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31.
A robust Fault Diagnosis (FD) scheme for a real quadrotor Unmanned Aerial Vehicle (UAV) is proposed in this paper. Firstly, a novel Adaptive Thau observer (ATO) is developed to estimate the quadrotor system states and build a set of offset residuals to indicate actuators’ faults. Based on these residuals, some rules of Fault Diagnosis (FD) are designed to detect and isolate the faults as well as estimate the fault offset parameters. Secondly, a synthetic robust optimization scheme is presented to improve Fault Estimation (FE) accuracies, three key issues include modeling uncertainties, and magnitude order unbalances as well as noises are addressed. Finally, a typical fault of rotors is simulated and injected into one of four rotors of the quadrotor, and experiments for the FD scheme have been carried out. Unlike former research works on the FD schemes for quadrotors, our proposed FD scheme based on the ATO can not only detect and isolate the failed actuators, but also estimate the fault severities. Regardless of roughness of the real flying data, the FD results still have sufficient FE accuracies.  相似文献   
32.
Majorana syriaca is an important food‐flavouring ingredient in the Middle Eastern culture known commonly as Za'atar. The components of the plant were extracted in a Soxhlet apparatus sequentially with solvents of increasing polarity, specifically with petroleum ether (P), diethyl ether (D), ethyl acetate (EAc), and ethanol (E). The activity of the extracts to scavenge the 2,2‐diphenyl‐1‐picrylhydrazyl radical (DPPH?) followed the order D > E > EAc > P. Moreover, the antioxidant activity in corn oil at concentrations of 200, 500 and 1000 ppm was monitored through peroxide value and conjugated hydroperoxide measurements and revealed that D and E extracts resulted in the highest protection followed by EAc and P extracts. Increasing the concentration from 200 to 500 ppm depressed peroxide formation, while a further increase had no effect. The main components of the P extract according to GS‐MS analysis were thymol (42.89%) and carvacrol (42.75%). The remaining extracts comprise flavonoids and phenolic acids that provide the antiradical and antioxidant activity.  相似文献   
33.
A new polymeric system has been applied for structural modification of (noncompactable) sandy soils. The system is based on a water‐borne styrene acrylic polymeric formulation (emulsion) containing varying amounts of solid polymer. The present work deals with system optimization and measurements designed to examine the effects of polymer content on hydraulic conductivity and compressive strength. Samples were prepared from prescribed amounts of polymer, water, and sand by using two different preparations methods (mixing and spraying). Measurements of hydraulic conductivity for both sets of samples were conducted in a flexible membrane test apparatus. For the first set of samples, the permeability coefficient of the sand was noted to be reduced 10‐fold (from 10?5 to 10?6 m s?1) upon the incorporation of about 2% polymer. In the second set (samples prepared with the spraying method), the hydraulic conductivity was further reduced to 7.2 × 10?7 at a polymer concentration of about 2%. Stress–strain measurements made on dry cylindrical specimens disclosed remarkable enhancement in the mechanical behavior of the system. For both types of preparation methods, the compressive strength and modulus of elasticity increased linearly with the polymer concentration in the sample. Scanning electron microscopic examination revealed that the dramatic reduction in the permeability and the improved mechanical properties are attributed to the polymer coverage of the sand particles and the development of interconnecting ties between them. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 2484–2491, 2003  相似文献   
34.
Batch experiments were carried out to asses the effect of Cu(II) and Zn(II) on the biosorption of lead(II) ions by non-living Chlorella vulgaris. The uptake of Pb(II) was examined for single, binary and ternary solutions at different initial concentrations and different pH values. The experimental results showed that the uptake increased with increasing pH from 3.0 to an optimum value of 5.0. The biosorption of Pb(II) was found to be adversely affected by the presence of Cu(II) ions, while Zn(II) ions seemed to have negligible effect on the process. The equilibrium data were fitted to four isotherm models: Langmuir, Freundlich, Sips and Dubinin–Radushkevich; the Sips isotherm gave the best fit for the data. Modeling of the controlling mechanisms indicated that both intrinsic kinetics and mass transfer played major roles in controlling the process. A new dimensionless parameter, Ψ, was defined to asses the relative contributions of the two mechanisms to the biosorption of lead(II). Mass transfer seemed to be the dominant mechanism at low initial lead(II) concentrations, while intrinsic kinetics dominates at high concentrations.  相似文献   
35.
The present study was designed to examine the effects of EFA deficiency (EFAD) on biochemical, functional, and structural aspects of the kidney in growing and adult rats fed a normal or EFAD diet for 9 wk after weaning. Food and fluid intake (FI), urine volume, and Na+ and K+ excretions were measured weekly from weeks 4 to 8 by placing the rats in individual metabolic cages for 24 h. At week 9, Li+ and a 5% water load, respectively, were administered at 14 and 1.5 h prior to glomerular and proximal tubular function studies, as assessed by 3-h creatinine (CCr) and Li+ (CLi+) clearances. Hematocrit and urine volume; serum and urine [Cr], [Li+], [Na+], and [K+]; and renal FA distribution were also measured. Data [corrected to 100 g/body weight (bw) and presented as means ±SEM] were significant, at P<-0.05. Despite a similar ingestion of solids from weeks 4 to 7 (weeks 7 to 10 of life), the rats on the EFAD diet showed a decreased body weight from week 5. From weeks 4 to 8, Fl and urine volume were similar for both groups, but the Fl increased at week 6 in the EFAD group; 24-h Na+ and K+ excretions were similar at all weeks, except for an increase in the EFAD group for both ions at week 7. In the EFAD group, CCr and CLi+ decreased by 27 and 56.3%, respectively (385.7±33.4 vs. 280±21.1, and 21.0±2.1 vs. 9.2±1.1 μL/min/100 g; n=9 vs. 10), the latter result suggesting increased proximal reabsorption. The 3-h Na+ and K+ excretions were similar, but the Li+ decreased (0.78±0.06×10−2 vs. 0.32±0.03×10−2 μeq/min/100 g) in the EFAD group, giving additional support to the suggestion. Renal structure was normal and similar for both groups, but the EFAD group showed a more prominent proximal tubule brush border, together with heavier periodic acid-Schiff staining in all specimens from weeks 5 to 9. In the EFAD group, FA of the n−9 and n−7 series were higher, but most of the n−6 series were lower as a percentage of total lipids in the medulla and cortex. Medullary levels of 20∶4n−6 were maintained, 22∶4n−6 declined twice, arachidonic acid was maintained, and 20∶5n−3 was lower. The EFAD diet affected glomerular function, proximal tubular structure and function, and FA distribution in the rat kidney.  相似文献   
36.
Indium tin oxide‐coated thin films (200 nm) are deposited on glass substrates by using R.f. sputtering technique. Here, we investigate the influence of new technique of treatment, which is called as “oil thermal annealing” on the nano‐structured indium tin oxide thin films at fixed temperature (150 °C) which improves adhesion strength, electrical conductivity and optical properties (transmittance) of the films. Oil thermal annealing is used to reduce inherent defects that may be introduced during the prepared thin film and cooling processes. Proposed technique is highly suitable for liquid crystal displays, solar cells and organic light emitting diodes, and many other display‐related applications.  相似文献   
37.
Miniemulsion copolymerization of styrene/n‐butyl acrylate was investigated as a means of encapsulating hydrophilic titanium dioxide (TiO2) in a film‐forming polymer. Dispersion studies of the TiO2 were first carried out to determine the choice of stabilizer, its concentration, and the dispersion process conditions for obtaining stable TiO2 particles with minimum particle size. Through screening studies of various functional stabilizers and shelf‐life stability studies at both room and polymerization temperatures, Solsperse 32,000 was selected to give relatively small and stable TiO2 particles at 1 wt % stabilizer and with 20–25 min sonification. The subsequent encapsulation of the dispersed TiO2 particles in styrene/n‐butyl acrylate copolymer (St/BA) via miniemulsion polymerization was carried out and compared with a control study using styrene monomer alone. The lattices resulting from the miniemulsion encapsulation polymerizations were characterized in terms of the encapsulation efficiencies (via density gradient column separations; DGC) and particle size (via dynamic light scattering). Encapsulation efficiencies revealed that complete encapsulation of all of the TiO2 by all of the polymer was not achieved. The maximum encapsulation efficiencies were 79.1% TiO2 inside 61.7% polystyrene and 63.6% TiO2 inside 38.5% St/BA copolymer. As the density of the particles collected from the DGC increased from one layer to another, both the average particle size and the number of the TiO2 particles contained in each latex particle increased. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3479–3486, 2006  相似文献   
38.
The kinetics of non-congruent dissolution of long E-glass fiber in saturated calcium hydroxide solution has been investigated at 25°C in a closed reactor adopting the rotating disc method for the sample holder. The fiber dissolution rate (), measured from the relative loss weight of the fiber after selective dissolution of the attack layer in acetic acid, is a linear function of time, what implies an interfacial dissolution process. However, the kinetics does not stay regular for a long time due to local detachment of the attack layer. The comparison between = f (t) and ′ = f (t) curves, where ′ is the formation rate of the attack layer, shows that the formation of the layer does not only imply the deposit of a bad-crystalline hydrated calcium silicate but the nucleation and growth of solid calcium hydroxide and calcium carbonate resulting from the transfert, to the interface, of ions coming from the liquid phase. This phenomenon was precedently observed by some other authors in the case of glass-fiber reinforced cement matrix.  相似文献   
39.
Prudent management of Iraqi water resources under climate change conditions requires plans to be based on actual figures of the storage capacity of existing reservoirs. With the absence of sediment flushing measures, the actual storage capacity of Dokan Reservoir (operated since 1959) has been affected by the amount of sediment delivered during its operational life leading to an undetermined reduction in its storage capacity. In consequence, there has not been an update on the dam's operational storage capacity curves. In this research, new operational curves were established for the reservoir based on a recent bathymetric survey undertaken in 2014. The reduction in reservoir capacity during the period between 1959 and 2014 was calculated by the mean of the difference between the designed storage capacity and the storage capacity which was concluded from the 2014 bathymetric survey. Moreover, the rate of sediment transported to the reservoir was calculated based on the overall quantities of accumulated sediment and the water discharge of the Lesser Zab River into the reservoir. The results indicate that the dam capacity is reduced by 25% due to sedimentation of an estimated volume of 367 million cubic metres at water level 480 m.a.s.l. The annual sedimentation rate was about 6.6 million cubic metres, and the sediment yield was estimated to be 701.2 t?km?3?year.  相似文献   
40.
针对循环流化床锅炉冷态启动用油量较大的问题,采用两台相邻锅炉一次热风风道联络的方法,实践中利用邻炉一次热风进行锅炉冷态启动,以煤代油缩短锅炉点火投油时间。结果表明:此方法使锅炉冷态启动时的用油量大幅下降,达到了显著的节能效果,并在此基础上展望了一次热风联络技术在锅炉防腐保养、冬季防冻等方面的应用前景。  相似文献   
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