铝阳极氧化膜颜色的检验和观察法

介绍铝及铝合金阳极氧化膜颜色的概念和描写,对颜色的儿种测量方法进行了比较,重点分析观察法及其在各国标准中的异同。在此基础上,提出了GB8013中的对颜色进行观察的条件和理论根据。     

二氧化硅包覆CsPbI3纳米晶薄膜的制备

卤化钙钛矿型(ABX3)纳米材料是近几年兴起的光电新材料,由于全无机钙钛矿CsPbX3(X=Cl,Br,I)纳米晶体的稳定性差,严重阻碍了实际应用,但因其具有窄带隙,在太阳能电池领域有着重要的应用前景.本研究在CsPbI3纳米晶周围使硅酸四甲酯(TMOS)发生水解反应,形成CsPbI3@SiO2纳米晶体复合材料,促使甲苯悬浮液的稳定性显著提高,发光稳定性可增加到29 d.通过进一步以聚(苯乙烯-乙烯-丁二烯-苯乙烯)三嵌共聚物(SEBS)对复合材料进行包裹,得到具有良好透明性和可拉伸性的SEBS/CsPbI3@SiO2薄膜,在水中有保持24 h稳定荧光现象,在水中12 h能保持原有发光强度的53％,而未经二氧化硅包裹的SEBS/CsPbI3纳米晶薄膜在水中仅8 h就失去荧光.本研究不仅为CsPbX3的表面改性提供了一种新方法,有助于解决稳定性问题,而且以聚合物复合的薄膜具有可拉伸性,也可应用在柔性器件中,具有重要的应用价值.     

风轮模拟试验平台的仿真与研究

分析风力机的特性,在上位机上搭建风力机的模型,通过上位机对变频器输入指令以实现对异步电机的控制,通过光电编码器和USB数据采集卡实现转速采集.设计一套基于LabVIEW的风轮模拟试验平台,为试验室的无风环境提供可控风速.提出一种转速控制方案并实现仿真,便于进行风力发电技术的研究.     

多孔β-TCP陶瓷药物载体的制备与体外释药速率的研究

本文用注浆成形的方法制备了以β-TCP为主晶相的多孔药物载体，体外测定了利福平的释药速率。实验结果表明，利福平在模拟体液中能够达到稳定的释放，可以作为骨结核手术后的辅助治疗。多孔β-TCP药物载体有望成为一种理想的药物缓释载体。     

软土地基油罐底板变形分析

分析了造成油罐底板变形的原因、形式及其危害，结合工程实例，提出了减少油罐底板不均匀变形的措施。     

Sex pheromone biology and behavior of the cowpea weevilCallosobruchus maculatus (Coleoptera: Bruchidae)

Female cowpea weevils,Callosobruchus maculatus (F.), emitted a pheromone which excited males. Pheromone release began soon after emergence and continued for one week. Synchronization of pheromone release with calling behavior was demonstrated. Mating reduced pheromone release but not male response. Pheromone obtained by aeration collection was utilized for determining a quantitative dose-response relationship.Mention of a commercial product does not constitute an endorsement by the USDA.Visiting scholar on leave from Shanghai Institute of Entomology, PRC.     

辽化裂解装置技术改造

辽阳石化烯烃厂裂解装置于2001年检修期间，完全采用国内技术，完成了120kt/a乙烯装置扩能改造工作，介绍了装置改造的主要内容和特点，生产运行和考核情况，以及扩能改造存在的问题和解决措施。     

Rapid pyrolysis of brown coal and oil shale

A brown coal, peat and oil shale were subjected to a rapid pyrolysis process and medium-heat-value gases together with tar were collected. The char residue was of high activity and suitable for gasification to create a two-stage gasification system. The coal-tar is used for manufacturing liquid fuels and chemicals.     

High temperature polymerization of propylene catalyzed by MgCl2‐supported Ziegler–Natta catalyst with various cocatalysts

Four cocatalysts, referred to as ethylaluminoxanes, were synthesized by the reaction between triethylaluminium (AIEt₃) and water under various molar ratios of H₂O/Al at ?78°C. Aluminoxanes were used as cocatalysts for a MgCl₂‐supported Ziegler–Natta catalyst for propylene polymerization at temperatures ranging from 70 to 100°C. When the polymerization was activated by AlEt₃, the activity as well as the molecular weight and isotacticity of the resulting polymer gradually dropped as the temperature varied from 70 to 100°C. When ethylaluminoxane was employed as the cocatalyst, good activity and high molecular weight and isotacticity were obtained at 100°C. Furthermore, when the cocatalyst varied from AlEt₃ to ethylaluminoxane, the atactic fraction and polymer fraction with moderate isotacticity decreased and the high isotactic fraction slightly increased, which indicated that the variation of the cocatalyst significantly affects the isospecificity of active sites. It was suggested that the reactivity of the Al‐Et group and the size of the cocatalyst were correlated to the performance of the Ziegler–Natta catalyst at different temperatures. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1978–1982, 2006     

认识隐患预防事故

事故隐患是客观存在的，不论你是否承认，是否意识到，它都存在于企业的生产全过程，而且对员工的人身安全，国家的财产安全和企业的生存、发展都直接构成威胁。正确认识隐患的特征，对熟悉和掌握隐患产生的原因，及时研究并落实防范对策是十分重要的。下面就这方面的问题，谈一点粗浅认识。