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881.
Christopher M. Gourlay Arne K. Dahle Hans I. Laukli 《Metallurgical and Materials Transactions A》2004,35(9):2881-2891
Banded defects are often found in high-pressure die castings. These bands can contain segregation, porosity, and/or tears,
and changing casting conditions and alloy are known to change the position and make-up of the bands. Due to the complex, dynamic
nature of the high-pressure die-casting (HPDC) process, it is very difficult to study the effect of individual parameters
on band formation. In the work presented here, bands of segregation similar to those found in cold-chamber HPDC aluminum alloys
were found in laboratory gravity die castings. Samples were cast with a range of fraction solids from 0 to 0.3 and the effect
of die temperature and external solid fraction on segregation bands was investigated. The results are considered with reference
to the rheological properties of the filling semisolid metal and a formation mechanism for bands is proposed by considering
flow past a solidifying immobile wall layer. 相似文献
882.
核磁共振谱的岩石孔喉结构分析 总被引:20,自引:1,他引:19
刘堂宴 ,王绍民 ,傅容珊 ,周明顺 ,李艳华 ,罗曼 .核磁共振谱的岩石孔喉结构分析 .石油地球物理勘探 ,2 0 0 3,38(3) :32 8~ 333岩心核磁共振 T2 谱和压汞分析数据均在一定程度上反映了岩石的孔喉结构 ,理论分析表明 ,这两组数据具有相关性。应用岩心核磁共振 T2 谱研究岩石孔喉结构 ,关键是确定 T2 与 Pc的转换系数。但以前的方法在 T2与 Pc 的转换过程中 ,需要涉及某些岩石特性参数 ,实用中有一定困难。本文直接利用岩心核磁共振 T2 谱和压汞分析数据之间的相关性 ,客观地确定 T2 与 Pc之间的转换系数 ,避免了确定岩石特性参数的困难。应用本文方法 ,对 6块岩心的多种核磁共振分析数据进行了对比分析 ,做出了 NMR (Nuclear Magnetic Resonance,简称NMR) T2 毛管力曲线和孔喉半径分布 ,并将这些结果与压汞分析的结果进行了对比。结果表明 ,岩心 NMR T2谱在实用性和评价精度上均略显优势 ;至少是在饱含油的条件下 ,岩心的 NMR T2 谱可以用于研究孔喉结构分布 ,油气的弛豫特性作为影响背景值存在 ,对于评价结果没有明显的影响 ;在全部 6块岩心中 ,T2 与 Pc 的转换系数位于 2 5 0 0~ 4 0 0 0μs· MPa之间。 相似文献
883.
Review on testers for measuring flow properties of bulk solids 总被引:3,自引:2,他引:1
Jörg Schwedes 《Granular Matter》2003,5(1):1-43
The author was asked by the International Fine Particle Research Institue (IFPRI) to write a critical review on shear testers
for IFPRI-members. The review was delivered to IFPRI in summer 1999. Following the contract with IFPRI it was not allowed
to publish the review elsewhere for at least two years. Granular Matter invited the author to submit the review in the original
form; during the refereeing process (besides other changes) it turned out that some remarks should be added here for clarification:
- Since 1999, the author is not aware of a really new device for testing bulk solid properties, which could lead to a change
of the general comments and conclusions provided in the review.
It was argued, that the review is referring too much to the work of Jenike, while the works of Johanson and Peschl were not
adequately cited. Both are excellent engineers with a lot of experience, but their basic ideas are not available in published
form, and if, they are not set in relation to alternative approaches so that an objective comparison in detail would be a
future research issue rather than a topic in this report.
A discussion on the influence of electrostatic charges was missing. There hardly is an influence, since the particles are
in continuous contact. Only with non-conducting plastic particles electrostatic charges could cause problems. But no relevant
experiments and results are known. In closed systems, the effect of electric charges is thus mainly neglected, but it is clear
that electrostatic forces are eminent in flows with a free surface – an issue not addressed in this review.
Received: 1 November 2002 相似文献
884.
885.
Grain refinement of Al-7Si alloys and the efficiency assessment by recognition of cooling curves 总被引:5,自引:0,他引:5
Under sand cup solidification condition, the influence of Ti, B concentration, and holding time on the grain size of a high-purity
Al-7Si alloy has been systematically studied. It is found that the grain size decreases rapidly at lower Ti or B additions,
and is almost constant at the higher concentrations. For Al-3B refined Al-7Si alloys, the grain size increases at the initial
period of holding time, and then rapidly becomes independent of holding time; while for Al-7Si alloys refined with Al-5Ti-1B,
the grain size increases with holding time throughout. To evaluate the refinement efficiency, a new method named “intelligent
evaluating of melt quality by pattern recognition of thermal analysis cooling curves” has also been introduced in this article.
The results show that comparing the cooling curve of the evaluated melt with those in a database to find the most similar
one to it can precisely assess the grain refinement efficiency of the measured Al-7Si alloy. In addition, the influence of
Ti, B addition levels, and pouring temperatures on some characteristic parameters of cooling curve has also been discussed. 相似文献
886.
887.
Effect of deformation route on microstructural development in aluminum processed by equal channel angular extrusion 总被引:3,自引:0,他引:3
Pei-Ling Sun Po-We Kao Chih-Pu Chang 《Metallurgical and Materials Transactions A》2004,35(4):1359-1368
Aluminum has been deformed by equal channel angular extrusion (ECAE) to obtain submicron-grained structures under different
deformation routes. The deformation routes were varied by rotating billets through 0, 90, and 180 deg between each extrusion
pass, and were designated as route A, BC, and C, respectively. Based on quantitative microstructural analysis, the effectiveness of the deformation route is shown
to depend upon the different definition used. The order of effectiveness is (a) A > BC > C for both 90 and 120 deg dies, in terms of the generation of high-angle grain boundaries (HAGBs); (b) BC > C > A for both 90 and 120 deg dies, in terms of the formation of equiaxed shape of grains; and (c) BC > A > C for 90 deg die and BC ∼ A > C for 120 die, in terms of reducing grain size. It is suggested that the generation of HAGBs can be related to the
accumulation of nonredundant strain, while the shape and orientation of grains may be linked to the shearing patterns of the
deformation route. 相似文献
888.
A fully-dense Cu-75 vol pct ZrW2O8 metal matrix composite was fabricated by hot isostatic pressing of Cu-coated ZrW2O8 particles. A small amount of the high-pressure γ-ZrW2O8 phase was created during the cooldown and depressurization following densification; near complete transformation to γ-ZrW2O8 was achieved by subsequent cold isostatic pressing. The thermal expansion behavior of the composite between 25°C and 325°C
was altered by the cold isostatic pressing treatment, and also depended on the length of time that had passed between thermal
cycles. The measured thermal expansion coefficients within specific temperature ranges varied from −6·10−6 K−1 to far above the thermal expansion coefficient of the copper matrix. The complex temperature-dependent expansion/contraction
behavior could be justified by considering the evolution of phase transformations taking place in the ZrW2O8 phase, which were observed by in-situ synchrotron X-ray diffraction measurements. 相似文献
889.
本文综术了集成电路工艺的Cu布线中Cu薄膜化学气相沉积(CVD)的研究背景,详细介绍了CVD生长Cu金属薄膜的国内外研究进展及CVD对前趋物的要求,并对前趋物的一些物理、化学性质进行了总结,最后,对薄膜沉积的计算机摸拟作了简要介绍。 相似文献
890.
挤出成型中遇到的最严重问题是熔体破裂,应用含氟改性剂可很好地消除熔体破裂现象。介绍了含氟改性剂对线性低密度聚乙烯(LLDPE)树脂挤出性能的影响及表面性能的改善。结果表明,在LLDPE挤出成型过程中加入含氟改性剂可有效消除熔体破裂现象,降低熔体温度,减小挤出机头压力,提高挤出效率,改善制品的外观质量。 相似文献