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941.
Zinc-containing nanoparticles stable in the liquid phase are synthesized by the radiation chemical reduction of zinc ions
in solutions of inverse micelles. The effects of the absorbed radiation dose and the size of the micelle water pool on the
spectral characteristics of samples are studied. The HPLC and electron microscopy results indicate that the composition of
nanoparticles synthesized depends on the salt nature.
Original Russian Text ? A.A. Revina, E.V. Oksentyuk, A.A. Fenin, 2007, published in Zashchita Metallov, 2007, Vol. 43, No.
6, pp. 613–618. 相似文献
942.
I.L. Lehr 《Corrosion Science》2007,49(5):2210-2225
This work is a study of the electropolymerisation of pyrrole onto iron electrodes in the presence of sodium bis(2-ethylhexyl) sulfosuccinate in a wide pH interval. The characterisation of the films was done using electrochemical techniques, SEM/EDX and IR spectroscopy. We show that it is possible to synthesise homogeneous, adherent and very compact films in the pH range between 7 and 12 under potentiodynamic, galvanostatic and potentiostatic conditions without substrate dissolution. The effects of various parameters on electrodeposition were investigated. The new procedure for the electrochemical synthesis of polypyrrole results in improved anticorrosion properties. The inhibition is proposed to be due to the sum of a repulsion of chloride ions because AOT remains entrapped in the polymer matrix and the presence of the iron oxide. Advantages of the use of surfactants in the electropolymerisation solution are discussed. 相似文献
943.
It is essential to automate the scanning path generation process to effectively implement the micro-stereolithography. However, a scanning path that is generated based only on a 3D CAD model introduces dimensional inaccuracies. In micro-stereolithography, the photopolymer solidification is affected by fabrication conditions, such as the optical properties (laser power, laser scanning speed, laser scanning pitch focusing condition, etc.) and material properties of the photopolymer. Thus, the photopolymer solidification phenomena must be considered when generating a laser scanning path. In this paper, a scanning path generation algorithm that uses 3D CAD data and considers the photopolymer solidification phenomena is proposed to improve the dimensional accuracy in micro-stereolithography. Multi-line photopolymer solidification experiments were performed for various laser scanning conditions to examine the photopolymer solidification phenomena. From these experiments, linear relations between the solidification length (width) and scanning length (width) were acquired and stored in a database. Subsequently, these data were utilized to compensate the scanning path of the laser beam. In addition, experiments for determining the layer thickness in the z-direction were performed and these results were also used in the scanning path generation algorithm.This research was supported by the Highly Advanced National Project (http://www.most.go.kr), which performs some of the National R&D Program, and sponsored by the Korean Ministry of Science and Technology under the contract project code M10214000116-02B1500-02010. 相似文献
944.
R. B. Vasil’ev S. G. Dorofeev M. N. Rumyantseva L. I. Ryabova A. M. Gas’kov 《Semiconductors》2006,40(1):104-107
The impedance spectra of nanocrystalline SnO2 ceramics with an average grain size d ranging from 3 to 43 nm were investigated in the frequency range 1–106 Hz at temperatures from 25 to 300°C in a dry oxygen atmosphere. Analysis of the experimental data by the graphoanalytical method made it possible to separate the contributions of grain bulk and grain boundaries to the conductivity. It is shown that the samples investigated can be arbitrarily divided into two groups with respect to the character of their conductivity. For the samples with an average grain size d < 25 nm, the charge transfer processes are almost completely determined by the grain boundaries. In samples with a larger grain size, the contribution of grain bulk to the conductivity is comparable with that of grain boundaries. 相似文献
945.
A. E. Barabanov 《Automation and Remote Control》2006,67(10):1547-1572
A new algorithm to solve the H ∞ control problem in the case of full information was presented. It combines the spectral and matrix methods. The polynomial Lur’e-Riccati operator was introduced. Parametrization of all solutions of the controlled plant equation by hidden variables was presented within the framework of the J.C. Willems behavioral approach. The kernel of the polynomial Lur’e-Riccati operator was decomposed into the direct sum of subspaces that are similar to the Jordan blocks. The saddle point of the linear-quadratic game which was found by V.A. Yakubovich in 1970 was shown to provide solution to the H ∞ control problem for a considerable class of controlled plants. 相似文献
946.
V. P. Vasilevskii M. N. Mikhailov A. A. Petrov M. I. Rozhdestvenskii Yu. M. Cherkashov 《Atomic Energy》2006,100(4):295-301
The basic stages and directions of upgrading and reconstruction of the power-generating units of nuclear power plants with
RBMK reactors over a period of 20 yr since the Chernobyl accident are reflected in this paper. The greatest amount of work
was done in 1986–1990 on all units with RBMK-1000 and-1500 reactors which were operating at that time in the USSR. The purpose
of the upgrade was to improve the neutron-physical characteristics of the reactor cores, increase the response speed of the
safety and control system and decrease the positive effect of water outflow from the cooling loop of this system, increase
the flow capacity of the systems performing emergency discharge of the steam-gas mixture from the reactor, and improve the
basic operating documentation.
The subsequent stages of the upgrading and reconstruction concerned mainly the first-generation power-generating units (Nos.
1 and 2 units of the Leningrad and Kursk nuclear power plants). These works were performed to make the power-generating units
conform to the requirements of the modern normative documents on safety and allow for the possibility of these units to remain
in operation after the nominal 30-yr service life has been exhausted.
__________
Translated from Atomnaya énergiya, Vol. 100, No. 4, pp. 312–320, April, 2006. 相似文献
947.
RM Martín‐Aranda E Ortega‐Cantero ML Rojas‐Cervantes MA Vicente‐Rodríguez MA Baares‐Muoz 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(2):234-238
α,β‐Unsaturated nitriles have been synthesized by Knoevenagel condensation of a carbonylic compound with malononitrile, assisted by sonochemical irradiation. Two alkaline‐promoted clays (Li+‐ and Cs+‐exchanged saponites) have been employed as catalysts. The influence of the carbonylic compound (benzaldehyde or cyclohexanone) and the use of a solvent on the catalytic activity have been studied. Remarkable increase in the conversion values has been found when the reaction is activated by ultrasound, as compared with the thermal activation. In this green, solvent‐free procedure, α,β‐unsaturated nitriles have been produced in very high yields (97%) when the Cs+‐saponite is used as catalyst. Copyright © 2004 Society of Chemical Industry 相似文献
948.
The effect of some additives on the equilibrium of valence forms of iron is investigated. It is demonstrated that tin and carbon more significantly than fluorine reduce iron. The redox potential of the glass matrix affects the equilibrium between difference valence forms of iron much less than additives correcting spectral characteristics of glass. 相似文献
949.
Against the background of increasing nutrient concentrations in Irish water bodies, this study set out to gain information on the potential of agricultural grassland to lose nutrients to water. Overland flow, flow from artificial subsurface drains and stream flow were gauged and sampled during heavy rainfall events. Dissolved reactive phosphorus (DRP), potassium (K), total ammonia (TA), and total oxidised nitrogen (TON) were measured in water samples. When the nutrient concentrations in water were examined in relation to the grassland management practices of the study catchments it emerged that soil P levels, the application of organic and inorganic fertilisers before heavy rainfall and the presence of grazing animals could all influence nutrient concentrations in surface and subsurface drainage water. Overall, the drainage characteristics of soil were found to have a considerable influence on the potential of land to lose nutrients to water. 相似文献
950.
Dixon J. Moran L. Rodriguez E. Domke R. 《Proceedings of the IEEE. Institute of Electrical and Electronics Engineers》2005,93(12):2144-2164
This paper presents an overview of the state of the art in reactive power compensation technologies. The principles of operation, design characteristics and application examples of Var compensators implemented with thyristors and self-commutated converters are presented. Static Var generators are used to improve voltage regulation, stability, and power factor in ac transmission and distribution systems. Examples obtained from relevant applications describing the use of reactive power compensators implemented with new static Var technologies are also described. 相似文献