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111.
Summary The chlorine in poly(epichlorohydrin) was found to be substituted by diethyldithiocarbamate (ETC) group by the reaction with NaETC in tetrahydrofuran at 60°C. The reaction product was analyzed by RI-UV dual-detector GPC. The composition i.e. the percentage of the chlorine replaced by the ETC group was found to be invariant with the elution count. This result might indicate the absence of polymer effect in the carbamation of poly(epichlorohydrin). 相似文献
112.
Koichi Hatada Tatsuki Kitayama Kinzo Fujikawa Koji Ohta Heimei Yuki 《Polymer Bulletin》1978,1(2):97-102
Summary Copolymer of methyl methacrylate-d8(M1) with a small amount of trityl methacrylate(M2) was radically prepared in tetrahydrofuran and converted into the copolymer of methyl methacrylate-d8 with a small amount of undeuterated methyl methacrylate by the selective hydrolysis of the trityl group and subsequent methylation with diazomethane. From the 1H NMR spectrum of the derived copolymer the assigned coisotactic parameters 12 and 21 were determined to be 0.14 and 0.61, respectively. This may be the first example of the unequivocal determination of assigned configurational parameters in cross propagation for copolymerization. 相似文献
113.
Acidophilic xylanase from Aureobasidium pullulans: efficient expression and secretion in Pichia pastoris and mutational analysis 总被引:1,自引:0,他引:1
Tanaka H Okuno T Moriyama S Muguruma M Ohta K 《Journal of Bioscience and Bioengineering》2004,98(5):338-343
A yeast-like fungus Aureobasidium pullulans var. melanigenum strain ATCC 20524 produces an extracellular acidophilic endo-1,4-beta-xylanase with an optimum pH of 2.0 [Ohta et al., J. Biosci. Bioeng., 92, 262-270 (2001)]. The xynI cDNA encoding the precursor protein (XynI) was expressed in the methylotrophic yeast Pichia pastoris under the control of the alcohol oxidase I gene promoter. The 34 amino acid prepro-signal peptide of the A. pullulans XynI directed the efficient secretion of 178 mg of active xylanase per liter of the culture medium. The secretion level of the xylanase with its own signal peptide was comparable to that of the mature protein fused to the prepro leader from Saccharomyces cerevisiae alpha-mating factor and twofold higher than that of the mature protein fused to the pre-type signal peptide from P. pastoris acid phosphatase. The N-terminal amino acid sequence and the apparent M(r) of 24 kDa of the secreted recombinant protein indicated the native-like processing of the A. pullulans XynI signal sequence in P. pastoris. The three-dimensional model and mutational analysis of the xynI gene product showed that Asp-73 and Glu-157 residues located at the upper and lower edges of the active site cleft, respectively, play a significant role in its low pH optimum. 相似文献
114.
Fukuwatari T Toriochi M Ohta M Sasaki R Shibata K 《Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan》2004,45(1):1-7
Bisphenol A, a monomer of polycarbonate plastics, disturbed the conversion pathway of the amino acid tryptophan to the vitamin nicotinamide. The conversion ratio of tryptophan to nicotinamide was reduced to 1/15 by feeding a diet containing 1% bisphenol A. A putative disturbing reaction is kynurenine-->3-hydroxykynurenine, which is catalyzed by kynurenine monohydroxylase. This is an FAD-enzyme and requires NADPH as a coenzyme. Styrene monomer (1% addition to a normal diet) did not affect the food intake or the body weight, but slightly reduced the conversion ratio of tryptophan-nicotinamide. 相似文献
115.
Energy absorption in blends of polycarbonate with ABS and SAN 总被引:21,自引:0,他引:21
Polycarbonate and its blends with ABS and SAN were tested to study the energy absorbing properties and the deformation mechanism. In tension and impact tests, these blends were found to possess a high energy absorbing capability, high yield strength and large rupture elongation. ABS and SAN particles in the blends deform in a ductile manner to an elongation of more than 100% under a tensile stress. In an elongation test of ABS under a hydraulic pressure of 90×105 N m–2, the transformation from crazing to a cold-drawing mechanism was found to occur. The large elongation of ABS and SAN in the blends is attributed to the cold drawing which occurs under the influence of the pressure acting on the dispersed ABS and SAN, caused by the difference between the elastic moduli of the dispersoid and the matrix. 相似文献
116.
Takemitsu Kunio Tatsuya Yamazaki Eiji Ohta Makoto Sakata 《Solid-state electronics》1983,26(2):155-160
The transient capacitance technique has been used to study the chromium-related levels in the silicon band gap. Chromium was diffused at temperature of 1100 and 1150°C for 0.5 and 3 hr. Five different levels at Ec?0.11 eV, Ec?0.21 eV, Ec?0.28 eV, Ec?0.36 eV and Ec?0.45 eV were obtained from the Arrheniu plots of the electron thermal-emission rates. The number of levels in the upper half of the band gap decreased from five to two with an increase of Cr-diffusion period. Two levels were located at Ec?0.20 eV (donor) and Ec?0.43 eV (acceptor). A donor level was also observed at Ev + 0.25 eV. The donor level was not affected by the diffusion condition. The majority carrier capture cross sections of the three dominant levels have been measured by the transient capacitance technique modified by the pulse transformer. The values were σn = 4.1 × 10?15 cm2 for the upper donor at Ec?0.20 eV, σn = 2.0 × 10?16 cm2 for the acceptor at Ec ?0.43 eV and σp = 9.1 × 10?18 cm2 for the lower donor at Ev + 0.25 eV, and were independent of temperature. The three dominant levels are due to distinct chromium centers. 相似文献
117.
New Submicron (0.5-1.0 mu m diam) bubble garnets have been developed. In order to reduce saturation induction4piMs as low as possible, suitable choice of amounts of nonmagnetic ions substituting for ferric ions in both tetrahedral and octahedral sites were studied in (YSm)3 (FeAl)5 O12 , (YSmLu)3 - (FeGaSc)5 O12 , (YSmLu)3 (FeAlSc)5 O12 and (LaLuSm)3 - (FeGa)5 O12 garnet systems. For example, in (YSmLu)3 - (FeAlSc)5 O12 a film with the following properties was grown; strip widthw = 0.7mu m, film thicknessh= 0.7mu m, quality factorq=2.8 , Curie temperatureTc= 140deg C and4piMs=770 G. The temperature properties of those films could be improved drastically by doping with a small amount of Gd ion. Wall mobilities μw of those films are in the region from 200 to 500cm/s/Oe. Preceding these material studies, several film characterization methods have been investigated. Film thickness was measured by Fluorescent X-ray method, strip width by using a highly sensitivity TV camera, and bubble collapse field by FMR resonance technique respectively. 相似文献
118.
Two simple chromenes with anti-JH activity have been isolated and identified from the bedding plant Ageratum houstoianum. By contact and fumigation these compounds induce precocious metamorphosis and sterilization in several hemipteran species of insects. Certain holometabolous species are sterilized, forced into diapause, or both. Each of these biological actions is equivalent to removal of the corpora allata, which produce the JH's, and is reversible by treatment with exogenous JH. Thus, the action of these compounds is to stop the production or depress the titer of the JH's. To our knowledge, this is the first discovery of anti-JH, and we hope it will guide the way to the emergence of a fourth generation of safe and insect-specific pesticides. 相似文献
119.
The expressions for Walsh functions in terms of shifted Rademacher functions are applicable to the design of a directive and selective array antenna for Walsh waves which is capable of eliminating the interference caused by impulsive noises. They also are applicable to voice processing because of their shift-invariant property. The shifted Rademacher functions were previously introduced by shiftiAg horizontally the periodic Rademacher functions. It was shown that the Walsh functions could be expressed as a linear combination of a finite number of the shifted Rademacher functions. This paper develops the actual expansions of the Walsh functions in terms of the shifted Rademacher functions. The coefficients in this series take only the values of either + 1 or -1. The shifted Rademacher coefficients appearing in the expansion of a given function in tenns of shifted Rademacher functions have the advantage that the coefficients of a shifted function are available by shifting cyclically the original coefficients. 相似文献
120.