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101.
为研究离子液体/NMP对双马萃余煤的结构和萃取性能影响,首先分别用乙醇和丙酮对宁东双马煤样(SM)进行分步萃取,得到萃余煤(SMEC),然后将不同种类的离子液体(ILs)分别与N-甲基吡咯烷酮(NMP)混合后对SMEC进行萃取.用TG研究ILs/NMP萃取前后煤样热分解特性的变化,用FT-IR研究ILs/NMP萃取前后煤样官能团的变化,用GC/MS分析萃取物的种类.结果表明,ILs/NMP萃取后煤样的热失重增大,萃余煤中含氧官能团含量下降.另外,疏水型离子液体/NMP对SMEC煤的累积萃取率大于亲水型离子液体/NMP的累积萃取率.亲水型离子液体[Bmim]Cl/NMP和[Bmim]BF4/NMP分别萃取出51种和44种有机物质;疏水型离子液体[Bmim]NTf2/NMP和[Bmim]PF6/NMP分别萃取出28种和29种有机物质.疏水型离子液体/NMP对SMEC煤中含氧官能团化合物的萃取能力强于亲水型离子液体/NMP;疏水型离子液体/NMP对SMEC煤中含杂原子化合物的萃取能力小于亲水型离子液体/NMP. 相似文献
102.
热压烧结Ti3AlC2材料的制备、结构与性能研究 总被引:3,自引:0,他引:3
采用热压工艺研究了不同工艺制度和原料中不同的Si含量对Ti3AlC2合成的影响.研究表明在1 300℃~1 500℃,30MPa压力和Ar气氛中热压摩尔比为n(TiC)n(Ti)n(Al)n(Si)=2110.2的混合粉末,可以得到纯度达98%(质量分数)以上的致密块体Ti3AlC2材料;添加的Si均匀分布在基体中,形成固溶体,当添加Si的摩尔比为0.2时,固溶体的化学式为Ti2 76Al0 78Si0.22C2.烧结试样的晶体为层片状结构,1 300℃和1 400℃时,烧结试样的晶粒尺寸分别为10μm~15μm和20μm~30μm.材料的维氏硬度为3.3 GPa~5.0 GPa,弹性模量为289 GPa,抗压强度为785 MPa,抗弯强度为375 MPa,断裂韧性为7.0 MPa·m1/2;25℃时,电导率为3.1×106 S·m-1,热容为125.4 J/mol·K,热导率为27.5 W/m·K;热膨胀系数为8.8×10-6 K-1. 相似文献
103.
含硼金刚石的金属包膜成分及其物相的研究 总被引:1,自引:0,他引:1
本文采用铁基触媒加入硼铁的方法,在高温高压条件下合成了含硼金刚石,利用电子探针(EPMA),透射电子显微镜(TEM)两种检测手段,分析了含硼金刚石金属包膜的微观组织结构,化学组成成分,各组成成分的物相及其可能形成的原因。研究结果表明:金属包膜的成分及其物相由正交立方结构的(Fe,Ni)3C,面心立方的γ-(Fe,Ni),面心立方的Fe23(C,B)。及少量的FeB,Ni3B组成,这些成份主要来源于原材料,其含量在高温压过程中是瞬间变化的。 相似文献
104.
MicrostructureofTitaniumafterHydrogenationWangYu;WangPeixuan;ZhangJianwei(王宇)(王佩璇)(张建伟)UniversityofScienceandTechnologyBeijin... 相似文献
105.
106.
Hong Mei Gang Huang Tiancheng Liu Junguo Li 《International Journal of Software and Informatics》2007,1(1):101-128
Being the most popular runtime infrastructure for distributed systems, middleware can be viewed as a collection of common services. Since the development, deployment and maintenance of distributed systems rely largely on middleware services, the failure of middleware services puts a significant impact on the reliability and availability of the whole system. Though recovery-based fault tolerance is an effective way to improve the reliability of middleware services, it is far away from practice mainly because of the high complexity and cost of the recovery of correlated failures between interdependent services. In this paper,a framework for detecting and recovering the correlated failures of middleware services in an automated way is presented. First, the problem is investigated from two perspectives, i.e.,analyzing the role and impact of middleware services and illustrating a set of correlated failures in J2EE standard services as motivating examples. Then, a general coordinated recovery model is constructed with the elements necessary and su±cient for detecting and recovering correlated failures in middleware services. The supporting framework is demonstrated on three J2EE application servers, i.e., PKUAS, JBoss and JOnAS, one by one without fundamental modifications. Finally, based on the three enhanced application servers, many cases on J2EE common services, including the transaction service, database service, naming and directory service, security service and messaging service, are studied. The experiment results show the effectiveness and applicability of the framework presented in this paper. 相似文献
107.
甲基异噻唑啉酮类防腐剂是一类具有高效、广谱的杀菌和抑菌性能的防腐剂,广泛应用于各类防腐领域,但该类防腐剂能否用于食品相关产品还有待研究。文章主要介绍了甲基氯异噻唑啉酮与甲基异噻唑啉酮的混合物和甲基异噻唑啉酮两类防腐剂,以及近年各国对化妆品中甲基异噻唑啉酮类防腐剂的限量要求。从调查数据看,市场上大多食品用洗涤剂都含有甲基异噻唑啉酮类防腐剂,有的含量甚至超过化妆品安全技术规范中最大允许浓度,对人体健康可能会产生较大威胁。因此,有必要对食品用洗涤剂中甲基异噻唑啉酮类防腐剂进行检测,并建议在食品用洗涤剂国家标准中列入对甲基异噻唑啉酮类防腐剂的限量。 相似文献
108.
Chemical looping gasification (CLG) of Ningdong coal by using Fe2O3 as the oxygen carriers (OCs) was studied, and the gasification characteristics were obtained. A computation fluid dynamics (CFD) model based on Eulerian‐-Lagrangian multiphase framework was established, and a numerical simulation the coal chemical looping gasification processes in fuel reactor (FR) was investigated. In addition, the heterogeneous reactions, homogeneous reactions and Fe2O3 oxygen carriers' reduction reactions were considered in the gasification process. The characteristics of gas flow and gasification in the FR were analyzed and it was found that the experiment results were consistent with the simulation values. The results show that when the O/C mole rate was 0.5:1, the gasification temperature was 900 ℃ and the water vapor volume flow rate was 2.2 ml·min-1, the mole fraction of syngas reached a maximum value of the experimental result and simulation value were 71.5% and 70.2%, respectively. When the O/C mole rate was 0.5:1, the gasification temperature was 900 ℃, and the water vapor volume flow was 1.8 ml·min-1; the gasification efficiency reached the maximum value was 62.2%, and the maximum carbon conversion rate was 84.0%. 相似文献
109.
110.
Ruoyi Lin Tao Zou Qiming Mei Zhengfeng Wang Mei Zhang Shuguang Jian 《International journal of molecular sciences》2021,22(9)
Canavalia rosea (bay bean), distributing in coastal areas or islands in tropical and subtropical regions, is an extremophile halophyte with good adaptability to seawater and drought. Late embryogenesis abundant (LEA) proteins typically accumulate in response to various abiotic stresses, including dehydration, salinity, high temperature, and cold, or during the late stage of seed development. Abscisic acid-, stress-, and ripening-induced (ASR) genes are stress and developmentally regulated plant-specific genes. In this study, we reported the first comprehensive survey of the LEA and ASR gene superfamily in C. rosea. A total of 84 CrLEAs and three CrASRs were identified in C. rosea and classified into nine groups. All CrLEAs and CrASRs harbored the conserved motif for their family proteins. Our results revealed that the CrLEA genes were widely distributed in different chromosomes, and all of the CrLEA/CrASR genes showed wide expression features in different tissues in C. rosea plants. Additionally, we introduced 10 genes from different groups into yeast to assess the functions of the CrLEAs/CrASRs. These results contribute to our understanding of LEA/ASR genes from halophytes and provide robust candidate genes for functional investigations in plant species adapted to extreme environments. 相似文献