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11.
M. Del C. Ruiz J. A. González J. B. Rivarola 《Metallurgical and Materials Transactions B》2004,35(3):439-448
The mechanism and kinetics of β-Ta2O5 chlorination, mixed with sucrose carbon, have been studied by a thermogravimetric technique. The investigated temperature
range was 500 °C to 850 °C. The reactants and reaction residues were analyzed by scanning electronic microscopy (SEM), X-ray
diffraction (XRD), and Brunauer-Emmett-Teller method for surface area (BET). The effect of various experimental parameters
was studied, such as carbon percentage, temperature, chlorine partial pressure, and flow, use of the multiple sample method,
and carbon previous oxidation. The carbon percentage and previous treatment have an effect on the system reactivity. The temperature
has a marked effect on the reaction rate. In the 500 °C to 600 °C temperature interval, the apparent activation energy is
144 kJ/mol of oxide, while at higher temperatures, the activation energy decreases. With high chorine partial pressures, the
order of reaction is near zero. The kinetic contractile plate model, X=kt, considering carbon oxidation as the controlling stage, is the one with the best fit to the experimental data. A probable
mechanism for the carbochlorination of β-Ta2O5 is proposed: (1) activation of chlorine on the carbon surface, (2) chlorination of Ta2O5, (3) oxidation of carbon, and (4) recrystallization of β-Ta2O5. 相似文献
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M Loscertales Abril F Jaldo Alba E Díaz Lucas E Narbona López A Ruiz Extremera E Ocete Hita JA Molina Font 《Canadian Metallurgical Quarterly》1993,39(4):339-342
Four patients who complained of symptoms and signs compatible with biliary tract disease and in whom the diagnosis of gallbladder (three cases) and common bile duct ascariasis (one case) was made sonographically are reported. In two patients with gallbladder ascariasis, cholecystectomy corroborated the presence of the round-worms, and was curative. The third patient was a pregnant woman (32nd gestational week) who took piperazine citrate, and a second sonogram performed 29 days later was completely normal. The fourth patient with common bile duct ascariasis underwent choledochotomy with extraction of one ascaris lumbricoides from the common duct, and a T tube was left in place for 15 days. All patients received antiparasitics and had a favorable outcome. Ultrasonography is an important noninvasive diagnostic procedure in the work-up of these patients, who usually describe a clinical picture suggesting gallstone disease: this is especially true in the presence of pregnancy. 相似文献
17.
X. Ruiz 《Microgravity science and technology》2006,18(3-4):51-56
The binomial single g-pulses — dopant segregation in a generic virtual µg Bridgman growth arrangement is discussed here with the help of a time dependent two-dimensional scheme. To attain this objective, the so-called solid composition drop distribution has been previously defined enabling a global two-dimensional information of the segregation impact in each virtually grown crystal. Based on this parameter it has been concluded that, at equal g-dose, solid segregation is independent on the shape of the single external pulse and that, for single g-pulses of equal g-dose, compositional variations are practically independent on the activity time but depend on the crystal growth rate. Finally, taking into account all these set of results, the pertinence of the g-dose as the only self-consistent parameter to describe the segregation impact has been discussed. 相似文献
18.
Extending the power line LAN up to the neighborhood transformer 总被引:1,自引:0,他引:1
Abad J. Badenes A. Blasco J. Carreras J. Dominguez V. Gomez C. Iranzo S. Riveiro J.C. Ruiz D. Torres L.M. Comabella J. 《Communications Magazine, IEEE》2003,41(4):64-70
This article reports on the performance of audio, video, multimedia, and other high-data-rate in-home networking applications. The article starts by describing the problems encountered in power line communication channels in terms of frequency response and noise characteristics, and explains how in-home power line LANs can be extended to the neighborhood transformer. OFDM physical layers providing speeds of 45 Mb/s and 200 Mb/s as well as QoS and security are introduced. Finally, the results of large tests involving several thousands of nodes are described. 相似文献
19.
Rafael Gallego Lucia Comino Alberto Ruiz‐Cabello 《International journal for numerical methods in engineering》2006,66(12):1913-1933
In this paper, the material constant sensitivity boundary integral equation is presented, and its numerical solution proposed, based on boundary element techniques. The formulation deals with plane problems with general rectilinear anisotropy. Expressions for the computation of sensitivities for displacements, tractions, strains and stresses are derived, both for boundary and interior points. The sensitivities can be computed with respect to the bulk material properties or to the properties of part of the domain (inclusions, coatings, etc.). To assess the accuracy of the proposed approach, the computed results are compared to analytical ones derived from exact solutions obtained by complex potential theory, when possible, or finite difference derivatives otherwise. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
20.
The kinetics of the chlorination reaction of molybdenum trioxide with gaseous carbon tetrachloride has been studied at temperatures between 713 and 753 K. The effects of temperature, reaction time, residence time and gaseous reactant concentration on conversion were studied throughout the reaction. In all cases, there was an increase in conversion when the above operating variables were increased. The kinetic model proposed is consistent with and correlates the experimental data. In the range studied for the different variables, the step that controls the rate of reaction is the surface chemical reaction. Values of the rate constant and the activation energy were estimated. 相似文献