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51.
Retrogradation rate and extent were determined by differential scanning calorimetry and rheology measurements on 40% dry matter gels made from pea, modified waxy maize, rice, waxy rice, wheat, manioc, potato and microwaved irradiated potato starches. As a result, each starch retrogrades differently, depending also on the measurement technique. Nevertheless, potato and pea starches seem to be the most sensitive and the waxy and modified waxy types are the least sensitive to retrogradation. 相似文献
52.
Specific cationic photoinitiators for near UV and visible LEDs: Iodonium versus ferrocenium structures
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Haifaa Mokbel Joumana Toufaily Tayssir Hamieh Frederic Dumur Damien Campolo Didier Gigmes Jean Pierre Fouassier Joanna Ortyl Jacques Lalevée 《应用聚合物科学杂志》2015,132(46)
Two iodonium salts based on a coumarin chromophore are investigated for polymerization upon light emitting diode irradiations (LEDs). They work as one‐component photoinitiators. They initiate the cationic polymerization of epoxides (under air) and vinylethers (laminate) upon exposure to violet LEDs (385 and 405 nm). Excellent polymerization profiles are recorded. Their efficiency is quite similar to that of a ferrocenium salt. Interpenetrating polymer networks can also be obtained through a concomitant cationic/radical photopolymerization of an epoxy/acrylate blend monomer. The light absorption properties of these new salts as well as the involved photochemical mechanisms are investigated for the first time through electron spin resonance, laser flash photolysis, steady state photolysis experiments. Molecular orbital calculations are also used to shed some light on the initiation mechanisms. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 42759. 相似文献
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54.
Design challenges of a 65 nm CMOS stacked folded differential PA structure for mobile communications
Yohann Luque Nathalie Deltimple Eric Kerhervé Didier Belot 《Analog Integrated Circuits and Signal Processing》2011,66(2):155-162
In this paper, a novel phase-locked loop (PLL) architecture with multiple charge pumps, which is used to design a fast-locking
PLL and a low-phase-noise PLL, is proposed. The effective capacitance and resistance of the loop filter in terms of voltage
is scaled up/down according to the locking status by controlling the magnitude and direction of the charge pump current. Two
PLLs, one with a fast-locking characteristic and the other with a low-phase-noise characteristic, are designed and fabricated
in a 0.35-μm CMOS process based on the proposed architecture. The fast-locking PLL has a locking time of less than 6 μs and
a phase noise of −90.45 dBc/Hz at 1 MHz offset. The low-phase-noise PLL has a locking time of 25 μs, a phase noise of −105.37 dBc/Hz
at 1 MHz offset, and a reference spur of −50 dBc. Both PLLs have an 851.2 MHz output frequency. 相似文献
55.
Florence Barbé Olivia Ménard Yann Le Gouar Caroline Buffière Marie-Hélène Famelart Béatrice Laroche Steven Le Feunteun Didier Dupont Didier Rémond 《Food chemistry》2013,136(3-4):1203-1212
This study aimed to determine the kinetics of milk protein digestion and amino acid absorption after ingestion of four dairy matrices by six minipigs: unheated or heated skim milk and corresponding rennet gels. Digestive contents and plasma samples were collected over a 7 h-period after meal ingestion. Gelation of milk slowed down the outflow of the meal from the stomach and the subsequent absorption of amino acids, and decreased their bioavailability in peripheral blood. The gelled rennet matrices also led to low levels of milk proteins at the duodenum. Caseins and β-lactoglobulin, respectively, were sensitive and resistant to hydrolysis in the stomach with the unheated matrices, but showed similar digestion with the heated matrices, with a heat-induced susceptibility to hydrolysis for β-lactoglobulin. These results suggest a significant influence of the meal microstructure (resulting from heat treatment) and macrostructure (resulting from gelation process) on the different steps of milk proteins digestion. 相似文献
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57.
Liyuan Liang Jaime Ruiz Didier Astruc 《Journal of Inorganic and Organometallic Polymers and Materials》2010,20(3):503-510
Alkyne protection by complexation of ethynylferrocene with dicobalt octacarbonyl followed by regioselective acetylation, then deprotection and “click” reaction with a nona-azido-terminated arene-cored dendrimer leads to the heterodifunctional nona(1,2,3-triazolyl-acetylferrocenyl) dendrimer. Cyclic voltammetry of this metallodendrimer shows recognition of both ATP2? and Pd2+. HAuCl4 is reduced much more slowly to gold nanoparticles by the nona(triazolyl-acetylferrocenyl dendrimer than by the nona(triazolylferrocenyl) dendrimer due to the shift of redox potential in the new heterodifunctional dendrimer compared to that of the parent ferrocenyl dendrimer. 相似文献
58.
Fabrice Rigaud Jean-Michel Portal Didier Nee Fabrice Argoud 《Microelectronics Reliability》2011,51(6):1136-1141
The objective of this paper is to present a mixed test structure designed to characterize yield losses due to hard defect and back-end process variation (PV) at die and wafer level. A brief overview of the structure, designed using a ST-Microelectronics’ 130 nm technology, is given. This structure is based on a SRAM memory array for detecting hard defects. Moreover each memory cell can be configured in the Ring Oscillator (RO) mode for back-end PV characterization. The structure is tested in both modes (SRAM, RO) using a single test flow. The test data analysis method is presented and applied to experimental results to confirm the ability of the structure to monitor PV and defect density. 相似文献
59.
Olivier Pras Davide Beneventi Didier Chaussy Paul Piette Sandra Tapin-Lingua 《Journal of Materials Science》2013,48(20):6911-6920
In this study, microfibrillated cellulose (MFC) and dendritic copper were used as binder and conductive phase for the elaboration of self-standing conductive films and coatings. A filtration technique was used to prepare MFC/Cu films from particle dispersions in water and ethanol. In aqueous slurries copper oxidized and an additional corona treatment or the use of zinc particles as sacrificial anode were necessary to obtain films with conductivities ranging from 70 to 2500 S m?1, respectively. In ethanol-based MFC/Cu slurries, copper was subjected to limited oxidation. However, the low packing density of conductive particles (below the percolation threshold) led to resistive films which, after densification by calendering, displayed extremely high conductivities, up to 70000 S m?1. Aqueous MFC/Cu slurries were successfully used for the deposition of conductive coatings on copy paper by Mayer rod coating and screen printing, which were subsequently treated by corona discharge and calendering. The obtained coatings displayed intermediate conductivity (i.e. 95 and 570 S m?1 for rod coating and screen printing, respectively), which can be further increased using zinc particles or ethanol-based formulations. 相似文献
60.
Virginie Dulong Renauld Forbice Eric Condamine Didier Le Cerf Luc Picton 《Polymer Bulletin》2011,67(3):455-466
Rheological and swelling properties of hydrogels based on pullulan crosslinked with sodium trimetaphosphate (STMP) are explained
according to various polymer and crosslinking agent concentrations using 31P-nuclear magnetic resonance study. This method has allowed determining the amount of all the species present in the medium
when varying both pullulan and STMP concentrations. We have clearly demonstrated with a good agreement by both 31P-NMR and rheology that a critical STMP concentration occurs which is function of pullulan concentration. This typical crosslinking
agent concentration delimitates the maximum of gel structure together with the minimum of swelling. 相似文献