高负荷下聚酯工艺参数的优化

介绍原 2 0万t/a装置增容到 2 4万t/a时的工艺参数优化。PTA平均粒径 95～ 110 μm ,n(EG) /n(PTA) =2 .6～ 2 .7,酯化液位 63 %～ 64 % ,温度 2 92～ 2 96℃ ;乙二醇锑催化剂 ,稳定EG、DEG量 ,选择TiO2 消光剂 ,滤除凝聚粒子 ;预缩聚温度 2 87～ 2 89℃ ,压力 2 .4～ 2 .8kPa,液位 42～ 48cm ;终缩聚温度 2 90～ 2 91℃ ,压力 2 .5～ 3 .0hPa,液位 60～ 62cm ,搅拌速度 2 .7r/min。     

对策论在雷达阵地综合防护效能分析中的应用

针对雷达阵地的防护特点,运用对策论的基本原理探索雷达阵地综合防护效能分析问题.构建了雷达阵地综合防护效能分析指标体系,结合对策论建立了评估模型,并用实例检验该方法具有较好的应用价值.     

Electroless nickel plating on the surface of carbon fibers

The electroless nickel plating on the surface of carbon fibers was prepared by pretreating the carbon fibers in order to increase their conductivity,and consequently enhance the EMI shielding effectiveness of the composites.The relationship between the performance of depositing coat and pH value,temperature,reaction time and the way of agitation was studied.Results show that the depositing quality is stable under pH between 4.5 and 5.0,temperature between 75 ℃ and 85 ℃,reaction time for 10 min and air agitation.The uniform and compact nickel layer deposited on carbon fibers was proved by XRD and SEM,and the electrical resistivity of carbon fibers with nickel coating was tested.Results indicate that the electrical resistivity of carbon fibers with electroless nickel plating is decreased by an order of magnitude compared with that of carbon fibers.It means that nickel coating can greatly improve the electromagnetic interference shielding properties of carbon fibers.     

灰色线性回归组合模型在计算给水管道阻力系数中的应用

为了求解管道阻力系数,将其应用到工程中的水力计算中,运用灰色线性回归组合模型进行求解,得出了计算管道阻力系数的数学模型,并结合工程实例进行验证.实践表明该模型的精度较高,具有一定参考价值.     

CPCI架构MVB通信卡硬件设计与实现

简要介绍多功能车辆总线(MVB)总线及CPCI总线的特点,通过分析列车通信系统和局部总线技术,给出了基于CPCI的MVB总线通信网卡的硬件设计与实现方案.通信网卡的硬件包括本地处理器、MVB控制器、本地总线逻辑、CPCI接口信号及热插拔电源管理电路等.通过调试,通信卡的各项功能达到了设计目标,符合IEC-61375国际标准,可以应用于实际.     

强磁场对硅锰铸钢于A_1点附近等温珠光体相变的影响

通过开展12 T强磁下硅锰铸钢(50Si_2Mn_3)于A_1点温度附近不同等温时间的热处理试验,并对比强磁场与无磁场条件下等温珠光体相变试验结果,研究了磁场对珠光体转变量及组织形貌的影响。研究表明,对于50Si_2Mn_3在A1点以下较高温度范围内,强磁场可缩短珠光体相变的孕育期,促进硅锰铸钢珠光体转变,使其转变量明显增加;强磁场能够提高珠光体转变临界点,使50Si_2Mn_3在A1点以上等温过程中能够发生珠光体相变。     

Numerical investigation on flow and convective heat transfer of aviation kerosene at supercritical conditions

In this paper,characteristics of flow and convective heat transfer of China RP-3 kerosene in straight circular pipe were numerically studied.Navier-Stokes equations were solved using RNG k-turbulence model with low Reynolds number correction.The thermophysical and transport properties of the China RP-3 kerosene were calculated with a 10-species surrogate and the extended corresponding state method(ECS) combined with Benedict-Webb-Rubin equation.The independence of grids was first studied and the numerical results were then compared with experimental data for validation.Under flow conditions given in the paper,the results show that deterioration of convective heat transfer occurs when the wall temperature is slightly higher than the pseudo-critical temperature of kerosene for cases with wall heat flux of 1.2 and 0.8 MW/m 2.The degree of the heat transfer deterioration is weakened as the heat flux decreases.The deterioration,however,does not happen when the heat flux on the pipe wall is reduced to 0.5 MW/m 2.Based on the analysis of the near-wall turbulent properties,it is found that the heat transfer deterioration and then the enhancement are attributed partly to the change in the turbulent kinetic energy in the vicinity of pipe wall.The conventional heat transfer relations such as Sieder-Tate and Gnielinski formulas can be used for the estimation of kerosene heat convection under subcritical conditions,but they are not capable of predicting the phenomenon of heat transfer deterioration.The modified Bae-Kim formula can describe the heat transfer deterioration.In addition,the frictional drag would increase dramatically when the fuel transforms to the supercritical state.     

Annexin V的125I标记及其在正常小鼠体内的分布

采用Iodogen法对Annexin V进行了^125I标记,并观察了其在正常小鼠体内的分布情况.标记结果显示,^125I-Annexin V 标记率达94.9%,纯化后放化纯度达99%;室温放置72 h后,放化纯度仍保持在92%以上,表明其体外稳定性较好.生物分布结果显示,^125I-Annexin V在肾脏中放射活性最高,其次为血液、肝脏、心、肺、脾;脑不吸收^125I-Annexin V;肌肉、骨骼组织摄取亦较少;各组织、器官放射性摄取在1 h内除血液下降稍慢外,其余均有明显下降.表明^125I-Annexin V 适合用作核医学诊断试剂.     

中小型铝电解厂供电系统调度运行方式的探讨

公司2 0 0kA电解槽投产后,用电负荷增大,自备电厂负荷小,不能满足生产需求,由于所在地区电网薄弱,供电不稳定,特别是遇到发、供电设备检修和突发故障时,电流强度波动大,对电解槽生产影响较为严重。根据这种现状,经过长期运行实践,制定了不同设备检查及故障状态下35kV发、供电系统生产调度运行的最佳方式,保证了企业正常生产,提高了企业经济效益     

智能电磁流量计及其组态

介绍了电磁流量计的工作原理、安装与使用要点、智能终端的使用与电磁流量计的组态方法等