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排序方式: 共有431条查询结果,搜索用时 437 毫秒
121.
The reaction between tungsten(VI) complex [W(eg)3] (eg = 1,2-ethanediolato dianion) and a phenolic ligand precursor 2,4-di-tert-butyl-6-(((2-hydroxyethyl)(methyl)amino)methyl)phenol (H2L) affords a monomeric oxotungsten complex [WO(eg)(L)]. This complex reacts further with Me3SiCl, which leads to the displacement of ethanediolato ligand from the complex unit and formation of cis- and trans-isomers of corresponding dichloro complex [WOCl2(L)]. Identical dichloro complexes were also prepared by the reaction between H2L and WOCl4. Molecular structure of [WO(eg)(L)] was verified by X-ray crystallography. 相似文献
122.
Merrell WC Aslam S Brown AD Chervenak JA Huang WC Quijada M Wollack EJ 《Applied optics》2012,51(15):3046-3053
The future needs of space-based, observational planetary and astronomy missions include low mass and small volume radiometric instruments that can operate in high-radiation and low-temperature environments. Here, we focus on a central spectroscopic component, the bandpass filter. We model the bandpass response of the filters to target the wavelength of the resonance peaks at 20, 40, and 60 μm and report good agreement between the modeled and measured response. We present a technique of using standard micromachining processes for semiconductor fabrication to make compact, free-standing, resonant, metal mesh filter arrays with silicon support frames. The process can be customized to include multiple detector array architectures, and the silicon frame provides lightweight mechanical support with low form factor. 相似文献
123.
Shinonaga T Donohue D Aigner H Bürger S Klose D Kärkelä T Zilliacus R Auvinen A Marie O Pointurier F 《Analytical chemistry》2012,84(6):2638-2646
Plutonium (Pu) dioxide particles were produced from certified reference material (CRM) 136 solution (CRM 136-plutonium isotopic standard, New Brunswick Laboratory, Argonne, IL, U.S.A., 1987) using an atomizer system on December 3, 2009 after chemical separation of americium (Am) on October 27, 2009. The highest density of the size distribution of the particles obtained from 312 particles on a selected impactor stage was in the range of 0.7-0.8 μm. The flattening degree of 312 particles was also estimated. The isotopic composition of Pu and uranium (U) and the amount of Am were estimated by thermal ionization mass spectrometry (TIMS), inductively coupled plasma mass spectrometry (ICPMS), and α-spectrometry. Within uncertainties the isotopic composition of the produced particles is in agreement with the expected values, which were derived from the decay correction of the Pu isotopes in the CRM 136. The elemental ratio of Am to Pu in the produced particles was determined on the 317th and 674th day after Am separation, and the residual amount of Am in the solution was estimated. The analytical results of single particles by micro-Raman-scanning electron microscopy (SEM)-energy-dispersive X-ray spectrometry (EDX) indicate that the produced particles are Pu dioxide. Our initial attempts to measure the density of two single particles gave results with a spread value accompanied by a large uncertainty. 相似文献
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Kärkkäinen AH Tamkin JM Rogers JD Neal DR Hormi OE Jabbour GE Rantala JT Descour MR 《Applied optics》2002,41(19):3988-3998
Direct photolithographic deforming of hybrid glass films is used to fabricate optical structures. The structure is fabricated in polyethylene-oxide-acrylate modified hybrid glass films with (1) binary and gray-scale photomasks using a mercury UV-lamp exposure and (2) maskless UV-laser patterning. Fabrication of isolated lenslets, lens arrays, and gratings is presented, including the associated exposure patterns. The hybrid glass material yields light-induced deformation peak-to-valley (p.v.) heights up to 12.8 microm with mercury UV-lamp exposure and p.v. deformation heights up to 6.8 microm with 365-nm UV-laser exposure. The fabricated lenslets' surface data are presented as Zernike-polynomial fit coefficients. Material synthesis and processing-related aspects are examined to understand and control the material's deformation under exposure. The hybrid glass material exhibits a maximum spectral extinction coefficient of 1.6 x 10(-3) microm(-1) at wavelengths ranging from 450 to 2,200 nm and has a refractive index of 1.52 at 632.8 nm. The fabricated structures exhibit rms surface roughness between 1 and 5 nm. 相似文献
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128.
Ville Karavirta Ari Korhonen Lauri Malmi Thomas Naps 《Journal of Visual Languages and Computing》2010,21(1):1-22
In this paper, we present a taxonomy of algorithm animation languages that augments Price's well-known taxonomy of software visualization. Whereas Price's taxonomy is directed to classifying features and characteristics of visualization systems, the new taxonomy focuses on evaluating current animation languages. The taxonomy can be used by algorithm visualization system designers as a tool to compare visualization system languages with each other as well as for designing and implementing new systems and language features. In addition, the taxonomy provides guidelines to the features that are needed for transferring animations between systems. This is an ongoing project that elaborates upon the work reported on in a briefer version of the taxonomy. 相似文献
129.
130.
Analyzing skewed symmetries 总被引:1,自引:1,他引:0
Symmetry is pervasive in both man-made objects and nature. Since symmetries project to skew symmetries, finding axes of skew symmetry is an important vision task. This paper presents a linear time algorithm for finding the axes of skew symmetry, where the degree of symmetry is known. First, we present a review and critique of current methods for finding the axes of skew symmetry. Next, we decompose the problem of finding skew symmetry into the subproblems of solving for the rotational parameter of a shear symmetry and recovering the shear parameter of a reflexive symmetry. Using this approach, the authors derive a direct, non-heuristic moment-based technique for finding the axes of skew symmetry. For skew symmetric figures with degree of symmetry less than five we obtain a closed-form solution. The method does not rely on continuous contours but assumes there is no occlusion and requires knowing the contour's degree of symmetry. It is the first algorithm to find the axes of skew symmetry inO(n) time, where n is the number of contour points. The method is especially suited to industrial applications where the degree of symmetry is often knowna priori. Examples of the method are presented for both real and synthetic images, and an error analysis of the method is given. 相似文献