集聚纺纱胶辊、胶圈的应用技术探讨

针对集聚纺纱对胶辊、胶圈的技术要求更高的特点,通过试验指出,胶辊硬度低、直径大有利于提高成纱质量.结合生产实践指出,精磨胶辊磨削量以0.2 mm为宜,表面粗糙度Ra值以0.4μm～0.5μm为宜,并适当缩短磨砺周期,牵伸胶辊与牵引胶辊应按比例控制磨削量.胶圈要新旧搭配,并且要及时清洗.     

蒸汽发生器二次侧清洁度的视频检查

立式平管板Ｕ形管束的压水堆核电站蒸汽发生器安装至瞬变工况期间，管板上表面的铁基金属残余物的堆积和外来物的存在，以及商业运行后管板、传热管、管子支撑板等的低流速区域里沉积物的堆积要求进行蒸汽发生器的清洁度检查。介绍了蒸汽发生器二次侧清洁度的视频检查技术。该技术适用于蒸汽发生器安装至瞬变工况和投入商业运行后可能发生污染的各阶段的清洁度检查。     

（1S，2S，5R）-薄荷基取代烯烃的合成

以(L)-薄荷基氯为原料,通过薄荷基氯化镁分别与烯丙基溴、2-甲基-3-氯丙烯、1-溴-3-甲基-2-丁烯在Cul催化下发生偶联反应,首次合成了3-(1S,2S,5R)-薄荷基-1-丙烯,2-甲基-3-(1S,2S,5R)-薄荷基-1-丙烯和2-甲基-4-(1S,2S,5R)-薄荷基-2-丁烯,总收率分别为80.5%、83.1%和79.6%.探讨了影响反应的多种因素,找到了较好的合成条件,并用IR、 1HNMR和元素分析对产物进行了表征.     

新理念催生新结构——IMTS2006观后感之三

自上世纪90年代以来,机床出现了许多新结构,其中绝大多数没有知识产权问题,也即没有专利的约束。在需要时,任何人均可采用。每一种结构均来自     

TEM method for rapid and precise evaluation of continuous recrystallization

With the aid of a double-tilt holder in a transmission electron microscope, a new method for a rapid and precise determination of the misorientations of a large number of subgrain or grain boundaries is given in this article. By use of the method, the continuous recrystallization can be rapidly and precisely evaluated when compared to the other conventional methods.     

Effect of polymerization conditions on o‐phenylenediamine and o‐phenetidine oxidative copolymers

A series of new o‐phenylenediamine (OPD)/o‐phenetidine (PHT) copolymers with partly phenazine‐like structures has been successfully synthesized at three polymerization temperatures by chemically oxidative polymerization in four different polymerization media. The molecular structures and properties of the resulting OPD/PHT polymers were investigated by IR, UV–vis and high‐resolution ¹H NMR spectroscopies, and DSC, in order to ascertain the effect of reaction temperature, comonomer ratio and acid medium. The copolymerization mechanism of OPD with PHT monomers has been proposed. It is found that the statistical OPD/PHT copolymer obtained at a temperature of 118 °C has a higher degree of polymerization than that obtained at 12–17 °C. The OPD content in the copolymers calculated from NMR spectroscopic analysis is higher than that in the feed OPD content, whereas the OPD content calculated from element analysis is slightly lower than the feed OPD content. It can be predicted that denitrogenation takes place in the OPD units during the polymerization process at OPD/PHT molar ratios of 90/10 and 100/0. These OPD/PHT copolymers exhibit a much better solubility than the OPD homopolymer, hence suggesting an incorporation of PHT units into the phenazine structure of the homopolymer. The thermal behavior of the copolymers was also studied. Copyright © 2004 Society of Chemical Industry     

隧道工程施工中应注意的问题

通过对海南省东线高速公路大茅山隧道施工的全程监理,阐明了在施工中应重点注意的几个问题,在此基础上,总结出隧道工程质量监督中必须做到的几点,以确保隧道工程施工安全及工程质量.