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961.
Gibbs energies of formation of CoF2 and MnF2 have been measured in the temperature range from 700 to 1100 K using Al2O3-dispersed CaF2 solid electrolyte and Ni+NiF2 as the reference electrode. The dispersed solid electrolyte has higher conductivity than pure CaF2 thus permitting accurate measurements at lower temperatures. However, to prevent reaction between Al2O3 in the solid electrolyte and NiF2 (or CoF2) at the electrode, the dispersed solid electrolyte was coated with pure CaF2, thus creating a composite structure. The free energies of formation of CoF2 and MnF2 are (± 1700) J mol−1; {fx37-1} The third law analysis gives the enthalpy of formation of solid CoF2 as ΔH° (298·15 K) = −672·69 (± 0·1) kJ mol−1, which compares with a value of −671·5 (± 4) kJ mol−1 given in Janaf tables. For solid MnF2, ΔH°(298·15 K) = − 854·97 (± 0·13) kJ mol−1, which is significantly different from a value of −803·3 kJ mol−1 given in the compilation by Barinet al. 相似文献
962.
A minimal integrated filter containing four MOS transistors as the only circuit elements is presented. Voltage tuning is used to set the cutoff frequency and band-edge peaking. A filter test chip occupies an active area of 0006mm2, has acutoff frequency of 40 MHz and dissipates 580W. 相似文献
963.
In the letter, two schemes of circuit partitioning for pseudo-exhaustive testing are described. The complexities of both are proved to be NP-complete. 相似文献
964.
D. C. Peets R. Liang C. Stock W. J. L. Buyers Z. Tun L. Taillefer R. J. Birgeneau D. A. Bonn W. N. Hardy 《Journal of Superconductivity and Novel Magnetism》2002,15(6):531-534
We have grown cubic centimeter-size crystals of YBa2Cu3O x suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2% Y2BaCuO5 and 0.5% Pt (by mass) were required to prevent melt loss and to obtain the highest crystallinity. A neutron diffraction study on a mosaic of six such crystals found that the final Y2BaCuO5 concentration was 5%, while other impurity phases comprised less than 1% by volume. The oxygen content was set to x = 6.5, the crystals were detwinned, and then carefully annealed to give the well-ordered ortho-II phase. The neutron study determined that 70% of the mosaic's volume was in the majority orthorhomic domain. The neutron (006) and (110) rocking curve widths were ~1° per crystal and ~2.2° for the mosaic, and the oxygen chain correlation lengths were >100 Å in the a- and b-directions and ~50 Å in the c-direction. 相似文献
965.
Volatile Compounds of Raw Beef from 5 Local Spanish Cattle Breeds Stored Under Modified Atmosphere 总被引:7,自引:0,他引:7
Volatile compounds of raw beef from Asturiana de los Valles, Morucha, Parda Alpina, Pirenaica, and Retinta cattle breeds were studied. Steaks were packaged under 60% O2, 30% CO2, and 10% N2, and 53 volatile compounds were tentatively identified by purge‐and‐trap extraction and gas chromatography with mass spectrometry after 0, 5, 10, and 15 d of chill storage. The degradation of beef quality with increasing storage time was evidenced by the increase in 2,3,3‐trimethylpentane, 2,2,5‐trimethylhexane, 3‐octene, 3‐methyl‐2‐heptene, 2‐octene, and 2‐propanone and by the decrease in dimethyl sulfide. Consequently, some of the volatile compounds, which are believed to be formed by thermal degradation of meat, might be formed during chill storage, and the rate of formation of some was dependent on the specific compound. 相似文献
966.
ABSTRACT: The thermal stability of Bacillus licheniformis α-amylase at low moisture content was studied, based on isothermal experiments performed in a temperature range 113 to 125 °C. The thermal inactivation was monitored by measuring the decrease in thermal denaturation enthalpy and/or the decrease in enzymic activity on pnitrophenyl-α-D-maltoheptaoside, or on starch as a substrate. Based on enthalpy readings, an enzymic system with a z-value of 10.4 °C was observed when using a relative humidity of 81% at 4 °C. A theoretical study showed that this system could be used as a Time Temperature Integrator (TTI) to monitor the safety of sterilization processes of numerous food products. 相似文献
967.
Androstenedione labeled with tritium at positions 1 and 2 was prepared. The molar radioactivity of the sample prepared using homogeneous catalysts was as high as 1.4-1.5 PBq mol-
1. [1,2-3H]Androst-4-ene-3,17-dione can be converted into the [1-3H]steroid with the molar radioactivity of 0.9 PBq mol-
1. 相似文献
968.
969.
M. Ravi U. T. S. Pillai B. C. Pai A. D. Damodaran E. S. Dwarakadasa 《Metallurgical and Materials Transactions A》2002,33(2):391-400
The effect of Fe content (0.2 to 0.6 pct) on the microstructure and mechanical properties of a cast Al-7Si-0.3Mg (LM 25/356)
alloy has been investigated. Further, 1 pct mischmetal (MM) additions (a mixture of rare-earth (RE) elements) were made to
these alloys, and their mechanical properties at room and at elevated temperatures (up to 200 °C) were evaluated. A structure-property
correlation on this alloy was attempted using optical microstructure analysis, fractographs, X-ray diffraction, energy-dispersive
analysis of X-rays (EDX), and quantitative metallography by image analysis. An increase in Fe content increased the volume
percentage of Fe-bearing intermetallic compounds (β and π phases), contributing to the loweryield strength (YS), ultimate tensile strength (UTS), percentage elongation, and higher
hardness. An addition of 1 pct MM to the alloys containing 0.2 and 0.6 pct Fe was found to refine the microstructure; modify
the eutectic silicon and La, Ce, and Nd present in the MM; form different intermetallic compounds with Al, Si, Fe, and Mg;
and improve the mechanical properties of the alloys both at room and elevated temperatures. 相似文献
970.
Field R. D. Hartwig K. T. Necker C. T. Bingert J. F. Agnew S. R. 《Metallurgical and Materials Transactions A》2002,33(13):965-972
The equal-channel angular extrusion (ECAE) technique has been applied to a powder metallurgy (P/M) source Be alloy. Extrusions
have been successfully completed on Ni-canned billets of Be at approximately 425°C. No cracking was observed in the billets,
and significant grain refinement was achieved. In this article, microstructural features and dislocation structures are discussed
for a singlepass extrusion, including evidence of <c> and <c+a> dislocations. Significant crystallographic texture developed during ECAE, which is discussed in terms of this unique deformation
processing technique and the underlying physical processes which sustain the deformation.
S.R. AGNEW, formerly with the Oak Ridge National Laboratory, Oak Ridge, TN 37831-6115
This article is based on a presentation made in the symposium entitled “Defect Properties and Mechanical Behavior of HCP Metals
and Alloys” at the TMS Annual Meeting, February 11–15, 2001, in New Orleans, Louisiana, under the auspices of the following
ASM committees: Materials Science Critical Technology Sector, Structural Materials Division, Electronic, Magnetic & Photonic
Materials Division, Chemistry & Physics of Materials Committee, Joint Nuclear Materials Committee, and Titanium Committee. 相似文献