Material properties and growth control of undoped and Sn-doped In2O3 thin films prepared by using ion beam technologies

Undoped (IO) and Sn-doped In₂O₃ (ITO) films have been deposited on glass and polymer substrates by an advanced ion beam technologies including ion-assisted deposition (IAD), hybrid ion beam, ion beam sputter deposition (IBSD), and ion-assisted reaction (IAR). Physical and chemical properties of the oxide films and adhesion between films and substrates were improved significantly by these technologies. By using the IAD method, non-stoichiometry and microstructure of the films were controlled by changing assisted oxygen ion energy and arrival ratio of assisted oxygen ion to evaporated atoms. Relationships between structural and electrical properties in ITO films on glass substrates were intensively investigated by using the IBSD method with changing ion energy, reactive gas environment, and substrate temperature. Smooth-surface ITO films (R_rms ≤ 1 nm and R_p-v ≤ 10 nm) for organic light-emitting diodes were developed with a combination of deposition conditions with controlling microstructure of a seed layer on glass. IAR surface treatment enormously enhanced the adhesion of oxide films to polymer substrate. The different dependence of IO and ITO films' properties on the experimental parameters, such as ion energy and oxygen gas environment, will be intensively discussed.     

Improvement in the volume efficiency of multilayered ceramic capacitors (MLCCs)

An attempt was made to improve the conventional lamination process in the multilayered ceramic capacitors (MLCCs) fabrication by adapting a solvent treatment on the BaTiO₃ green sheets. During the lamination process, additional particle rearrangement in the BaTiO₃ green block was stimulated by solvent treatment. This rearrangement resulted in a more compact structure of the BaTiO₃ green sheets compared to that obtained through the conventional lamination process. The overall thickness of BaTiO₃/Ni/BaTiO₃ laminates was also reduced after solvent treatment. It is suggested that miniaturization in the fabrication of MLCCs can be improved by adapting a solvent treatment during the lamination process.     

Preparation of SnO2 whiskers via the decomposition of tin oxalate

A new method for preparing SnO₂ whiskers by the decomposition of SnC₂O₄ is suggested. A Whisker-like morphology of a SnC₂O₄ precipitate was attained via the gradual addition of an oxalic acid solution to a hot SnCl₂ aqueous solution (T > 50^∘C). In comparison, when the solution temperature was either lower than 50^∘C or when ethanol was used as the solvent, the SnC₂O₄ precipitate showed an angular and relatively isotropic morphology. The morphology of the SnC₂O₄ precipitate remained even after its thermal decomposition into SnO₂ at 400^∘C indicating that SnC₂O₄ precipitation is a key step in preparing the whiskers. The formation mechanism of SnO₂ whiskers was explained by the supersaturation during the precipitation of SnC₂O₄.     

Baseband derived RF digital predistortion

A unique baseband derived RF predistortion system which uses lookup table coefficients extracted at baseband that directly RF envelope modulate a quadrature vector modulator is presented. The primary advantages of this architecture are that it combines the narrowband advantage of envelope predistortion with the accuracy of baseband predistortion.     

A miniature UWB planar monopole antenna with 5-GHz band-rejection filter and the time-domain characteristics

A planar monopole antenna with a staircase shape and small volume (25/spl times/26/spl times/1 mm/sup 3/) is proposed in this paper. With the use of a half-bowtie radiating element, the staircase-shape, and a modified ground plane structure, the proposed antenna has a very wide impedance bandwidth measured at about 11.6 GHz (2.9-14.5 GHz, bandwidth ratio about 1:5) below VSWR 2 including the WLAN band notched in the vicinity of 5 GHz. An omnidirectional radiation pattern is obtained. The group delay which is an indication of linearity between two proposed antennas is less than 1 ns. The electrical characteristics in terms of frequency and time domains and physical ones of the proposed antenna make it attractive for use in ultrawideband (UWB) systems.     

MLS‐based variable‐node elements compatible with quadratic interpolation. Part I: formulation and application for non‐matching meshes

Two‐dimensional variable‐node elements compatible with quadratic interpolation are developed using the moving least‐square (MLS) approximation. The mapping from the parental domain to the physical element domain is implicitly obtained from MLS approximation, with the shape functions and their derivatives calculated and saved only at the numerical integration points. It is shown that the present MLS‐based variable‐node elements meet the patch test if a sufficiently large number of integration points are employed for numerical integration. The cantilever problem with non‐matching meshes is chosen to check the feasibility of the present MLS‐based variable‐node elements, and the result is compared with that from the lower‐order case compatible with linear interpolation. Copyright © 2005 John Wiley & Sons, Ltd.     

Recrystallization and grain growth of cold-rolled gold sheet

Recrystallization and grain growth of a cold-rolled gold sheet with 98 pct reduction in area (RA) were investigated with electron backscatter diffraction (EBSD) and X-ray diffraction (XRD). Gold with some dopants (Be, Ca, and La) was used in this research and its recrystallization temperature was 320 °C. Isothermal annealing experiments at 400 °C, 500 °C, and 600 °C were carried out for the cold-rolled gold sheet, and recrystallization texture was examined. In the cold-rolled gold sheet, α- and β-fibers were measured mainly and some shear texture components were found on the surface. Shear texture components remained on the surface for 2 hours at 400 °C and were consumed by other recrystallized grains after 24 hours at 400 °C. Microstructure and texture evolution during in-situ annealing at 400 °C were investigated from the cold-rolled state to the fully recrystallized state using EBSD. Most of the newly, recrystallized grains came from the deformed β-fiber regions and consisted of β-fiber, cube, and other random orientations.     

Process Modeling for Precision Forming of Discrete Parts – State of the Technology and Critical Issues

This paper presents an overview on the application of FE simulation as a virtual manufacturing tool in designing manufacturing processes for precision parts. The processes discussed include forging, sheet metal forming and hydroforming. Determination of reliable input parameters to simulate a process is a key element in successful application of process simulation for process design in all the mentioned areas. These issues are discussed in detail. Practical examples of application of FE simulation are presented for improvement of the existing metal forming process and/or designing new metal forming process for manufacturing discrete precision parts in forging, sheet metal forming and hydroforming.     

Effect of Hot Band Annealing on Magnetic Properties in 3% Si Grain‐oriented Electrical Steels

Hot band annealing is known to be a prerequisite for good magnetic properties irrespective of manufacturing methods in grain‐oriented Fe‐3 wt.% Si electrical steels. In this study, the effects of hot band annealing on magnetic properties were investigated in 3% grain‐oriented electrical steels of low soluble AI contents and one‐stage cold rolling. Microstructure and precipitate distribution were compared with hot band annealing conditions. Secondary recrystallization behaviour with hot band annealing condition was also discussed.