Synthesis of ultrafine LiCoO2 powders by the sol-gel method

Ultrafine high-temperature (HT) LiCoO₂ powders were synthesized by the sol-gel method using polyacrylic acid (PAA) as a chelating agent. The decomposition process of the gel precursor was examined to determine the crystallization temperature and the dependence of the physicochemical properties of HT-LiCoO₂ powders on the PAA quantity was extensively investigated. Polycrystalline HT-LiCoO₂ powders, composed of very uniformly sized ultrafine particulates with an average particle size of 30–50 nm and a specific surface area of 2.3–17 m²g^–1, could be obtained at the lower calcination temperature of 550 °C and the shorter calcination time of 1 h compared to the solid-state reaction.     

Fe－Cu包埋团簇的制备及其微观结构的研究

基于溅射－气体－聚集（ＳＧＡ）形成团簇的原理，提出了蒸发－气体－聚集（ＥＧＡ）共沉积方法，并在方华膜载网上成功地制备了Ｆｅ－Ｃｕ纳米磁性包理团簇样品。ＴＥＭ／ＥＤ分析表明，样品中Ｆｅ团簇被Ｃｕ原子所包裹，形成了以Ｆｅ团簇为芯，Ｃｕ膜为壳的良好的芯－壳式包埋结构。当衬底温度由２５℃变化到２００℃时，样品形貌由弥散状过渡到集团状，直至形成大的块状；其结构也相应的由Ｆｅ－Ｃｕ多晶共存变化为一种不规则的单晶形态。     

DF_4内燃机车柴油机润滑油的热重分析

通过对DF_4内燃机车柴油机润滑油的热重曲线TG和微商热重曲线DTG的分析,探讨了这种润滑油的衰变规律。     

油溶性减阻功能聚合物的研制

介绍了以混合α-烯烃为原料,制备了具有减阻功能的共聚物。讨论了催化剂浓度、聚合温度、预聚合时间、原料单体中杂质含量对共聚物特性粘度和转化率的影响。试验表明,在较低的催化剂浓度和预聚合温度下,能得到较高分子量的聚合物。气相色谱法和DSC法测定其组成和单体混合物的组成基本一致,表明共聚物是一种无规的梳状结构聚合物。该聚合物达到较高特性粘度时,能获得较好的减阻率。     

最小能量有限拍鲁棒控制系统的设计

本文采用2自由度控制器,以传递函数分式分解理论为基础,提出了一种在保证系统内部稳定和最佳鲁棒性前提下,实现最小能量控制的有限拍系统设计法。设计过程本质上是控制能量与响应时间的折衷。本文导出了折衷的最终界限,并给出了确定最佳响应时间的方法。     

目标机动规范模型研究

分析和总结了飞机各种机动动作的内在因素,提出了目标机动规范模型,研究了模型的数学描述方式、控制参量的相互约束关系及其组织形式,并通过模拟导弹对目标的攻击过程对模型进行了验证。     

低旋流进气直喷燃烧系统在195柴油机上的应用研究

介绍了低旋流进气直喷燃烧系统应用于１９５柴油机的试验结果，着重探讨了燃烧室结构尺寸和供油系统主要参数对柴油机性能和燃烧放热规律的影响。研究表明，这种燃烧系统应用于小缸径直喷柴油机具有良好的推广前景。     

Interface microstructure and reaction in Gr/Al metal matrix composites

The interface structure in Gr/Al composites fabricated with liquid metal infiltration has been studied using transmission electron microscopy (TEM). Morphologies of interfacial reaction product, aluminium carbide Al₄C₃, formed at different manufacturing parameters were compared and, the growth mechanism of the carbide was studied by means of high resolution electron microscopy (HREM). It has been shown that the morphology of the carbide is intimately related to the processing parameters with which the composites were produced. There are two kinds of interfaces between the carbide and the aluminium matrix. They have different growth mechanisms and relative growth rates under different growth driving forces. Several crystal orientation relationships between the carbide and the aluminium matrix have been observed.     

关于深冲薄钢板中的夹杂和成形性的商榷

对深冲薄钢板大生产的全工艺过程进行了跟踪，研究了ＷＹ０８ＡｌＡ薄钢板中Ａｌ＿２Ｏ＿３的形成，形态以及它们对冷轧成品的深冲性能和冲压小件的冲压成形废品率的影响。