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71.
Scientometrics - We analyzed breakthrough patents that serve as the basis of emerging technological trajectories and paradigm over 25-years. The results showed that although technological fields... 相似文献
72.
73.
The present work has been carried out with the aim to synthesize tin oxide decorated reduce graphene oxide nanocomposite (SnO2/RGO-Nc) via in-situ synthesis process and the influence of RGO loading on structural, optical, thermal and dielectric properties of SnO2 has been discussed. The XRD, FESEM coupled with EDX elemental mapping, TEM, FTIR, Raman and XPS results reveal that the SnO2 nanoparticles have been successfully incorporated onto the RGO sheets. The reduction in the energy gap of the composite sample as compared to SnO2 measured from the Tauc’s relation can be attributed to strong coupling between RGO and SnO2 NPs. Thermogravimetric analysis (TGA) shows improved thermal stability of the SnO2/RGO-Nc. From the dielectric measurements, it is observed that the dielectric constant and dielectric loss decreases as frequency of applied field increases. AC conductivity of all samples increases as applied frequency increases which follows Jonscher’s power law. All composite samples show better conductivity as compared to SnO2. This is due to the formation of continuous conductive pathway between SnO2 and RGO sheets. Further high dielectric constant, low loss and high ac conductivity have been observed at optimum loading of RGO in SnO2/RGO2-Nc as compared to other composite samples which is due the percolation effects. The impedance analysis exhibits only one semicircle for SnO2 and SnO2/RGO composite which suggests that the involvement of grain boundaries dominated over the grain contribution. 相似文献
74.
Ravet N Abouimrane A Armand M 《Nature materials》2003,2(11):702; author reply 702-702; author reply 703
75.
Most recent research on channel‐based key generation oriented to time division duplex system because the channel reciprocity feature is applied directly for secret key generation. Most of commercial cellular systems depend on frequency division duplex (FDD) systems. In this paper, we investigate the impact of uplink and downlink of FDD systems for the generation of shared secret keys between two parties in the presents of passive eavesdropper. In addition, we are considering improving the rate of the secret key for wireless communication in FDD mode. The main idea is to use the fading coefficient of the channels between the relay and other parties as an additional random common source for the secret key generation. Also, explore the using of channel estimation techniques to reduce the channel training sequence and study its effect on the generation of shared key for wireless communications in FDD mode. We derive the upper bound of the generated shared key rate for four scenarios and give numerical examples to reveal the performance of our suggested improvement approaches. 相似文献
76.
77.
The Nickel base Superalloys are the most famous complicated and useable of Superalloys to make hot zone components of the gas turbines. The complicated dimensional tolerances, specially at the root of the blade show importance of grinding processes at the production of blades root. The prediction of the effect of machining parameters on the soundness of component surface strengthening for reaching to a suitable surface finishing and avoiding from crack formation at the work part during machining operation often is not easy and feasible so needs to more industrial investigation.This research is about frame 5 blade designed by GE and made from Superalloy IN738LC has been investigated. The formation of a plastically deformed and heat affected zone during grinding of Superalloy IN738LC with a high depth of cut but slow work speed (creep feed grinding) was investigated. Parameters such as work speed, depth of cut and radial dressing speed have been considered as variables and their effects have been studied. During experimental performed, the voltage and current of motor measured and power and special energy calculated.Some samples heat-treated (of the 1176℃ for 1 hr under neutral argon gas and cooling rate of 15℃/min up to 537℃ and then air cooling) to study grains recrystallization. Other samples have been created from the roots of blades and then coated by Nickel to measure boundary layer micro-hardness. The results show that increasing work speed leads to increasing the use power. Increasing the depth of cut, by increasing material removal rate, and the radial dressing speed, by decreasing power, lead to decreasing special energy. The temperature created by grinding lead to decreasing plastic deformation and boundary layer formation. When the radial dressing speed changes from 1 to 0.6μm/rev and other parameters are kept unchanged the roughness of surface increases and the special energy decreases. Sufficient dressing is very essential in limiting the width of the molten zone to few micrometers. As a result, it was found that local melting at contact spots to be a rather common mechanism during grinding of superalloys, lead to so-called white layers which can easily be observed on metallographic cross sections. 相似文献
78.
Existing analytical thermal models for predicting surface burns due to grinding have limited use because of their reliance on parameters that are not readily obtainable in practice. This paper presents a practical and consistent fuzzy rule-based model for estimating the grinding conditions at which “burn limits” occur. The model consists of 37 absolute and eight relative rules. It has a wide range of applications over many types of steels, Alundum wheels, and grinding conditions. It is also simple to implement, from a rule-chart mode to an intelligent on-line adaptive control mode. 相似文献
79.
在许多情况下,只应用一种NDT技术存在不足,这就迫使NDT操作人员使用一种以上的技术以保证检测出危害被检物使用寿命或功能的缺陷。但分别实施多种技术的检测,就会延长检验时间。介绍了一种新的NDT设施,采用两种不同的非接触无损检测技术进行互补,即电磁声换能器(EMAT)和脉冲涡流(PEC)探头。检测结果表明,脉冲涡流和电磁声换能器因是非接触,所以可应用于材料生产过程中的自动在线检验,也可用于在役检验。 相似文献
80.
Ali Hassanzadeh 《Corrosion Science》2007,49(4):1895-1906
In our previous works, the corrosion inhibition properties of propylamine (PA), iso-propylamine (i-PA), butylamine (BA), tert-butylamine (t-BA), hexylamine (HA), ethylenediamine (EDA), diethanolamine (DEA), 3-amino-1-propanol (3-AP), 2-dimethylethanolamine (2-DEA), cyclohexylamine (CHA), N-methylcyclohexylamine (N-MCA) and dicyclohexylamine (DCHA) have been investigated by means of electrochemical impedance spectroscopy (EIS) with a carbon steel rotating disc electrode in some petroleum/water corrosive mixtures containing acetic acid and NaCl at 25 °C. In this work, the Kramers-Kronig transformations (KKTs) were applied to evaluate the validity of the impedance data of these amine compounds in hydrodynamic condition. The results obtained showed that experimental impedance data did not satisfy in K-K relations completely viz. indicated some errors. These errors were related to stray capacitances, external transmission line effects, pits formation and change in interface during data acquisition at high and low frequencies regions. In addition, the selection of a suitable equivalent circuit strongly emphasized to better interpret of EIS data which in turn cause better resulted KKTs spectra. With considering obtained transformations, more effective inhibitor was selected with regard to its charge transfer resistance, the corrosion capacitance and well satisfying in K-K relations. 相似文献