助催化剂对TiCl_4/MgCl_2催化丙烯高温聚合的影响

研究了助催化剂种类(三甲基铝、三异丁基铝、三正己基铝、三乙基铝和甲基铝氧烷)及其含量对无内、外给电子体的TiCl4/MgCl2催化剂催化丙烯高温(100℃)聚合性能的影响,并用结晶分级分析、示差扫描量热和凝胶渗透色谱等方法分析了所得聚丙烯的结晶熔融行为和微观结构。实验结果表明,聚合温度从70℃升至100℃时,TiCl4/MgCl2催化剂的定向能力基本不变;100℃聚合时,以烷基化能力较弱的三异丁基铝为助催化剂时TiCl4/MgCl2催化剂的活性最高,而采用烷基化能力最强的三甲基铝为助催化剂时TiCl4/MgCl2催化剂的活性最低;100℃聚合时,助催化剂的种类对TiCl4/MgCl2催化剂的定向能力影响很小。     

Shape-Controlled Synthesis and Upconversion Luminescence of Y2O3:Yb, Er Microstructures

The Y2O3: Yb3 , Er3 microstructures were fabricated by a hydrothermal method without surfactants.The microstructures structure was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM,KYKY 1000B).The up-conversion luminescence spectra were studied under 978 nm laser diode excitation.In Yb3 and Er3 codoped Y2 O3 microcrystals, the relative intensity of green emission became stronger as the morphology of sample changed from wires to films.     

高速线材生产的弹簧钢盘卷的表面脱碳分析

从金相角度对高线生产的弹簧钢盘卷的表面脱碳进行了分析，找出相关的影响因素，并针对实际情况提出了相应的改进方法。     

Composition Range of Amorphous Mg-Ni-Y Alloys

Based on the thermodynamic point of view, a method for predication of the composition range of amorphous ter-nary alloys was proposed. The composition range of amorphous ternary alloys is determined by the comparison of the excess free energy of the amorphous alloy and the free energy of competing crystalline states. The free energy is extrapolated from the data of three binary alloys by using Toop‘s model. The method was applied to predict the composition range of amor-phous Mg-Ni-Y alloys. The theoretical results are in good agreement with the available experimental results. It indicates that the present method can be used to predict the composition range for amorphous ternary alloys.     

发生在北美的合成内燃机油定义之争

加氢异构化油是不是合成油?简述了20世纪90年代末重新激活的合成油定义之争、NAD的裁决以及该裁决对各润滑油公司和合成基础油市场的影响.     

Deposition and Properties of Superconducting MgB2 Thin Films

The recently discovered superconductor MgB₂ with T _c at 39 K has great potential in superconducting electronics. In this paper, we review the deposition techniques used for MgB₂ thin films in the light of a thermodynamic study of the Mg-B system with the calculation of phase diagrams (CALPHAD) modeling technique. This thermodynamic study identifies a growth window in the pressure–temperature phase diagram, in which the magnesium pressure is very high for likely in situ growth temperatures. A Hybrid Physical–Chemical Vapor Deposition (HPCVD) technique that successfully achieves such a high Mg pressure is shown to produce in situ epitaxial MgB₂ thin films with bulk superconducting properties.     

一种基于混沌的随机数发生器设计及其IC实现

在密码学、仿真学以及集成电路测试等许多领域 ,随机数起着重要的作用。在密码学中 ,通常要求所使用的随机数具有不可预测性。基于混沌现象 ,使用开关电容技术 ,用集成电路实现了一种硬件随机数发生器。测试结果表明 ,其产生的序列具有不可预测性 ,可以满足密码学的应用要求。     

税库行横向联网系统接口处理平台的设计与实现

文章介绍了湖南省国税局横向联网系统接口处理平台的设计方案，对应用接口的体系结构、业务流程、接口数据结构和数据传输等进行了讨论，建立了基于javasocket和java多线程等主要技术的系统基本框架，重点阐述了系统的业务流程实现方式。该方案实现了异构系统间的数据交换，很好地解决了税务、国库和银行之间“信息孤岛”的问题，确保了横向联网系统安全稳定运行。     

EXPERIMENTAL INVESTIGATIONS ON LONGITUDINAL DISPERSION CHARACTERISTICS OF TIDAL RIVERS

1 .　ＩＮＴＲＯＤＵＣＴＩＯＮＵｎｄｅｒｔｈｅｉｎｆｌｕｅｎｃｅｏｆｎａｔｕｒａｌｔｉｄｅｓ,ｔｈｅｉｎｔｅｒａｃ ｔｉｏｎｓｂｅｔｗｅｅｎｆｌｏｗｆｅａｔｕｒｅｓａｎｄｐｏｌｌｕｔａｎｔｌｏｎｇｉｔｕｄｉｎａｌｄｉｆｆｕｓｉｏｎｉｎｔｉｄａｌｒｉｖｅｒｓａｒｅｉｍｐｏｒｔａｎｔｆｏｒｗａｔｅｒｅｎｖｉ ｒｏｎｍｅｎｔｒｅｃｔｉｆｉｃａｔｉｏｎｉｎｅｓｔｕａｒｉｎｅｒｅｇｉｏｎｓ.Ｔｈｅｄｉｆｆｕ ｓｉｏｎａｎｄｔｒａｎｓｐｏｒｔｏｆｐｏｌｌｕｔａｎｔｉｎｎａｔｕｒａｌｒｉｖｅｒｓｆａｌｌｉｎ ｔｏｍ…     

基于组织协同进化分类算法的遥感图像目标识别

针对遥感图像目标识别问题,提出了一种基于组织协同进化分类算法的识别方法。它没有复杂的运算,训练和识别速度都很快。对实测遥感图像的实验表明,本文方法性能稳定,优于文献[3]和[4]中基于支撑矢量机的方法,识别率均达到了95％以上,且训练时间非常短,不到1秒钟。