双级时效对1420铝锂合金超塑性的影响

采用金相、透射电镜、高温拉伸等检测手段研究了双级时效对1420铝锂合金组织及超塑性的影响,结果表明:与单级时效相比,双级时效处理得到分布更均匀、体积分数更大的析出相粒子.双级时效经过轧制和再结晶退火后,得到的晶粒尺寸为8～12μm;500℃条件下8×10-4s-1超塑性伸长率达到860%.第一级低温时效先在基体形成较均匀的细小粒子,这些粒子不仅在晶界,也在晶内大量析出.在高温时效时,这些粒子长大形成分布均匀,体积分数大的析出相粒子.     

SPS烧结时间对Ti_2AlNb合金组织与力学性能的影响

采用高能球磨法和放电等离子烧结技术（SPS）制备了Ti_2AlNb合金,研究了不同烧结时间对Ti_2AlNb合金微观组织及力学性能的影响。利用扫描电子显微镜（SEM）和X射线衍射仪（XRD）对合金显微组织及物相结构进行表征,利用万能拉伸试验机对合金拉伸性能进行测试。结果表明,烧结时间不会改变合金的物相组成,不同烧结时间下所制备的Ti_2AlNb合金均由B2相、胞状α2相和针状O相组成;在烧结温度1000℃、烧结时间70min、压强50MPa条件下,Ti_2AlNb合金中针状O相数量较多且分布均匀,其室温拉伸强度可达454.6 MPa。     

Formation mechanism of gradient-distributed particles and their effects on grain structure in 01420 Al-Li alloy

Fine-grained 01420 Al-Li alloy sheets were produced by thermo-mechanical processing based on the mechanism of particle stimulated nucleation of recrystallization. The thermo-mechanically processed sheets were observed to contain layers of different microstructures along the thickness. The precipitate behavior of the second phase particles and their effects on the distribution of dislocations and layered recrystallized grain structure were analyzed by optical microscopy（OM）, scanning electron microscopy（SEM）, transmission electron microscopy（TEM） and X-ray diffractometry（XRD）. The formation mechanism of the gradient particles was discussed. The results show that after aging, a gradient distribution of large particles along the thickness is observed, the particles in the surface layer（SL） are distributed homogeneously, whereas those in the center layer（CL） are mainly distributed parallel to the rolling direction, and the volume fraction of the particles in the SL is higher than that in the CL. Subsequent rolling in the presence of layer-distributed particles results in a corresponding homogeneous distribution of highly strained regions in the SL and a banded distribution of them in CL, which is the main reason for the formation of layered grain structure along the thickness in the sheets.     

Evolution of grain structure in AA2195 A1-Li alloy plate during recrystallization

The evolution of the grain structures in AA2195 Al-Li alloy plate warm-rolled by 80% reduction during recrystallization annealing at 500℃ was investigated by electron backscatter diffraction, scanning electron microscopy and transmission electron microscopy. It is found that the elongated grain structures are caused by the lamellar distribution of recrystaUization nucleation sites, being lack of large second phase particles （〉 1μm）, and dispersive coherent particles （such as δ′ and β′concentrated in planar bands. The recrystallization process may be separated into three stages： firstly, recrystallization nucleation occurs heterogeneously, and the nuclei are concentrated in some planar zones parallel to rolling plane. Secondly, the grain boundaries interacted with small particles concentrate in planar bands, which is able to result in the elongated grain structures. The rate of the grain growth is controlled by the dissolution of these small particles. Thirdly, after most of small particles are dissolved, their hindrance to migration of the grain boundaries fades away, and the unrecrystallized zones are consumed by adjacent recrystallized grains. The migration of high angle grain boundaries along normal direction leads a gradual transformation from the elongated grains to the nearly equiaxed, which is driven by the tension of the grain boundaries.     

Development of cube texture in multistage annealing of high purity aluminum foils

1　INTRODUCTIONThecubetextureisimportanttohighpurityalu minumfoilsforhighvoltagecapacitorsbecauseitcanenlargeeffectivesurfaceofaluminumfoilsandin creasecapacitancethroughchanneletching .Inordertoincreasethevolumefractionofthecubecompo nent ,a greatdealofresearchesontheformationmechanismofcubetexturehavebeendone ,andmanymethodswere proposed ,suchasimpuritycontrol ling[1,2 ] ,directionalsolidification[3] ,preheating[4 ] ,inhomogeneousrolling[5] ,vacuumannealing[6 ] andsoon .Inthispaperamulti…     

热变形参数对TC11合金微观组织的影响

在Gleebe-1500型热模拟试验机上进行了TC11合金在变形温度1023～1233K、应变速率0.001～10.0s-1、变形程度30％～70％时的热模拟压缩试验.结果表明,在α+β两相区变形时,变形温度对初生α相晶粒尺寸有影响;高应变速率下变形时,在一定的变形温度下合金内部将发生动态再结晶,且随变形程度增大,再结晶温度逐渐降低.同时,应变速率、变形程度和变形温度对合金动态再结晶发生的影响逐渐减小;确定了合金发生动态再结晶的最佳变形参数是在应变速率1.0 s-1附近,变形程度约50％,变形温度1123～1213K.     

固溶温度对Ti6246钛合金组织与性能的影响

对Ti6246钛合金?200 mm棒材进行不同温度固溶和593℃时效处理,研究了固溶温度对合金显微组织及力学性能的影响。结果表明,当固溶温度在860~900℃时,初生α相和次生α相的含量和尺寸变化较小,显微组织为典型的等轴组织,棒材的室温和高温拉伸性能均变化不大,蠕变性能有所提高;当固溶温度高于915℃时,初生α相含量明显下降,次生α相的含量有所增加,且次生α相的尺寸增长变宽,显微组织呈双态组织,室温和高温拉伸强度均不断降低,塑性反之,且高温塑性的提高幅度明显大于室温塑性,蠕变性能进一步提高。     

热处理对TA15钛合金棒材冲击性能的影响

研究了热处理制度对TA15钛合金棒材显微组织的影响,并测试了热处理后试样的冲击性能.结果表明:通过调整退火温度及保温时间,可改变合金的显微组织,提高TA15钛合金的冲击性能.TA15钛合金在初生a相的形状和大小基本相同的情况下,次生a相的形状和大小对冲击韧度的影响比较大.次生a为条状时的冲击值明显高于次生仅为圆形或短棒状时的冲击值.经810℃×2h,AC热处理后,可获得冲击性能良好的TA15钛合金棒材,并且冲击性能提高了35%.     

基于晶体取向q值计算再结晶分数的改进方法

以大变形高纯铝在300℃的退火试样为例,提出了一种基于EBSD数据中q值计算再结晶分数的改进方法,该方法通过分离不同取向的q值数据,对于不同的取向数据分别采用Tarasiuk提出的q值积分算法计算再结晶分数,即与完全再结晶状态及变形态的q值数据进行对比并积分计算,再按各取向的再结晶分量权重求和得出总体的再结晶分数.结果...     

锻造工艺对Ti-6321合金棒材显微组织与力学性能的影响

研究了不同锻造工艺对Ti-6321合金棒材组织与力学性能的影响。结果表明:Ti-6321合金棒材经常规锻造后为等轴组织,经近β锻造后为双态组织,经β锻造后为网篮组织;双态组织不仅具有与等轴组织和网篮组织相当的强度和塑性,而且冲击韧性可达到850 kJ/m2以上,明显高于等轴组织和网篮组织。