Numerical analysis of IPIRG cracked pipe experiments subjected to dynamic and cyclic loading

This report contains results of a finite element study aiming to identify the influence of loading history and geometry for cracked pipes subjected to complex loading. The experiments have been performed within the International Piping Integrity Research Group (IPIRG) Program. The majority of the numerically analyzed experiments were conducted on straight pipes with an outside diameter of 168 mm and containing a large circumferential through-wall crack. The considered pipes were loaded in four-point bending under displacement control and at a temperature of 288°C. The types of loading were combinations of either quasi-static or dynamic and also monotonic or cyclic loading with different loading ratios R. Some analyses were also performed on surface-cracked pipes subjected to slow, monotonic loading.

In the finite element study, 20-node solid elements were used for the through-wall cracked pipes and a combination of shell and non-linear line spring elements for the surface-cracked pipes. Stable crack growth was simulated by gradual node relaxation and crack closure is accounted for by using simple contact elements. The J-integral for a remote contour is calculated and used as a characterizing fracture parameter although the cyclic loading violates the theoretical basis for this procedure. The near-tip J can not be used for growing cracks because of the weak energy singularity. The results of the numerical study confirm the trends from the experiments in that a high loading rate has a negative influence on the fracture properties of the studied carbon steel and that large cyclic loading, especially at R = −1, lowers the apparent J_R-curve for both carbon and stainless steels. To some extent geometry effects appear to be present when comparing the results from pipes containing surface cracks and through-wall cracks with results from CT specimens. These effects are more pronounced for large amounts of stable crack growth than at initiation.     

Optimization algorithms for calculation of the joint design point in parallel systems

In large structures it is often necessary to estimate the reliability of the system by use of parallel systems. Optimality criteria-based algorithms for calculation of the joint design point in a parallel system are described and efficient active set strategies are developed. Three possible algorithms are tested in two examples against well-known general non-linear optimization algorithms. Especially one of the suggested algorithms seems to be stable and fast.     

From the individual element test to finite element templates: Evolution of the patch test

This paper starts a sequence of three articles that follow an unconventional approach in finite element research. The ultimate objective is to construct high-performance elements and element-level error estimators for those elements. The approach takes off from our previous work in high-performance elements and culminates with the development of finite element templates. The present paper concentrates on the patch test and evolved versions of the test that have played a key role in this research. Following a brief review of the historical roots, we present the Individual Element Test (IET) of Bergan and Hanssen in an expanded context that encompasses several important classes of new elements. The relationship of the IET to the multielement forms A, B and C of the patch test and to the single-element test are investigated. An important consequence of the IET application is that the element stiffness equations decompose naturally into basic and higher-order parts. The application of this decomposition to the “sanitization” of the non-convergent BCIZ element is described and verified with numerical experiments. Two sequel papers in preparation are subtitled ‘the algebraic approach’ and ‘element-level error estimation’. These apply the fundamental decomposition to the derivation of templates for specific mechanical elements and to the construction of element-level error estimators, respectively.     

Evidence for an RNA binding region in the Escherichia coli processing endoribonuclease RNase E

The processing endoribonuclease RNase E (Rne), which is encoded by the rne gene, is involved in the maturation process of messenger RNAs and a ribosomal RNA. A number of deletions were constructed in order to assess functional domains of the rne gene product. The expression of the deletion constructs using a T7 promoter/RNA polymerase overproduction system led to the synthesis of truncated Rne polypeptides. The smallest gene fragment in this collection that was able to complement a temperature sensitive rnets mutation and to restore the processing of 9 S RNA was a 2.3-kilobase pair fragment with a 1.9-kilobase pair N-terminal coding sequence that mediated synthesis of a 70.8-kDa polypeptide. Antibodies raised against a truncated 110-kDa polypeptide cross-reacted with the intact rne gene product and with all of the shorter C-terminal truncated polypeptides, indicating that the N-terminal part of the molecule contained strong antigenic determinants. Furthermore, by analyzing the Rne protein and the truncated polypeptides for their ability to bind substrate RNAs, we were able to demonstrate that the central part of the Rne molecule encodes an RNA binding region. Binding to substrate RNAs correlated with the endonucleolytic activity. RNAs that are not substrates for RNase E did not bind to the protein. The two mutated Rne polypeptides expressed from the cloned gene containing either the rne-3071 or ams1 mutation also had the ability to bind 9 S RNA, while their enzymatic function was completely abolished. The data presented here suggest that the endonucleolytic activity is encoded by the N-terminal part of the Rne protein molecule and that the central part of it possesses RNA binding activity.     

Treatment of Humic Waters By Ozone

Two different generators for ozone were tested, a traditional electrical discharge generator and a generator based upon UV–irradiation of air at 150–180 nm. It was demonstrated that the traditional generator gave slightly higher reductions in levels of color for equivalent ozone dosages. Both gases affected the molecular weight distribution in the way that the bigger molecules were broken down to smaller ones. No significant difference between the molecular weight reduction efficiency of the gases was found.     

The effect of backbone fluorination on the carrier mobility in alkoxy and alkyl substituted conducting polymers of the poly(phenylenevinylene) type

Summary We report the synthesis of some new backbone fluorinated polymers of the poly(phenylenevinylene) type. The new polymers were characterised by NMR, SEC and X-ray powder diffraction. The charge carrier mobilities were determined using pulse radiolysis time resolved microwave conductivity (PR-TRMC) and the carrier mobilities were compared to the similar non-fluorinated analogues. The changes in charge carrier mobilities as a function of molecular substitution pattern is discussed in terms of other materials properties such as electronic structure and absorption properties. The major result is that it was found possible for this type of material to alter the electronic energy levels by molecular substitution without imparting significant changes in the magnitude of the charge carrier mobilities and the optical properties.     

Efficient return algorithms for associated plasticity with multiple yield planes

A new return method for implicit integration of linear isotropic yield criteria is presented. The basic idea is to perform all the manipulations in the principal stress space and thereby achieve very simple formulae for calculating the plastic corrector stresses, based on the constant gradient of such criteria. The return formulae are in closed form and no iteration is required. The method accounts for three types of stress return: return to a single yield plane, to a discontinuity line at the intersection of two yield planes and to a discontinuity point at the intersection between three or more yield planes. The infinitesimal and the consistent elastoplastic constitutive matrix are calculated for each type of stress return, as are the conditions to ascertain which type of return is required. The method is exemplified with the Mohr–Coulomb yield criterion. Copyright © 2005 John Wiley & Sons, Ltd.     

A Micellar Route to Ordered Arrays of Magnetic Nanoparticles: From Size‐Selected Pure Cobalt Dots to Cobalt–Cobalt Oxide Core–Shell Systems

Starting with Co‐salt‐loaded inverse micelles, which form if the diblock copolymer polystyrene‐block‐poly(2‐vinylpyridine) is dissolved in a selective solvent like toluene and CoCl₂ is added to the solution, monomicellar arrays of such micelles exhibiting a significant hexagonal order can be prepared on top of various substrates with tailored intermicellar distances and structure heights. In order to remove the polymer matrix and to finally obtain arrays of pure Co nanoparticles, the micelles are first exposed to an oxygen plasma, followed by a treatment in a hydrogen plasma. Applying in‐situ X‐ray photoelectron spectroscopy, it is demonstrated that: 1) The oxygen plasma completely removes the polymer, though conserving the original order of the micellar array. Furthermore, the resulting nanoparticles are entirely oxidized with a chemical shift of the Co 2p_3/2 line pointing to the formation of Co₃O₄. 2) By the subsequent hydrogen plasma treatment the nanoparticles are fully reduced to metallic Co. 3) By exposing the pure Co nanoparticles for 100 s to various oxygen partial pressures pequation/tex2gif-inf-5.gif, a stepwise oxidation is observed with a still metallic Co core surrounded by an oxide shell. The data allow the extraction of the thickness of the oxide shell as a function of the total exposure to oxygen (pequation/tex2gif-inf-7.gif × time), thus giving the opportunity to control the ferromagnetic–antiferromagnetic composition of an exchange‐biased magnetic system.     

An efficient return algorithm for non-associated plasticity with linear yield criteria in principal stress space

An efficient return algorithm for stress update in numerical plasticity computations is presented. The yield criterion must be linear in principal stress space and can be composed of any number of yield planes. Each of these yield planes may have an associated or non-associated flow rule. The stress return and the formation of the constitutive matrix is carried out in principal stress space. Here the manipulations simplify and rely on geometrical arguments. The singularities arising at the intersection of yield planes are dealt with in a straightforward way also based on geometrical considerations. The method is exemplified on non-associated Mohr–Coulomb plasticity throughout the paper.     

Societal Safety: Concept,Borders and Dilemmas

In most industrialized countries, the end of the Cold War marked a change in focus from preparedness for war to an increasing focus on civil society's own vulnerability and safety. To meet new threats and changing risks, there is also a need for new analytical concepts. Societal safety is a concept developed in Norway during the last decade. It could be defined as: ‘The society's ability to maintain critical social functions, to protect the life and health of the citizens and to meet the citizens' basic requirements in a variety of stress situations’. It aims to be a systematic approach for understanding, mitigating and responding to social problems such as extraordinary stresses and losses, interferences in complex and mutual dependent systems, or lack of trust in vital social institutions. Future threats to society are not limited to specific sectors or areas, but stem from complex interactions amongst economic, technological, social and cultural factors. Thus, the main challenges to improve societal safety will be the ability to coordinate, organize and assign clear roles to different actors at the international, national and local levels. Societal safety has interfaces with other safety‐related areas such as national security, sustainable development, human security and incident management (handling of isolated accidents, common illness and ordinary criminal acts). Societal safety is, however, a sensitive political issue containing dilemmas and value choices that are hardly possible to perceive or solve as pure scientific problems.