通过分析实验测得了热力学和动力学参数,结果表明,该吸附剂吸附氯气过程满足热力学的Fueundlich方程和动力学的Dubbin-Radushkevich方程,同时得出了有关吸附剂的反应机理。     

框架-剪力墙结构在水平荷载作用下的弯矩迭代计算

利用框架结构中同时考虑结点转动与侧移的弯矩迭代计算方法,分析了水平荷载作用下框架-剪力墙结构的内力并计算出结构的侧移变形。本方法适用于沿房屋高度方向层间刚度相同或不相同的框架-剪力墙结构,作用有任意分布形式的水平荷载。     

状态估计技术及其在聚合反应器控制中的应用

介绍了在线检测技术和状态估计技术，及利用状态估计技术获取单体转化率、聚合物相对分子质量分布和组成等产品特性，实现聚合反应器的在线控制的应用。     

青酶胺的研究现状及展望

本文详述了青酶胺的性质、应用和研究现状并展望其发展方向。     

控失尿素在夏玉米上的应用效果研究

通过田间试验,研究了控失尿素在夏玉米上的应用效果。结果表明,控失尿素追施处理比习惯施肥处理667 m2增产68.03 kg,增产率13.7%;控失尿素种肥同播处理比习惯施肥处理667 m2增产48.98 kg,增产率9.9%;控失尿素减量20%不会造成玉米产量下降;施用控失尿素可显著提高氮肥利用率。