Sol-Gel Preparation of LaNiO3 and Its Physical and Chemical Properties

LaNiO3 was synthesized by sol-gel method in which lanthanum nitrate and nickel nitrate were used as start materials and citric acid was used as complex for gel formation.The precursor was dried and subsequently heated at elevated temperature to form the desired product.XRD analysis shows that pure LaNiO3 was synthesized.Electrical conductivity and electrochemical performance of the material were tested.The electrical conductivity decreases from 34.5that there are current peaks in the curve, which is the evidence of the electrochemical activity of LaNiO3.     

技术攻关提高成材率

介绍了广钢集团高速线材生产线的生产和工艺概况，分析了成材率的影响因素，阐述了技术攻关提高成材率所采取的措施和取得的良好效果及经济效益。     

赴日无线电监测技术考察报告

首先介绍了日本总务省关东综合通信局电波监理部的情况，然后对日本安立公司生产的RR510A型无线电监测接收机和技术参数以及MS8609A型数字移动无线发射机测试仪的功能进行了分析和介绍。     

Bipolar electric fatigue behaviour as a function of field strength in antiferroelectric (Pb,Ba,La)(Zr,Sn,Ti)O3 ceramics

The bipolar electric fatigue behaviour of antiferroelectric ceramics with the composition of Pb_0.88Ba_0.10La_0.02(Zr_0.55Sn_0.35Ti_0.10)O₃ was investigated under various cycling fields. The material exhibits a degradation in the maximum field induced strain, a diffuse AFE-FE phase transition and an enhancement in the diffusion character of the FE-AFE phase transition due to electric cycling. Those variations increase with cycle number, indicating a logarithmic fatigue up to 10⁸ cycles. There is no indication for the variations to be recovered, and the symmetry of the negative and positive parts of the strain hysteresis loops still remains. Higher cycling field results in a stronger deterioration of the maximum field induced strain and a larger extent of diffusion in AFE-FE and FE-AFE phase transitions. The normalized maximum strain shows nearly the same scale of degradation when the materials are cycled at various electric fields. After a heat treatment at 500°C for 1 h, the variations in the AFE-FE and FE-AFE phase transition due to cycling disappear, whereas the maximum strain resumes almost to its original value. Electrochemical variations are considered to contribute to the main fatigue mechanism for the material under investigation.     

Tensile and flexural creep rupture tests on partially-damaged concrete specimens

Three series of novel tensile and flexural creep tests on partially-damaged concrete specimens were carried out in order to gain some insight into creep crack growth and failure of strain-softening materials. In the tests, each specimen was initially loaded to a given point in the descending branch and thus had a lower load-carrying capacity than that at the peak-point. Then, the specimen was unloaded and reloaded to sustain a load which was from 70% to 95% of its current load-carrying capacity. Experimental creep curves display a three-stage process, consisting of primary, secondary and tertiary stages, with a decreasing, constant and increasing creep rate, respectively. The secondary stage dominates the whole failure lifetime, whereas both the secondary and tertiary stages are important in terms of creep deformation. Failure life-time seems to be more sensitive to the change of load level in flexural tests rather than in tensile tests. The decrease in load-carrying capacity due to damage tends to result in a shorter failure lifetime and a lower critical load level for creep rupture. The descending branch of the static load-deflection or load-CMOD curve may be used as an envelope criterion for creep fracture.     

爆炸焊接——热轧双相不锈钢复合钢板研制

本文主要阐述了通过爆炸焊接和热轧的方法,研制成功可焊性良好的且具有较好强度、韧性与综合性能的双相耐应力腐蚀的不锈复合钢板。还将热轧与热处理的两种试验作了较全面的常规、特殊检验试验,结果完全达到使用要求。     

烧成及热处理工艺对钛酸锶铅基热敏材料性能及显微结构的影响

研究了烧成及热处理工艺对钛酸锶铅基热敏材料的阻温特性及显微结构的影响。通过扫描电镜（ＳＥＭ）和能量分散仪（ＥＤＡＸ）分析了材料的显微结构及不同形貌晶粒的成份。通过对组成、烧成及热处理工艺的控制，可得到具有Ｖ型ＰＴＣＲ特性的热敏材料。     

正交双频光栅CCD系统剪切干涉测量二维温度场

以半导体激光器为光源，利用正交双频光栅（ＯＤＦＧ）ＣＣＤ系统剪切干涉对带平板边界的半圆柱体热源的二维温度场进行实时诊断，分析剪切干涉图时，用柱函数系作为拟合基底，给出二维自然对流温度场的定量分布。     

改善磁盘阵列性能的方法

磁盘阵列是解决计算机Ｉ／Ｏ瓶颈问题的有效方法之一，通过对现有磁盘阵列结构的研究，提出了４种改善磁盘阵列性能的方法，即良分利用磁盘带宽，平衡多盘的负载，减少奇偶检验数据存取时间和磁盘阵列Ｃａｃｈｅ技术等，分析结果表明：在事务处理应用领域，利用Ｃａｃｈｅ来把小写转化为大写可大大改善目前一般情况下，以一道数据大小来作为磁盘的基本存取大小是合适的选择，磁盘阵列负载平衡设计不足是指正常模式下系统请求在多盘间