Influence of electroplating conditions on magnetic properties of Fe-36wt.% Ni alloy film

A Fe-Ni soft magnetic film was prepared in sulphate solution by electroplating. The influences of the molar ratio of n [Fe2+ ]/ n [Ni2+ ], current density, bath temperature, pH and L-ascorbic acid concentration on magnetic properties of Fe-Ni alloy film were investigated. The results show that the saturated flux density(BS) of the film increases initially and decreases after it reaches the specific value with the increase of n [Fe2+ ]/ n [Ni2+ ] molar ratio, current density, bath temperature and pH. However, the relationship between L-ascorbic acid concentration and B S keeps linear. It is observed that the coercive force( Hc) is enhanced with the increase of n [Fe2+ ]/ n [Ni2+ ] molar ratio, current density and pH. By comparison, when the bath temperature increases, Hc always decreases. With the increase of L-ascorbic acid concentration, the coercive force increases initially and then decreases.     

厚实工作台的铸造工艺

对厚大工作台铸件表面结疤和石墨孔洞缺陷的原因进行了分析，并采取相应措施：采用过滤网挡渣，确保造型、刷涂料、浇注之间有充分的时间间隔，控制涂料的配制和涂刷，控制铁液成分，采用冷铁等，使铸件达到质量要求。     

CoSb3基Skutterudite化合物拉曼光谱研究

Skutterudite材料因具有特殊的晶体结构成为当前最有前途的热电材料之一,为深入研究填充Skutterudite化合物的热传导机制,对化合物的声子振动模式及置换、填充原子对声子模的影响进行了研究.通过对CoSb3,Co3.5Fe0.5Sb12的偏振拉曼谱研究,确认了一个Ag模,且与理论计算吻合较好.对CoSb3,Co3.5Fe0.5Sb12和La0.6Co3.5Fe0.5Sb12拉曼谱的对比研究表明,单纯Fe置换对拉曼谱影响很小,而La部分填充则使部分拉曼峰明显展宽,分析认为,这一现象主要源于填充原子在晶格空隙中的扰动.     

激光近成形金属零件过程中涂覆层的组织及性能

利用激光近成形技术，在1Cr18Ni9Ti不锈钢基体上采用镍基合金和钴基合金粉末进行单道涂覆烧结试验，获得具有快速凝固组织特征的激光涂覆层，并分析了影响涂覆层组织和质量的激光参数和工艺参数。     

氮化硅陶瓷刀具表面涂覆高硬耐磨氮化钛涂层研究

用高能量密度脉冲等离子体于室温下在氮化硅陶瓷刀具上成功沉积了高硬耐磨的氮化钛涂层。薄膜厚度用光学显微镜和俄歇电子能谱仪测定，薄膜元素和相组成与分布分别用俄歇电子能谱仪、X光电子能谱以及X光衍射仪测定，薄膜微观结构用扫描电镜观察，薄膜表面粗糙度用光学显微镜测定，薄膜力学性能由纳米压痕实验和纳米划痕实验确定，薄膜的磨损性能用上业条件下的切削实验评价。实验结果表明，在最优化条件下，涂层与基体的结合力很好，纳米划痕实验临界载荷达80mN以上；氮化钛涂层具有很高的硬度和杨氏模量，分别达28GPa和350GPa以上。涂层刀具用于HB达2200MPa—2300MPa的HT250钢切削实验表明，刀具耐磨损能力增强，寿命明显提高。     

The integrated intelligent system for welding seam error and penetration depth identification

A integrated intelligent system for seam tracking and penetration control is given. The system received information of welding seam error and penetration depth from only one sensor, then, it realized seam tracking and penetration control simultaneously. This paper introduces constitution of the system, methods of information recognition, design of the neuralfuzzy controller and results practically.     

FRACTAL ANALYSES OF DIRECTIONAL SOLIDIFICATION BEHAVIOR OF A Ni-BASE SUPERALLOY

The morphology of solid/liquid interface of a directionally solidification process is describedby means of fractal analysis,and the relations among the fractal dimension of the solid/liq-uid interface,solidification rate,dendrite arm space and the phosphorus content of the test al-loys have been given.It was found that the increase of the solidification rate and the phos-phorus content of the test alloy will lead to a increase,following the regularity of exponentialfunction,in the fractal dimension of solid/liquid interface.Furthermore,by combining thefractal theory and the thermodynamic principle with the measured results,it has been provedthat the fractal dimension is not only a kind of simple geometrical parameter used in des-cribing irregular geometry,but also a state function depending the change of solidificationparameters and chemical compositions.     

SiO2微粉分形分布对超薄切割砂轮片拉伸性能的影响

在研究利用光敏树脂快速成型工艺制作超薄切割砂轮片时，发现往光敏树脂中添加适量的SiO2微粉，光敏树脂的拉伸强度明显增加。添加的SiO2微粉的用量的不同，在光敏树脂中形成的分形分布不同，对光固化成型后的超薄切割砂轮片的拉伸强度有不同的影响。本文通过研究SiO2微粉在光敏树脂中分布特征，根据分形理论，用分形维来描述其分布特征及其对光敏树脂光固化成型后的超薄切割砂轮片的拉伸性能的影响。     

北满特钢40t-LFV精炼炉真空系统改造

简要介绍了西安重型机械研究所为北满特钢一电炉分厂原有 40 t-LFV设备真空系统进行改造的具体内容。改造后其真空系统不仅能满足不同钢种精炼工艺的要求 ,且真空系统的能耗指标达到世界先进水平