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101.
One major problem that arises in the design of plastic parts, especially those that are fiber reinforced, is the change of shape and dimension as a result of shrinkage and warpage. These material inhomogeneities are caused by flowinduced fiber orientation, curing, poor thermal mold lay-out, and other processing conditions. This paper presents a simulation that predicts shirnkage and warpage of 3-D compression molded fiber reinforced composite parts. The simulation represents the structure with the 3-noded shell elements used in mold filling simulations. The calculated results indicate that fiber orientation strongly affect the final properties, which vary with different chage locations, have a significant effect on warpage. Unsymmetric curing, caused by uneven mold temperatures, could lead to a thermal moment that could possibly help reduce warpage. 相似文献
102.
Jia‐Wei Li Yu‐Jing Chiu Chia‐Jui Chang Hung‐Chieh He Yi‐Hsuan Tu Kuan‐Ting Lin Yu‐Liang Lin Tzu‐Hsun Kao Hsun‐Hao Hsu Hsiao‐Fan Tseng Tien‐Chang Lu Jiun‐Tai Chen 《大分子材料与工程》2020,305(1)
Polyimides (PIs) possess excellent mechanical properties, thermal stability, and chemical resistance and can be converted to carbon materials by thermal carbonization. The preparation of carbon nanomaterials by carbonizing PI‐based nanomaterials, however, has been less studied. In this work, the fabrication of PI nanofibers is investigated using electrospinning and their transformation to carbon nanofibers. Poly(amic acid) carboxylate salts (PAASs) solutions are first electrospun to form PAAS nanofibers. After the imidization and carbonization processes, PI and carbon nanofibers can then be obtained, respectively. The Raman spectra reveal that the carbon nanofibers are partially graphitized by the carbonization process. The diameters of the PI nanofibers are observed to be smaller than those of the PAAS nanofibers because of the formation of the more densely packed structures after the imidization processes; the diameters of the carbon nanofibers remain similar to those of the PI nanofibers after the carbonization process. The thermal dissipation behaviors of the PI and carbon nanofibers are also examined. The infrared images indicate that the transfer rates of thermal energy for the carbon nanofibers are higher than those for the PI nanofibers, due to the better thermal conductivity of carbon caused by the covalent sp2 bonding between carbon atoms. 相似文献
103.
Chia En Liu Wen Chieh Lan Hao Ting Yu Han Lin Yang I. Tseng Liu Hsiao Ping Hsu Chung Wen Lan 《International Journal of Applied Ceramic Technology》2020,17(1):146-152
Silicon kerf loss during wafer slicing and the broken quartz crucibles after silicon casting are two major solid wastes from photovoltaic (PV) industry. Especially, the recycle of kerf-loss silicon has become an urgent issue because near 100 000 t of solid wastes are generated every year. One of the most meaningful recycle routes of the kerf-loss silicon is to make silicon nitride crucibles to replace the quartz crucibles. In this study, we demonstrated how this is feasible through acid leaching refining, slip casting, and nitridation. The reaction-bonded silicon nitride (RBSN) crucibles after oxidation were found pure enough for silicon ingot growth. More importantly, they could be reused after ingot growth. With the present examples, the potential of using the kerf-loss silicon for fine ceramics is prominent. 相似文献
104.
Pauline Hibon Heinz von Seggern Hsin-Rong Tseng Christoph Leonhard Manuel Hamburger Gaëlle Béalle 《应用聚合物科学杂志》2020,137(29):48895
Interface control remains a top challenge of solution-processed organic light emitting diodes (OLED) stacks since the device performance heavily relies on it. Film stability of an inkjet deposited and crosslinked layer against subsequent exposure to a suitable inkjet printed solvent has been investigated. Impact of processing solvent (solvent used to prepare the polymer layer) on solution-cast thin film properties has already been shown for polymer films. To our knowledge, this study is the first one analyzing thin films stability against solvent exposure using technology relevant materials processed via inkjet printing (IJP). The outcome of this research showed that the stability of the crosslinked films is affected by the solvent used for ink formulation. These findings are of great interest for multilayered semiconductors devices, such as OLEDs, field-effect transistors and dye-sensitized solar cells. Differential scanning calorimetry (DSC) was used to quantify the efficiency of the polymer crosslinking reaction in pure powder and in thin films, as processed from different solvents. Crosslinking efficiency measured by DSC correlated well with the deformation induced by the solvent and observed on layer surfaces. The interaction in solution between polymer and solvent has also been evaluated to explain its impact on thin film stability against successive solvent printing. © 2020 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2020 , 137, 48895. 相似文献
105.
The microwave dielectric properties of (BaxMg1−x)(A0.05Ti0.95)TiO3 (A=Zr, Sn) ceramics were investigated with regard to substitution of Ba for Mg of A-site. The microwave dielectric properties were correlated with the Ba content. With an increase in Ba content from 0.01 to 0.1, the dielectric constant and the τf value increased, but the Q×f value decreased. The sintered (BaxMg1−x)(Zr0.05Ti0.95)TiO3 (called BxMZT) ceramics had a permittivity in the range of 19.1−20.6, quality factor from 180,000 to 25,000 GHz, and variation in temperature coefficient of resonant frequency from −35 to −39 ppm/°C with increasing composition x. For sintered (BaxMg1−x)(Sn0.05Ti0.95)TiO3 (called BxMST) ceramics, the dielectric constant increased from 19 to 20.5, Q×f value increased from 120,000 to 37,000 (GHz), and the τf value increased from −50 to −3.3 ppm/°C as the x increased from 0.01 to 0.1. When A=Sn and x=0.1, (Ba0.1Mg0.9)(Sn0.05Ti0.95)TiO3 ceramics exhibited dielectric constant of 20.5, Q×f value of 37,000 (GHz), and a near-zero τf value of −3.3 ppm/°C sintered at 1210 °C for 4 h. 相似文献
106.
TaN-Ag nanocomposite films were deposited by reactive co-sputtering on tool steel substrates. The films were then annealed using RTA (Rapid Thermal Annealing) at 350 °C for 2, 4, 8 min respectively to induce the nucleation and growth of Ag particles in TaN matrix and on film surface. C-AFM (Conductive Atomic force Microscopy) and FESEM (Field-Emission Scanning Electron Microscopy) were applied to examine the Ag nano-particles emerged on the surface of these thin films. A nano-indenter and a pin-on-disk tribometer were used to study the effect of annealing on the films' mechanical properties. The results reveal that annealing by RTA can cause Ag nano-particles to emerge on the TaN surface. Consequently, the mechanical properties of the films will vary depending on annealing conditions, Ag content, and Ag particle emergence. 相似文献
107.
This paper presents an approach in simulating complex manufacturing systems. The approach is founded on developing several general purpose simulation generators for an assembly station, a manufacturing cell, and an inventory transfer function. These simulation generators can then be linked together to create a model of a complex manufacturing system. A typical manufacturing system is modelled using these simulation generators and the results summarized. 相似文献
108.
Libo Zhao Yi‐Tsung Lu Fuqiang Li Kui Wu Shuang Hou Juehua Yu Qinglin Shen Dongxia Wu Min Song Wei‐Han OuYang Zheng Luo Tom Lee Xiaohong Fang Chen Shao Xun Xu Mitch A. Garcia Leland W. K. Chung Matthew Rettig Hsian‐Rong Tseng Edwin M. Posadas 《Advanced materials (Deerfield Beach, Fla.)》2013,25(21):2897-2902
109.
Wen-Kang Chen Hui-Hsin Tseng Ming-Chi Wei En-Chin Su I.-Ching Chiu 《International Journal of Hydrogen Energy》2014
A series of mesoporous Zr-SBA-15-supported Na catalysts was prepared and applied to the heterogeneous catalysis of canola oil transesterification. The effects of Si/Zr ratio, reaction time, and percentage of Na loading on the conversion to fatty acid methyl esters (FAME) were studied. The dependence of the textural structure and chemical properties of Zr-SBA-15 supports on Zr content was investigated using small-angle X-ray diffraction, Brunauer–Emmett–Teller analysis, transmission electron microscopy (TEM), and Fourier transform infrared (FTIR) spectroscopy. The results obtained from FTIR and TEM indicate that the incorporation of Zr atoms into the SBA-15 structure facilitated the formation of Brönsted acid sites and decreased the particle size of Na species. Catalysts with a higher Zr content enhanced the FAME yield. The optimum conditions determined were as follows: reaction temperature of 70 °C, 15 wt.% Na, reaction time of 6 h, and 12% catalyst content (wt.% oil) with a methanol/oil molar ratio of 6:1. The optimum conditions resulted in a FAME yield of up to 99%. 相似文献
110.
Li-Wei Kang Ching-Yu Tseng Chao-Long Jheng Ming-Fang Weng Chao-Yung Hsu 《电子科技学刊:英文版》2017,15(2):141-146
Straightforward image resizing operators without considering image contents (e.g., uniform scaling) cannot usually produce satisfactory results, while content-aware image retargeting aims to arbitrarily change image size while preserving visually prominent features. In this paper, a cluster-based saliency-guided seam carving algorithm for content-aware image retargeting is proposed. To cope with the main drawback of the original seam carving algorithm relying on only gradient-based image importance map, we integrate a gradient-based map and a cluster-based saliency map to generate a more reliable importance map, resulting in better single image retargeting results. Experimental results have demonstrated the efficacy of the proposed algorithm. 相似文献