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41.
Flame retardant and the degradation mechanism of high impact polystyrene/Fe-montmorillonite nanocomposites 总被引:1,自引:1,他引:0
High impact polystyrene/Fe-montmorillonite (HIPS/Fe-MMT) nanocomposites were successfully prepared by melting intercalation.
The nanostructures of HIPS/Fe-MMT were testified by X-ray diffraction (XRD) and transmission electron microscope (TEM). Corresponding
to pure HIPS, the thermal stability of HIPS/Fe-MMT nanocomposites was notably improved. The peaks of heat release rate (PHRR)
and the mass loss rate (MLR) were significantly reduced after the formation of the HIPS/Fe-MMT nanocomposites from cone calorimetry.
And nanocomposites PHRR was further lower with the increase of Fe-MMT content in the range of 1 to 5 wt%. The degradation
mechanism of HIPS and HIPS/Fe-MMT nanocomposites was conducted by pyrolysis gas chromatography mass spectrometry (Py-GC-MS).
And the reason of the enhancement of thermal stability maybe is that structural iron is the operative site for radical trapping
in the Fe-MMT and the nanostructure enhances the interaction of the chains of the HIPS. 相似文献
42.
超低碳奥氏体不锈钢00Cr18Ni10还原脱磷研究 总被引:1,自引:0,他引:1
在 2 5kg真空感应炉上用镁钙合金对超低碳奥氏体不锈钢 0 0Cr18Ni10进行了还原脱磷试验。通过充入工业纯氩使炉内压力为 6 6 .6 6kPa和精炼时的反应温度 14 5 0~ 15 0 0℃ ,加入镁钙合金 5 0kg t和助熔剂CaF2 11kg t,可使精炼后 0 0Cr18Ni10的磷含量进一步降低到 (5 0~ 6 0 )× 10 - 6 ,钢中氧、硫含量分别稳定降到(4~ 6 )× 10 - 6 和 15× 10 - 6 。 相似文献
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DP Kiel RH Myers LA Cupples XF Kong XH Zhu J Ordovas EJ Schaefer DT Felson D Rush PW Wilson JA Eisman MF Holick 《Canadian Metallurgical Quarterly》1997,12(7):1049-1057
Previous studies of the vitamin D receptor (VDR) polymorphisms and bone mineral density (BMD) have suggested that there may be differences in calcium absorption among groups of women with different VDR genotypes, and that the association may be stronger in younger women. To investigate the association between the VDR polymorphisms and BMD, this study was undertaken in the Framingham Study Cohort and a group of younger volunteers. Subjects from the Framingham Study (ages 69-90 years) included those who underwent BMD testing and who had genotyping for the VDR alleles (n = 328) using polymerase chain reaction methods and restriction fragment length polymorphisms with BsmI (B absence, b presence of cut site). A group of younger volunteer subjects (ages 18-68) also underwent BMD testing and VDR genotyping (n = 94). In Framingham Cohort subjects with the bb genotype, but not the Bb or BB genotypes, there were significant associations between calcium intake and BMD at five of six skeletal sites, such that BMD was 7-12% higher in those with dietary calcium intakes greater than 800 mg/day compared with those with intakes < 500 mg/day. The data also suggested that BMD was higher in persons with the bb genotype only in the group with calcium intakes above 800 mg/day. No significant differences were found in the Framingham Cohort for age-, sex-, and weight-adjusted BMD at any skeletal site between those with the BB genotype and those with the bb genotype regardless of 25-hydroxyvitamin D levels or country of origin. In the younger volunteers, BMD of the femoral neck was 5.4% higher (p < 0.05) in the bb genotype group compared with the BB group and 11% higher (p < 0.05) in males with the bb genotype compared with the BB group. There were no significant differences at the lumbar spine. In this study, the association between calcium intake and BMD appeared to be dependent upon VDR genotype. The findings of an association between dietary calcium intake and BMD only in the bb genotype group suggests that the VDR genotype may play a role in the absorption of dietary calcium. Studies that do not consider calcium intake may not detect associations between VDR genotype and BMD. In addition, the association between VDR alleles and BMD may become less evident in older subjects. 相似文献
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通过在三种不同的强化负荷下进行深沟球轴承疲劳寿命试验,并与常规试验一组结果对比。结果表明,适当地加大滚动轴承疲劳寿命试验负荷,可以大大缩短试验时间,而疲劳寿命依然服从Weibul分布,且与常规试验结果基本一致,同时疲劳破坏的形式仍是表面下萌生裂纹,然后扩展至表面形成剥落。 相似文献
49.
目前,光折变非线性元件在光学并行图像处理中有着非常广泛的应用。光折变晶体用于图像边缘增强,图像加、减运算,非相干—相干转换(PICOC),图像相关和卷积运算等研究已取得显著成果。本文研究了Cu;KNSBN晶体中多重图像的存贮问题,指出可以利用这种技术实现光学目标识别并给出了一些初步实验结果。此外,还从理论上分析了具有相同衍射效率的多重全息信息记录技术。 相似文献
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