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51.
A El?i 《Canadian Metallurgical Quarterly》1994,50(12):8882-8884
52.
Organo-functional silanes which were able to form chemical bonds with kaolinite and could also have an affinity to the materials of concern here, were studied by the sol-gel process. Polymethacrylate with trialkoxy silyl functional groups were prepared, hydrolysed and co-condensed with kaolinite. The progress of the hydrolysis, which proceeded very slowly, was followed by Karl-Fischer titration. Thermal behavior was investigated by differential thermal analysis. The extent of the reaction leading to network formation was qualitatively followed by Fourier transform-infrared spectroscopy and X-ray diffraction. Free-radical polymerization was carried out ultrasonically in the presence of a catalyst. Trimethoxy silane end-capped silane was found to be covalently bonded to kaolinite. The copolymers, with various amounts of kaolinite, were then hydrolysed and co-condensed in the presence of a catalyst to yield sol-gel materials which have a controllable combination of properties of both the polymer and kaolinite. 相似文献
53.
P. Lobotka I. Vávra Š. Gaži A. Plecenik J. Dérer 《Journal of Low Temperature Physics》1997,106(3-4):381-386
A Josephson junction Nb/Si/Nb with a 10 nm thick amorphous silicon barrier is studied. The upper electrode contains a 2 nm
thick sublayer of amorphous phase adjacent to the barrier, as revealed by cross-sectional TEM. Thus, the junction can be considered
as a S-I-N-S system with the N layer represented by amorphous niobium. Peculiarities in the I–V and Δ(T) dependencies are
observed and explained as a consequence of a proximity effect present in the upper electrode. 相似文献
54.
The effects of an elevated temperature and a 5 wt% silicon addition on the resultant microstructure and inherent phases of Stellite 6 were investigated by using room and high temperature optical microscopy, X-ray diffraction, scanning electron microscopy (SEM) and also bulk hardness and microhardness measurements. It has been observed that exposing Stellite 6 to heat treatments at 1000°C results in a characteristic textured structure and coarsening of interdendritic regions due to bulk diffusion. In addition, both dendritic and interdendritic hardness values increase due to texture formation and increased amounts of carbide and intermetallic phases, respectively. On the other hand, silicon addition to Stellite 6 causes the transformation of the original spongy dendritic microstructure in as-cast Stellite 6 to a eutectic dendritic and skeleton interdendritic structure. Also, when silicon added Stellite 6 was heat treated at 1000°C, particulates emanating from the interdendritic skeleton become irregularly dispersed in the dendritic region. In addition, similarly to Stellite 6; a high temperature heat treatment results in an increase in hardness values of silicon added Stellite 6 due to the presence of an Co2 Si intermetallic phase. 相似文献
55.
F. Ditrói I. Mahunka 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》1985,236(2):375-379
A computerised method is presented for the construction of the level scheme on the basis of measured energies of the gamma transitions without any previous knowledge of the observed isotope. The method and the steps of the algorithm are discussed. The calculated results are compared with the published schemes for the given isotopes. 相似文献
56.
The role of silicon dioxide layers in microelectronics and the importance of their integrity are undisputable. From passivating coatings and masking layers for diffusion to ultra-thin tunneling films — all the silicon technology could not exist without silicon dioxide. This review deals with some aspects of the integrity of thin silicon dioxide films for VLSI applications. The problems of dielectric strength and wear-out are considered from the point of view of their mechanisms, models, oxide processing dependence, testing, and measuring. A brief presentation of statistical approaches commonly applied to reliability topics is also included. 相似文献
57.
Messing Karen Lefrançois Mélanie Saint-Charles Johanne 《Computer Supported Cooperative Work (CSCW)》2021,30(2):215-249
Computer Supported Cooperative Work (CSCW) - Work activity ergonomics (sometimes called francophone ergonomics) draws heavily on observation in order to support transformation of work to arrive at... 相似文献
58.
M. Kohl M. Odehnal V. Petříěek R. Tichý S. Šafrata 《Journal of Low Temperature Physics》1988,72(3-4):319-343
We describe an apparatus allowing the observation of the NMR static longitudinal component of nuclear magnetizationM
z
by a SQUID at low magnetic fields and atT=4.2 K in Plexiglas, Teflon, and CaF2. The higher order NMR Larmor lines at 2f
0, 3f
0, and 4f
0, wheref
0 is the Larmor frequency of the allowed NMR line, were measured. These lines correspond to a flip of two, three, and four spins, respectively, by one photon. The amplitudes of 2f
0 and 3f
0 lines and their field dependences show that the common assertion that the forbidden lines at 2f
0 and 3f
0 appear in the same order of perturbation theory and that their intensity decreases with static magnetic fieldB
0 asB
0
–2
is wrong. In fact, the third Larmor line 3f
0 appears at higher order than the second Larmor line 2f
0 and its intensity decreases asB
0
–4
. This is also shown by a theoretical calculation of its intensity. For the first time the NMR SQUID technique allowed the detection of the 4f
0 line, corresponding to the simultaneous flip of four spins by one photon. 相似文献
59.
Phenolic and amino resins on the basis of α,β-unsaturated aldehydes were synthesized in bulk or solution. Catalysts were HCl, H3PO4, or formic acid, and in some cases NaOH. The course of the reactions was followed by GPC and NMR while the structure of the reaction products was determined by one- and two-dimensional NMR. The course of the reactions is influenced by experimental conditions: the type of monomers, their molar ratio, the type and quantity of the catalyst, the reaction time and temperature, and the reaction medium. At the beginning of the reaction the addition of a nucleophile to an aldehyde takes place through parallel 1,2-addition to and 1,4-addition to group. Oligomers with ? OH, , and ? CHO functional groups are able to add new monomer units or to react mutually to form higher molecular weight addition and condensation products. The overall rate constants for the beginning of the reactions were between 10?3 L/mol s for the high reactive mixtures and 10?7 L/mol s for the less reactive mixtures. The resins were cured by heating at temperatures above 135°C with the addition of hexamethylenetetramine. 相似文献
60.
Pori Maja Arčon Iztok Dasireddy Venkata D. B. C. Likozar Blaž Orel Zorica Crnjak Marinšek Marjan 《Catalysis Letters》2021,151(11):3114-3134
Catalysis Letters - Industrial Cu/ZnO/Al2O3 or novel rate catalysts, prepared with a photochemical deposition method, were studied under functional CH3OH synthesis conditions at the set temperature... 相似文献