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101.
102.
Chunliang Li Theo Veldhuis Bart Reuvers Rafaël J Sablong Cor E Koning 《Polymer International》2020,69(1):24-30
Limonene‐derived polycarbonate‐based alkyd resins (ARs) have been prepared by copolymerization of limonene dioxide with CO2, catalysed by a β‐diiminate zinc–bis(trimethylsilyl)amido complex, and subsequent chemical modification with soybean oil fatty acids using triphenylethylphosphonium bromide as the catalyst. This quantitative partial modification was realized via epoxy–carboxylic acid chemistry, affording ARs with higher oil lengths, lower polydispersities and higher glass transition temperatures (Tg) in comparison to a conventional polyester AR based on phthalic acid, multifunctional polyol pentaerythritol and soybean fatty acid. The novel limonene polycarbonate AR and the conventional polyester AR were evaluated as coatings and both the physical drying (without the presence of the oxidative drying accelerator Borchi® Oxy Coat) and chemical curing (with Borchi® Oxy Coat) processes of these coatings were monitored by measuring the König hardness and complex modulus development with time. A better performance was obtained for the alkyd paint containing polycarbonates modified with fatty acids (FA‐PCs), which showed a faster chemical drying, a higher König hardness and a higher Tg in coating evaluation, demonstrating that the fully renewable FA‐PCs are promising resins for alkyd paint applications. © 2019 Society of Chemical Industry 相似文献
103.
104.
In this study, further analysis of the osmotic drying process was conducted to identify the optimum combination of parameters for drying rectangular alumina-gelatin beams. This study was designed to determine the effect of three variables related to the osmotic drying process (osmotic pressure, molecular weight, and immersion time) on the interaction between the liquid desiccant and the submerged alumina-gelatin samples. The water loss from the alumina-gelatin samples was positively correlated with the molecular weight, osmotic pressure, and immersion time. Up to 40% by weight of the initial water content was removed during the osmotic drying process. The samples also experienced solids gain due to the counterflow of solute from the liquid desiccant. The least amount of solids gain resulted from drying for the shortest immersion time at low osmotic pressure and high molecular weight. Evidence of possible interactions between variables was noted for the sintered density metric. Statistical methods were used to form regression equations for the measured responses (water loss, solids gain, bulk density). A verification experiment was conducted to compare the experimental outcomes to the predicted outcomes. The responses were simultaneously optimized to identify the combination of variable settings required to meet specified goals. In order to maximize water loss, minimize solids gain, and maximize bulk density, the ceramic-gelatin object should be immersed for approximately 60?min in an aqueous solution of 100,000?g/mol poly(ethylene oxide) at an osmotic pressure of 2.50?MPa. These values are valid for the range of parameter settings tested and the sample fabrication and drying methods used. 相似文献
105.
O.N. Kondrateva G.E. Nikiforova A.V. Tyurin M.A. Ryumin V.M. Gurevich A.P. Kritskaya K.S. Gavrichev 《Ceramics International》2018,44(15):18103-18107
The heat capacity of ytterbium orthovanadate was first measured by adiabatic calorimetry in the temperature range T?=?12.28–344.06?K. No obvious anomalies were observed on the curve obtained. The values of standard thermodynamic functions in the temperature range T?=?0–400 K were calculated. Based on low-temperature calorimetry data obtained, previously published data on the high-temperature heat capacity of ytterbium orthovanadate were corrected. The anomalous contribution to heat capacity for YbVO4 was compared with the data known for YbPO4. 相似文献
106.
107.
A. V. Kozlov I. A. Portnykh V. I. Pastukhov 《The Physics of Metals and Metallography》2018,119(4):396-401
The influence of the temperature gradient over the thickness of the cladding of a fuel element of a fast-neutron reactor on the migration of point defects formed in the cladding material due to neutron irradiation has been studied. It has been shown that, under the action of the temperature gradient, the flux of vacancies onto the inner surface of the cladding is higher than the flux of interstitial atoms, which leads to the formation of a specific concentration profile in the cladding with a vacancy-depleted zone near the inner surface. The experimental results on the spatial distribution of pores over the cladding thickness have been presented with which the data on the concentration profiles and vacancy fluxes have been compared. 相似文献
108.
The Raman spectrum of water adsorbed on a metallic silver surface reveals an anomalously large shift of the vibrational frequency as compared to that in the bulk. The results are compared to data reported by other researchers, and possible interpretations of the observed phenomenon are discussed. 相似文献
109.
S. A. Pul’nev A. I. Pryadko A. V. Chikiryaka V. I. Nikolaev 《Technical Physics Letters》2018,44(11):992-994
The behavior of a superelastic Cu?14.2% Al?4%Ni single crystal in the case of high reversible strains under a longitudinal bending force was investigated. The effect of strain confinement along the crystal length was revealed and studied. The highest reversible strains (up to 10%) were shown to be confined within the central part of the bent crystal. 相似文献
110.
X-ray diffraction analysis has been used to study the structure of the α-Zr matrix phase and the precipitation of β-Nb particles upon the annealing of a Zr–2.5% Nb deformed alloy. It has been found that the process of the precipitation of the strengthening β-Nb particles in the alloy is accompanied by the appearance of fields of elastic interphase deformations in the matrix α phase of the alloy due to the difference in the specific atomic volumes of the crystal structures of the matrix and precipitated phases. It has been shown experimentally that, as a result of the presence of interphase deformations in the alloy, the bcc crystal structure of the precipitating β-Nb particles undergoes monoclinic distortions. 相似文献