B和MoS_2添加量对Ni-Cr合金基材料高温摩擦、磨损行为的影响

本文以Ni-Cr高温合金粉为基,其间添加Mo,B和少量MoS_2。用粉末冶金热压法制备了含不同B和MoS_2添加量的Ni-Cr合金基自润滑材料。借助X射线衍射仪分析了材料结构,用布氏硬度计测试了材料硬度。以研制材料为销样,Al_2O_3陶瓷为盘样,在销-盘式高温摩擦试验机上考察材料在20～700℃温度范围内的摩擦磨损行为。试验结果表明,研制材料主要由Ni基固溶体、Cr_3S_4和MoB 3种相组成。材料硬度随B含量的增加而增加,但高温下其摩擦因数也随之增加。MoS_2添加量为4％(质量分数)的研制材料在20～700℃温度范围内有最佳减摩耐磨综合性能。     

Preparation and properties of β-tricalcium phosphate porous bloceramlc

Porous β-tricalcium phosphate bioceramic (PTCP) has important roles in surgical implants because of good biocompatibility. But the low compressive strength of the ceramic limits its application. The preparation of PTCP was improved with the adjustment of the constituents and the sintering-process. A new type of PTCP material with high compressive strength was made. The compositions, microstructure and properties of PTCP were analyzed by TG-DSC, XRD, TEM, SEM and so on. The result indicates that stearic acid burns sufficiently and gives out carbon dioxide and water vapor when slowly heated between 200℃ and 400℃ so that the porous structure like coral in β-TCP bioceramic is formed. Through crystallization at 470℃ and 570℃, more CaO-P2O3 glass-cement is converted into crystallite-glass, which is beneficial for improving the compressive strength of β-TCP bioceramic. PTCP can form a support action in bone imperfect section with good solubility.     

Ni-PS-MoS2复合镀层的制备及摩擦磨损性能

用苯乙烯单体聚合反应法,在MoS2微粒表面包覆一层聚苯乙烯,经红外线光谱检测证明聚苯乙烯成功包覆在MoS2表面上.制备Ni-MoS2及Ni-PS/MoS2复合镀层试样,在镀液中微粒浓度相等的情况下,复合镀层中PS/MoS2微粒比MoS2微粒含量高.用扫描电镜观测复合镀层表面和截面彤貌,Ni-PS/MoS2复合镀层表面比Ni-MoS2复合镀层表面平整规则.在圆-盘式摩擦磨损试验机上进行复合镀层的摩擦磨损性能测试,结果表明制备工艺相同时,Ni-PS/MoS2复合镀层的摩擦学性能均优于Ni-MOS2复合镀层,镀液中微粒浓度25 g/L时,Ni-PS/MoS2复合镀层的摩擦学性能最好.     

具有木材结构Al/C、Al/(SiC+C)复合材料的制备及热学性能

该研究以柳桉木材结构为模板,通过对木材的碳化、硅树脂的浸渍与反应、铝合金的浸渍处理,制备了具有木材结构的Al/C、Al/(SiC C)两种复合材料,并对复合材料的微观结构、热膨胀性能及导热性能进行了研究.结果表明:该复合材料保持了所选木材的天然结构特征,并且其热膨胀系数明显低于铝合金,导热系数远高于由木材转化的多孔碳.