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51.
A. Celaya Sanfiz T. W. Hansen F. Girgsdies O. Timpe E. Rödel T. Ressler A. Trunschke R. Schlögl 《Topics in Catalysis》2008,50(1-4):19-32
This work presents a detailed investigation of the preparation of MoVTeNbO x catalysts by hydrothermal synthesis. Phase-pure synthesis of M1 has been achieved applying the metals in a molar ratio Mo/V/Te/Nb = 1/0.25/0.23/0.12. Raman, UV/Vis spectroscopy, and SEM/EDX analysis show that the elements are inhomogeneously distributed in the initial suspension that is formed after mixing the metal salts in an aqueous medium. Iso- and heteropoly anions of molybdenum, free telluric acid as well as supra-molecular polyoxometalate clusters are observed in the solution, whereas all metals have been found in the precipitate. Complete rearrangement of molecular building blocks under hydrothermal conditions is essential for formation of phase-pure materials. Optimized synthesis conditions with respect to temperature and time result in the formation of a precursor consisting of nano-structured M1 characterized by an extended periodic organization in the [001] direction and a fairly homogeneous distribution of the elements. Residual ammonium containing supra-molecular species in the precursor result in the formation of phase mixtures during the subsequent crystallization by heat treatment in inert gas. Phase-pure M1 exhibits a distinct degree of flexibility with respect to the chemical composition that becomes obvious by incorporating Nb not exclusively into pentagonal bi-pyramidal units, but also into octahedral coordinated positions as shown by EXAFS. Anisotropic growth of the needle-like M1 crystals has been observed during the final heat treatment performed at 873–923 K in inert atmosphere disclosing a potential method to control the catalytic properties of MoVTeNbO x catalysts. 相似文献
52.
Barrier options are financial derivative contracts that are activated or deactivated according to the crossing of specified
barriers by an underlying asset price. Exact models for pricing barrier options assume continuous monitoring of the underlying
dynamics, usually a stock price. Barrier options in traded markets, however, nearly always assume less frequent observation,
e.g. daily or weekly. These situations require approximate solutions to the pricing problem. We present a new approach to
pricing such discretely monitored barrier options that may be applied in many realistic situations. In particular, we study
daily monitored up-and-out call options of the European type with a single underlying stock. The approach is based on numerical
approximation of the transition probability density associated with the stochastic differential equation describing the stock
price dynamics, and provides accurate results in less than one second whenever a contract expires in a year or less. The flexibility
of the method permits more complex underlying dynamics than the Black and Scholes paradigm, and its relative simplicity renders
it quite easy to implement. 相似文献
53.
Guillaume Bernard-Granger Christian Guizard Ahmed Addad 《Journal of Materials Science》2007,42(15):6316-6324
Sintering in air of an ultra pure α-alumina powder has been investigated. Isothermal experiments have been conducted on green
samples shaped by slip casting. The grain growth and densification kinetics have been established. The “relative density/grain
size” trajectory, called “sintering path”, has been drawn. Hypotheses concerning the mechanisms controlling grain growth and
densification have been formulated. For the first time, it is shown that grain growth and densification kinetics exhibit two
distinct regimes, where an initial point defect formation step plays a key role. When point defects have been generated, the
diffusion of the associated Al3+ cations controls grain growth and densification. 相似文献
54.
Peter Mertens Christian Stary Konrad Walser Thomas Deelmann Franz Lehner Sebastian Günther Christian Scheer 《WIRTSCHAFTSINFORMATIK》2006,48(4):288-295
Ohne Zusammenfassung 相似文献
55.
The influence of ointment formulation on the stability, the in-vitro release and the in-vivo absorption through the skin of rabbits was investigated. The choice of the selected ointments has no influence on the drug stability with the exception of an acidified emulsion base. A good correlation between in-vitro release and in-vivo absorption was found revealing that metronidazole was quickly released and effectively absorbed from a polyethylene glycol base. 相似文献
56.
S. Salar Behzadi Silvester Ölzant Reinhard Länger Christian Koban Frank M. Unger Helmut Viernstein 《European Food Research and Technology》2006,223(2):238-245
Inversion of sucrose is a stability problem particularly of candies with acidic taste that contain sucrose and small amounts of organic acids such as citric acid, since the free d-fructose produced by hydrolysis is hygroscopic. The following possibilities were investigated for preventing the hydrolysis of sucrose in tablets containing sucrose and citric acid: Adding various amounts of tri-sodium citrate to the formulation to neutralize the citric acid, (Hot) melt coating of citric acid and tri-sodium citrate with a vegetable fat at different coating ratios, variation of the ratio of coated citric acid and tri-sodium citrate in formulations, and compressing the formulations with different compression forces. After tablet processing and storage of tablets, the concentration of d-fructose was determined on the basis of enzymatic reactions. A response surface central composite design was used. The above-mentioned variations were chosen as independent variables and the amount of d-fructose was chosen as response variable. The lowest rates of inversion could be achieved by increasing the content of tri-sodium citrate and the ratio of coating material and decreasing the ratio of coated citric acid and tri-sodium citrate in the tablet formulations. The compression force had no significant effect on the inversion of sucrose. 相似文献
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59.
Markus Eisele Ralf Kolb Erwin Kraus Christian von Ehrenstein 《Informatik-Spektrum》2007,30(6):407-412
Zusammenfassung Das Schlagwort NetWeaver ist seit einiger Zeit in unserer Branche en vogue. Wie so oft, ist es nicht leicht, Marketingaspekte
vom informatischen Wesensgehalt zu unterscheiden. Dieser Beitrag m?chte hier helfen. 相似文献
60.