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21.
A novel supercritical-gas (toluene) extract, comprising 17.0% of a low-rank coal, was separated by a combination of solvent fractionation and both silica-gel and gel-permeation chromatography. The average structure of the soluble fractions, together amounting to 85% of the extract, was investigated by a variety of spectroscopic methods, including high-resolution 1H nuclear magnetic resonance, proton-decoupled pulse Fourier transform 13C magnetic resonance, infrared and low-ionizing-voltage mass spectrometry. Analyses were also made by gas chromatography. The results for the low-oxygen fractions are consistent with a generally open-chain polynuclear aromatic average structure with about 33% of the available sites carrying alkyl substituents. The most common of these is methyl, but there are also substantial numbers of longer-chain alkyls, some branched, and naphthenic groups. The fractions rich in oxygen also have similar structure but for the presence of phenolic hydroxyl groups, and, as is demonstrated for the first time by 13C n.m.r., ether oxygen links. Aliphatic constituents are mainly straight-chain alkanes with some branched-chain and isoprenoid hydrocarbons. These conclusions are discussed in terms of the thermal history of the extract and are compared with other contemporary views on the low-molecular-weight constituents of coal. 相似文献
22.
The partitioning of a single polymer chain into a slit in a good solvent with different surface interactions is examined through Monte Carlo simulations from subcritical regime to adsorptive regime. The chain conformation in the subcritical regime is not perturbed by the surface interactions significantly. In the adsorptive regime, the conformation of the chain is strongly perturbed by the surface interactions. The confinement free energy in the two regimes maybe written in a uniform formula, βΔμconf∼c1N(a/D)xεw+c2N(a/D)1/ν with x∼2.0 or larger in the subcritical regime and ∼1.0 in the adsorptive regime, where ν is the Flory exponent, D is the slit width, N is the chain length, a is the monomer size, and εw is the surface interaction energy between the polymer beads and the slit. This formula is valid for a long chain in the narrow slit in the subcritical regime or when the adsorption layer h>D in the adsorptive regime. A critical behavior occurs when εw is at the critical adsorption point and x=1/ν, then Δμconf will have little dependence on N or D. Higher order terms that are neglected in the above equation, however, may be present that could lead to a weak dependence of K on N and D even in the critical adsorption point. 相似文献
23.
Tessa E. Smith David H. Abbott Andrew J. Tomlinson Jerzy A. Mlotkiewicz 《Journal of chemical ecology》1997,23(11):2523-2546
The hypothesis was tested that marmosets have differential displays of investigatory behavior towards circumgenital scent marks from socially dominant females based on degree of familiarity. In a series of two-choice behavioral discrimination bioassays, dominant males together with subordinate and dominant females were presented concurrently with scent secretions from familiar versus unfamiliar dominant females, and their investigative behaviors towards the scent were recorded. Test animals directed significantly different amounts of investigative behaviors towards familiar versus unfamiliar scents when the scent stimuli involved complete circumgenital scent marks, glandular secretion only, or urine only. When animals discriminated between the two scent samples, they did so by directing significantly increased amounts of behavior to scent from unfamiliar females. Chemical cues promoting differential displays of behavior to familiar versus unfamiliar scents appeared to be volatile in nature and were effective in the scent mark for at least one day following deposition. The reliable ability of marmosets to consistently discriminate between odors from familiar versus unfamiliar dominant females provides strong circumstantial evidence that individual female marmosets have distinct chemical signatures. The ability of marmosets to discriminate the odor from familiar versus unfamiliar dominant females may be important in the context of intergroup relations. 相似文献
24.
We present a model of spatial navigation based on the non-convergent dynamics of brain activity. The system includes a hippocampal module that processes global spatial information and a cortical module that deals with local sensory information. We test the model using several spatial navigation paradigms: goal finding, shortcutting and detouring. Computer simulations show that the performance of the agent qualitatively matches that of animals and related models. This new approach provides a novel interpretation of how the brain accomplishes spatial navigation. 相似文献
25.
James M. Chappell Azhar Iqbal M. A. Lohe Lorenz von Smekal Derek Abbott 《Quantum Information Processing》2013,12(4):1719-1735
The Grover search algorithm is one of the two key algorithms in the field of quantum computing, and hence it is desirable to represent it in the simplest and most intuitive formalism possible. We show firstly, that Clifford’s geometric algebra, provides a significantly simpler representation than the conventional bra-ket notation, and secondly, that the basis defined by the states of maximum and minimum weight in the Grover search space, allows a simple visualization of the Grover search analogous to the precession of a spin- ${\frac{1}{2}}$ particle. Using this formalism we efficiently solve the exact search problem, as well as easily representing more general search situations. We do not claim the development of an improved algorithm, but show in a tutorial paper that geometric algebra provides extremely compact and elegant expressions with improved clarity for the Grover search algorithm. Being a key algorithm in quantum computing and one of the most studied, it forms an ideal basis for a tutorial on how to elucidate quantum operations in terms of geometric algebra—this is then of interest in extending the applicability of geometric algebra to more complicated problems in fields of quantum computing, quantum decision theory, and quantum information. 相似文献
26.
Derek A. Paley Naomi Ehrich Leonard Rodolphe Sepulchre 《Systems & Control Letters》2008,57(3):209-215
We provide a cooperative control algorithm to stabilize symmetric formations to motion around closed curves suitable for mobile sensor networks. This work extends previous results for stabilization of symmetric circular formations. We study a planar particle model with decentralized steering control subject to limited communication. Because of their unique spectral properties, the Laplacian matrices of circulant graphs play a key role. We illustrate the result for a skewed superellipse, which is a type of curve that includes circles, ellipses, and rounded parallelograms. 相似文献
27.
Derek Lea 《计算机光盘软件与应用》2008,(2):94-97
智能对象的出现使得在Photoshop和Illustrator中使用像素和矢量之间的差别迅速消失。Derek Lea将会在制作一个结构完美且矢量明显的作品的同时为你解释原因。 相似文献
28.
Derek Hull 《International Journal of Fracture》1994,70(1):59-79
A modification of Sommer's classical experiment [4] has been used to fracture rods of a brittle epoxy resin in mixed mode I/III stress conditions. The nucleation and growth of cracks in an increasing K
III/K
I stress field have been investigated, particularly in relation to the formation of river lines and the evolution of multiple cracks between river lines to form smooth helicoid surfaces. The fractographic features associated with the progressive development of river line patterns involving crack bowing at river line steps, interaction between arrays of cracks and the coalescence of river lines are described. As K
III/K
I increases the scale of the river line patterns increases but the patterns remain self similar. Using principles from differential geometry it is shown that helicoid surfaces can be generated entirely by crack evolution involving tilting without twiting.Emeritus Goldsmiths' Professor of Metallurgy, University of Cambridge, U.K. 相似文献
29.
Journal of Intelligent Information Systems - Offline evaluation of recommender systems (RSs) mostly relies on historical data, which is often biased. The bias is a result of many confounders that... 相似文献
30.
Kim Tak H. Sirdaarta Joseph P. Zhang Qian Eftekhari Ehsan St. John James Kennedy Derek Cock Ian E. Li Qin 《Nano Research》2018,11(4):2204-2216
Nano Research - The toxicity of nanoparticles in a biological system is an integration of effects arising from surface functionality, particle size, ionic dissolution, etc. This complexity suggests... 相似文献