利用α-甲基苯乙烯合成佳乐麝香的研究

介绍一种新的佳乐麝香合成方法，并就反应的参数对反应过程的影响进行了探讨。     

Algebraic operations in fuzzy object-oriented databases

The fuzzy object-oriented databases have been proposed to meet the need of dealing with fuzzy as well as complex objects. In this paper, we present a formal fuzzy object-oriented database model. Based on the semantic measure of fuzzy data, we first identify two kinds of fuzzy object redundancies, which are inclusion redundancy and equivalence redundancy, and then define three kinds of merging operation for redundancy removal. On the basis, we define some fuzzy algebraic operations for fuzzy classes and fuzzy objects. Finally, in the paper, we discuss fuzzy querying strategies and give the form of SQL-like fuzzy querying for the fuzzy object-oriented databases.     

LLDPE在振动剪切复合场中挤出成型的流变行为

利用振动剪切挤出装置研究了线性低密度聚乙烯(LLDPE)在振动与旋转剪切复合力场中挤出成型时的流变行为。结果表明:LLDPE熔体在复合力场中的表观黏度受振动频率、振幅、剪切速率等影响很大。在复合力场中存在使黏度降低最大的振动频率和剪切速率的最佳搭配。     

水热法制备锰锌铁氧体纳米晶

以水热法制备了粒径为20－40nm的锰锌铁氧体纳米晶，以XRD、SEM、磁强计等对产物做了表征，分析了影响锰锌铁氧体纳米晶的因素。结果表明，在T≥150℃,t≥5h条件下，均能得到阵锌铁氧体纳米晶粉末。T＝450℃时制备的纳米晶的磁强度最高；添加剂能改善水热体系的均匀性，使产物分布均匀、晶相单一、团聚少。     

Ionomer-silica hybrids via sol-gel reaction

Ionomer-silica hybrid materials were made from polyethylene-co-acrylic acid neutralized by a zinc salt (PI) and tetraethoxy silane (TEOS) via the sol-gel reaction. The effects of various experimental parameters such as solvents, H₂O/Si ratio and the amount of TEOS in the ionomer solution on the hybrid structure and properties were examined. The spectroscopic results show that solvents do not affect the structure of the hybrids, but influence the thermal properties. The hybrids made using highly polar solvent exhibit better thermal stability and dynamic mechanical properties at high TEOS contents. The amount of water used for hydrolysis and subsequent condensation play a significant role in the network formation. The varying amount of TEOS in solutions gives rise to different silica content of the hybrid. Above 50 wt%, the sample becomes opaque due to silica aggregation. The high ratio of H₂O/Si leads to phase separation during the reaction. Transparent hybrid materials can only be obtained when the ratio of H₂O/Si is below 5.     

电力工程自动化系统故障分析的方法

由于电力工程自动化系统的操作程序不断复杂化,故障的出现频率也随之增加。因此,必须建立完善的故障分析和解决方案,方能保证电力工程的正常、顺利推进。在此基础上,就电力工程自动化系统故障分析方法进行分析、探讨。     

税收电子数据分析在煤炭企业税源管理工作中的研究与实践

随着信息技术的不断发展,利用先进技术成果挖掘和提炼税收电子数据信息,深化数据分析,为税源管理特别是重点税源管理工作服务,已经成为了现代税收发展的潮流。它是信息管税、风险控制的重要组成部分,也是各级税务机关、专家和学者在税源管理方面面临的重要课题之一。以朔州市国家税务局煤炭企业税收管理信息系统建设为背景,研究税收数据分析在税源管理工作中作用和意义。     

基于OpenShift的非均衡数据完整性评估

设计并实现了一个基于OpenShift云计算环境的数据质量评估平台,对非均衡数据的完整性常规指标和专用指标具有评估功能。     

基于Nutch与元搜索引擎技术的高校网络舆情监测系统研究

针对高校网络舆情监测工作的不足,结合高校舆情信息的传播特点,提出了在校园网范围内基于Nutch搜索引擎技术进行信息检索,在互联网上采用元搜索引擎技术获取相关信息的舆情监测系统构建方案。采用关键词特征库匹配方式自动进行网络舆情监测,及时准确地发现网络舆情信息;探讨了高校对于网络舆情的监测、分析、引导和反馈等环节的处理方法,从而形成完善的应对机制。     

Adsorption of benzoic acid by CTAB exchanged montmorillonite

This paper reports the adsorption of benzoic acid from water on cetyl trimethylammonium exchanged montmorillonite (CTAB-montmorillonite). Important factors are the adsorbent concentration, ionic strength, equilibrium time and pH. The largest adsorption is at pH 9. The adsorption kinetics data fitted the pseudo-second-order equation. The adsorption isotherms at different pH were linear indicating a partition mechanism. Up to about 61% of the dissolved benzoic acid was adsorbed by CTAB-montmorillonite. These results indicate that CTAB-montmorillonite is a potential adsorbent for benzoic acid.