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91.
The feasibility of gallium as a catalyst for vapour-liquid-solid (VLS) nanowire (NW) growth deriving from an implantation process in silicon by a focused ion beam (FIB) is investigated. Si(100) substrates are subjected to FIB implantation of gallium ions with various ion fluence rates. NW growth is performed in a hot wall chemical vapour deposition (CVD) reactor at temperatures between 400 and 500?°C with 2% SiH(4)/He as precursor gas. This process results in ultra-fast growth of (112)- and (110)-oriented Si-NWs with a length of several tens of micrometres. Further investigation by transmission electron microscopy indicates the presence of a NW core-shell structure: while the NW core yields crystalline structuring, the shell consists entirely of amorphous material. 相似文献
92.
Vanita Vanita Aamir Iqbal Waidha Sandeep Yadav Jörg J. Schneider Oliver Clemens 《International Journal of Applied Ceramic Technology》2023,20(1):236-250
All-solid-state lithium-ion batteries (ASSLIBs) are promising alternatives to conventional organic electrolyte-based batteries due to their higher safety and higher energy densities. Despite advantages, ASSLIBs suffer from issues like high charge transfer resistances due to the brittleness of the inorganic solid electrolyte and chemical instabilities at the lithium/electrolyte interface. Within this work, we investigate composite electrolytes (CEs) based on garnet-type Li6.4La3Zr1.4Ta0.6O12 (LLZTO), polyethylene oxide, and lithium bis(trifluoromethanesulfonyl)imide, prepared via a solvent-free cryo-milling approach in contrast to conventional solvent-mediated synthesis. Compositions ranging from polymer-rich to garnet-rich systems are investigated via X-ray diffraction, Raman spectroscopy, and Fourier transform infrared spectroscopy in order to determine the compatibility of the cryo-milling process toward membrane fabrication along with the possible chemical interactions between the composite membrane components. Electrochemical impedance spectroscopy is used to study the role of ceramic to polymer weight fraction on ionic conductivity. It is shown that the addition of succinonitrile (SCN) to the garnet-rich CEs can significantly improve the ionic conductivity compared to the SCN-free CEs. 相似文献
93.
Benjamin J. Clemens;C. Michael Wagner; 《河流研究与利用》2024,40(8):1447-1468
Organisms have adapted to dynamic river flows as part of the natural flow regime. However, climate change and humans' use of fresh water are associated with decreases in the quality and quantity of surface waters. In addition, river impoundments and water withdrawals for human use regulate and dampen the dynamism of flow in many rivers. These changes to the natural flow regime can impact the spawning migrations of lampreys (Petromyzontiformes). Here, our goal is to review the ecology of lamprey spawning migrations associated with river flows, with considerations for controlling invasive sea lamprey (Petromyzon marinus) and conserving native lampreys (including native, anadromous sea lamprey). We identify five common themes: (1) natural flow regimes provide a competitive edge to native fishes over non-native fishes; (2) high flows (up to a threshold) attract adult lamprey and large streams attract large numbers of lamprey; (3) larval lamprey pheromones attract adult lampreys; (4) behavioral responses by adult lamprey to flow (including localized hydraulics) can inform dam passage and trapping methods; and (5) changes to rivers induced by climate change have been implicated in changing the phenology of run timing and spawning location. Controlling invasive sea lamprey and conserving native lampreys can be done with pheromones and flow management. Pheromones may be of more use under focused management efforts to control invasive sea lamprey, whereas flow management can provide a foundation for conservation of native lampreys. 相似文献
94.
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96.
Clemens Preisinger Moritz Heimrath Adam Orlinski Arne Hofmann Klaus Bollinger 《Stahlbau》2019,88(3):184-193
97.
Moritz Riebisch Philipp Weiß Clemens Cremer Ibrahim Aboulkhair Andreas Bührig-Polaczek 《Materials Science & Technology》2018,34(6):725-730
Solid solution-strengthened ductile iron (DI) exhibits outstanding mechanical properties due to the high silicon content. The strengthening by silicon addition is limited since additions above 4.3?wt-% lead to embrittlement. For a further improvement of mechanical properties, other alloying elements need to be considered. In the present work, the effect of various copper additions on the microstructure and the mechanical properties of solid solution-strengthened DI were investigated. The results show that no appreciable strengthening can be achieved by copper addition without the formation of pearlite in the matrix. The pearlite content increases considerably for Cu-additions above 0.23?wt-% and is independent of the cooling rate for the cooling conditions analysed. 相似文献
98.
Rotor‐stator‐machinery is characterized in continuous operation by a homogeneous power input and a defined residence time. The influence of the equipment configuration and process design in the laminar flow regime was considered little till now. In order to fill this knowledge gap, the process behavior of this type of device was systematically investigated experimentally under axial flow conditions, as well as an energetic optimization of the machine configuration was performed. 相似文献
99.
Modern high voltage direct current (HVDC) power cables consist of nonlinear electric field and temperature depending insulation materials, eg, polyethylene (PE) or mass-impregnated paper (MI). Within the insulation material, slowly time varying electric fields are the result of accumulated space charges. Due to the long operation time of power cables, the stationary charge distribution and the resulting additional field stresses inside the insulation material need to be taken into account, to ensure a stable operation of the cable system. The long accumulation time of charges in comparison to fast charge dynamics usually requires extended computation times within transient electro-quasistatic simulation models. An alternative approach to calculate the final steady-state charge distribution arises from the simultaneous solution of both, the stationary current and the electrostatic potential problem, which are nonlinearly coupled by Ohm's law. Each of the two potential equations are discretized using the finite difference method. Utilizing a nonlinear fixed point iteration for the electric potential, the steady-state solution of the charge distribution is computed until convergence is obtained. During this pseudo time stepping process, oscillations may occur that yield incorrect results of the charge distribution. These oscillations are eliminated utilizing underrelaxation strategies. Numerical tests on a cylindrical and a plane parallel problem, using both approaches for the calculation of the steady-state charge distribution, show a faster computation with the nonlinear fixed point iteration, reducing the computation time by at least one order of magnitude. 相似文献
100.
Ioanna Mela Chetan Poudel Miguel Anaya Géraud Delport Kyle Frohna Stuart Macpherson Tiarnan A. S. Doherty Anna Scheeder Samuel D. Stranks Clemens F. Kaminski 《Advanced functional materials》2021,31(23):2100293
Halide perovskites are a versatile class of semiconductors employed for high performance emerging optoelectronic devices, including flexoelectric systems, yet the influence of their ionic nature on their mechanical behavior is still to be understood. Here, a combination of atomic-force, optical, and compositional X-ray microscopy techniques is employed to shed light on the mechanical properties of halide perovskite films at the nanoscale. Mechanical domains within and between morphological grains, enclosed by mechanical boundaries of higher Young's Modulus (YM) than the bulk parent material, are revealed. These mechanical boundaries are associated with the presence of bromide-rich clusters as visualized by nano-X-ray fluorescence mapping. Stiffer regions are specifically selectively modified upon light soaking the sample, resulting in an overall homogenization of the mechanical properties toward the bulk YM. This behavior is attributed to light-induced ion migration processes that homogenize the local chemical distribution, which is accompanied by photobrightening of the photoluminescence within the same region. This work highlights critical links between mechanical, chemical, and optoelectronic characteristics in this family of perovskites, and demonstrates the potential of combinational imaging studies to understand and design halide perovskite films for emerging applications such as photoflexoelectricity. 相似文献