用磷铝杂原子固体酸催化剂合成马来酸二丁酯

以自制的磷铝杂原子固体酸催化剂催化合成了马来酸二丁酯，考察了反应时间、醇酸摩尔比、带水剂用量、催化剂用量等对酯化率的影响；同时考察了催化剂的重复使用性。对酯化产物物理性能进行了测试，其实测值与文献值相符。     

高油价下我国石油化工的发展对策思考

改革开放20多年来，中国经济向全球展示了持续快速的增长，作为支柱产业的中国石化工业也一直保持着良好的增长势头，得到了稳定快速的发展，尤其在“十五”期间，中国的石化工业在世界石化业中的地位有了突破性的提升。     

Al-Cu双金属复合结构的扩散连接试验研究

应用扩散连方法进行了Al-Cu双金属复合结构的试验研究，比较了不同的焊接工艺，材料组合以及母材状态情况Al合金与Cu的连接性，观察了接头区域的微观组织结构，研究表明，固相扩散连接是一种适用于异种材料连接的有效方法，通过在连接区域形成Al-Cu金属间化合物，达到Al和Cu的有效连接，材料组合，母材原始状态以及连接工艺参数对Al合金与Cu的扩散连接存在着明显的影响。表面镀Ni工艺不但能够有效阻止Al和Cu之间形成脆性相，而且Al和Ni之间形成了良好的扩散连接，改善了接头性能。     

Conduction band states of transition metal (TM) high-k gate dielectrics as determined from X-ray absorption spectra

This paper uses X-ray absorption spectroscopy to study the electronic structure of the high-k gate dielectrics including TM and RE oxides. The results are applicable to TM and rare earth (RE) silicate and aluminate alloys, as well as complex oxides comprised of mixed TM/TM and TM/RE oxides. These studies identify the nature of the lowest conduction band d^* states, which define the optical band gap, E_g, and the conduction band offset energy with respect to crystalline Si, E_B. E_g and E_B scale with the atomic properties of the TM and RE atoms providing important insights for identification high-k dielectrics that meet performance targets for advanced CMOS devices.     

A modified rainflow counting method

The rainflow counting method is commonly recognized to be a good cyclic counting method in fatigue life prediction and for testing engineering components and structures. However, it has some shortcomings, which are pointed out in this paper in connection with the analysis of the stress-strain response. A modified rainflow counting method is presented. Case studies show that all the cycles really existing in the stress-strain response that cannot be counted by the rainflow counting method can be counted by the modified rainflow counting method. So it can be said that the modified rainflow counting method is a more reasonable cycling counting method than the traditional rainflow counting method.     

传感器网络中基于二元簇的节能路由算法

传感器网络中的分簇算法已经被证明能够有效地节约能量。据此提出了一种基于二元簇的路由算法,其基本思想是网络中的每个节点同时属于2个不同簇,利用二元性来减少在路由发现中的资源浪费,并能够更加确定地发现路由以节约资源。理论分析和模拟实验都表明,该算法在能量消耗和网络生命周期延长方面较优。     

杭-宁输气管道工程定向钻穿越设计浅析

杭州-宁波天然气输气管道工程（简称杭-宁输气管道工程）是浙江省天然气长输管网主干线之一，根据工程河流穿越众多、渠塘穿越频繁的特点，对杭-宁输气管道工程水域穿越的特点和穿越方式作了总结；重点分析了水域定向钻穿越设计及需要注意的问题，为今后浙江省天然气管网建设的水域穿越设计作了探讨。     

山西省水文数据库的建设与结构分析

文中通过对山西省水文数据库建设的回顾，分析了数据库的库表结构及相关内容，并对今后数据库的建设工作提出了建议和展望。     

WiMAX系统中载波与采样钟同步的研究

IEEE802．16协议采用的OFDMA技术提供了两种子信道使用方式，分别为FUSC和PUSC，结合FUSC的固有结构特点，对导频配置方法和采样钟同步算法进行更深入的忱化。提出了一种更精确的载波和采样钟同步方案。仿真结果表明，此方案所得到的载波同步估计值比普通算法更加准确，同步性能也随之有了很大的改善。     

Intermittent Phenomena in Switched Systems With High Coupling Strengths

In this paper, one kind of intermittency generated by a discontinuous system is studied. Although this system, which is composed of two switched subsystems coupled with a high strength, is nonsmooth, the mechanism of this kind of intermittency can be analyzed with several explicit relations between the intermittency characteristics and the system control parameters. In particular, estimates of "steady-state" values of the system (in the laminar phases) and a critical value for this intermittency can be derived, which are helpful in relevant control systems design. Moreover, some power laws for the observed intermittency are obtained and discussed