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1.
Hydrophilic coatings based on 3‐glicidoxy propyl trimethoxy silane (GPTMS) and polyethylene glycol (PEG) were prepared with the incorporation of tetramethoxysilane (TMOS) and silica nanoparticle colloidal suspension by a sol–gel process. Characterization of the coatings has been performed by Fourier Transform Infrared (FTIR) and Attenuated Total Reflectance Infrared (ATR‐IR) techniques. Morphological properties were characterized by Scanning Electron Microscopy (SEM). The distribution of Si atoms in the hybrid system was obtained by Si mapping. The particle size in sol solution of the coating was measured by light scattering analyzer. Optical properties were characterized by using UV–vis spectrophotometer. The hydrophilicity of the coating was determined by contact angle measurements, and also the results have been confirmed by surface energy and water uptake investigations. The obtained results indicate that the surfactants affected the contact angles remarkably but did not change the transparency. It has been found that applying silica nano particles leads to coatings with different properties than those using TMOS, while siloxane contents were the same in these two set of coatings. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 5322–5329, 2006 相似文献
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Salah Bouktif Faheem Ahmed Issa Khalil Giuliano Antoniol 《Information and Software Technology》2010,52(12):1298-1311
Context:How can quality of software systems be predicted before deployment? In attempting to answer this question, prediction models are advocated in several studies. The performance of such models drops dramatically, with very low accuracy, when they are used in new software development environments or in new circumstances.ObjectiveThe main objective of this work is to circumvent the model generalizability problem. We propose a new approach that substitutes traditional ways of building prediction models which use historical data and machine learning techniques.MethodIn this paper, existing models are decision trees built to predict module fault-proneness within the NASA Critical Mission Software. A genetic algorithm is developed to combine and adapt expertise extracted from existing models in order to derive a “composite” model that performs accurately in a given context of software development. Experimental evaluation of the approach is carried out in three different software development circumstances.ResultsThe results show that derived prediction models work more accurately not only for a particular state of a software organization but also for evolving and modified ones.ConclusionOur approach is considered suitable for software data nature and at the same time superior to model selection and data combination approaches. It is then concluded that learning from existing software models (i.e., software expertise) has two immediate advantages; circumventing model generalizability and alleviating the lack of data in software-engineering. 相似文献
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M. Mumtaz Nawazish A. Khan S. M. Hasnain Faheem Ashraf 《Journal of Superconductivity and Novel Magnetism》2012,25(7):2291-2295
Superconductivity has been improved by partial substitution of slightly higher electronegative (M=Bi, Hg) elements at Tl sites in (Cu0.5Tl0.5?x M x )Ba2O4??? (x=0,0.25) charge reservoir layer of (Cu0.5Tl0.5?x M x )Ba2Ca2Cu3O10??? superconductor. These samples were characterized by X-ray diffractometry, dc-resistivity, ac-susceptibility, FTIR absorption spectroscopy, and fluctuation-induced conductivity (FIC) analysis. The FIC analysis has been carried out in the light of Aslamasov?CLarkin (AL) theory on the resistivity versus temperature curves of (Cu0.5Tl0.5?x M x )Ba2Ca2Cu3O10??? superconductor. The microscopic parameters such as cross-over temperature (T o ), zero-temperature coherence length ?? c (0), inter-layer coupling (J), and critical exponents (?? 2D and ?? 3D) have been determined from FIC analysis of these samples and tried to correlate them to the superconductivity order parameters. A?direct correlation between the cross-over temperatures (T o ) and zero resistivity critical temperature {T c (R=0)} and carrier concentration in these samples has been observed. The improvement in T c (R=0) and the shift of 3D AL region to higher temperature values with the doping of Bi and Hg have also been observed. 相似文献
5.
Yasir Ali Elsheikh Zakaria Man Faheem Hassan Akhtar 《Korean Journal of Chemical Engineering》2014,31(3):431-435
A study was undertaken to prepare biodiesel via two-step process using ionic liquid as first step catalyst due to the unsuitability of using the straight alkaline-catalyzed transesterification of high FFA presented in crude palm oil (CPO). In the first step, esterification of the FFA presented in the CPO was carried out using butylimidazolium hydrogen sulfate (BIMHSO4), in which the acid value was reduced from 6.93 to 1.02mg KOH/g and then, KOH-catalyzed transesterification was applied. The conversion rate of FFA attained 85.3% when 4.8 wt% of BIMHSO4 was applied to the reaction system containing methanol to CPO ratio of 12: 1 reacted at 170 °C for 150min. The final yield in 97.3% revealed that the process proposed in this study could lead to an excellent biodiesel meeting the ASTM requirements. Furthermore, this new two-step catalysis process could solve the old conventional catalysis process drawbacks. 相似文献
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Faheem Ullah Fatima Javed Muhammad Bisyrul Hafi Othman Zulkifli Ahmad 《国际聚合物材料杂志》2017,66(16):824-834
There is an urgent need to treat diabetes, and therefore, this work reports on a chitosan-built hydrogel functionalized by a glucose sensing moiety, which simulates pancreatic activity. The effect of external stimuli on various internal properties was investigated to establish the action of the hydrogel. The model drugs, fluorescein (D1) and rhodamine (D2), with a diol architecture, were investigated spectroscopically with 75.94% loading and 65.63% release. Consequently, a ligand to glucose ratio of 2:1 in comparison with a ligand to model drug ratio of 1:1 was addressed. The system was expected to lead to findings on applications for the self-controlled release of insulin in response to blood glucose levels. 相似文献
7.
Noor-Ul-Ain Babar Yasir Faheem Joya Hassan Khalil Fayyaz Hussain Khurram Saleem Joya 《International Journal of Hydrogen Energy》2021,46(11):7885-7902
Developing only Fe derived bifunctional overall water splitting electrocatalyst both for oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) while performing at low onset overpotential and with high catalytic stability is a rare instance. We present here the first demonstration of unique iron-oxide nanobeads (FeOx-NBs) based electrocatalyst executing both OER and HER with high activity. Thin-film electrocatalytic FeOx-NBs assembly is surface grown via simple spray coating (SC). The unique SC/FeOx-NBs propels OER initiating water oxidation just at 1.49 VRHE (η = 260 mV) that is the lowest observable onset potential for OER on simple Fe-oxide based catalytic films reported so far. Catalyst also reveals decently high HER activity and competent overall water splitting performance in the FeOx-NBs two-electrode system as well. Catalyst also presents stable kinetics, with promising high electrochemically active surface area (ECSA) of 1765 cm2, notable Tafel slopes of just 54 mV dec1? (OER) and 85 mV dec1? (HER), high exchange current density of 1.10 mA cm2? (OER), 0.58 mA cm2? (HER) and TOF of 74.29s1?@1.58VRHE, 262s1?@1.62VRHE (OER) and 82.5s1?@-0.45VRHE, 681s1?@-0.56VRHE (HER). 相似文献
8.
M. Shamshi Hassan Touseef Amna Faheem A. Sheikh Salem S. Al-Deyab Kyung Eun Choi I.H. Hwang Myung-Seob Khil 《Ceramics International》2013
The objective of this study was to develop a new class of bimetallic ZnO/Ag embedded polyurethane multi-functional nanocomposite by a straightforward approach. Bimetallic nanomaterials, composed of two unlike metal elements, are of greater interest than the monometallic materials because of their improved characteristics. In the present study the bimetallic composite was prepared using sol–gel via the facile electrospinning technique. The utilized sol–gel was composed of zinc oxide, silver and poly(urethane). The physicochemical properties of as-spun composite mats were determined by X-ray diffraction pattern, field emission scanning electron microscopy, energy dispersive X-ray spectroscopy and transmission electron microscopy. The antibacterial activity was tested using Escherichia coli as model organism. The antibacterial test showed that ZnO:Ag/polyurethane composite possesses superior antimicrobial activity than pristine PU and ZnO/PU hybrids. Furthermore, our results illustrate that the synergistic effect of ZnO and Ag resulted in the advanced antimicrobial action of bimetallic ZnO/Ag composite mat. The viability and proliferation properties of NIH 3T3 mouse fibroblast cells on the ZnO:Ag/polyurethane composite nanofibers were analyzed by in vitro cell compatibility test. Our results indicated the non-cytotoxic behavior of bimetallic ZnO:Ag/polyurethane nanofibers towards the fibroblast cell culture. In summary, novel ZnO:Ag/polyurethane composite nanofibers which possess large surface to volume ratio with excellent antimicrobial activity were fabricated. The unique combination of ZnO and Ag nanoparticles displayed potent bactericidal effect due to a synergism. Hence the electrospun bimetallic composite indicates the huge potential in water filtration, clinical and biomedical applications. 相似文献
9.
Roqia Ashraf Tariq Maqbool Mushtaq A. Beigh Arvind H. Jadhav Hasham S. Sofi Faheem A. Sheikh 《应用聚合物科学杂志》2021,138(25):50594
There is an extensive possibility of improving characteristics of fibers used in hard tissue engineering, being hydrophobic and less osteoconductive, resulting in the dynamic growth of new tissues. The current work focuses on the fabrication of nanofibers incorporated with titanium dioxide (TiO2) ''as osteoconductive'' and silver (Ag) ''as self-healing'' nanoparticles (NPs). The incorporation of AgNO3 by in situ method not only helped to impart the antibacterial activity but also changed the contact angle from 81 ± 03° in the case of pristine nanofibers to 74 ± 03°, 61 ± 03°, 50 ± 08°, and 39 ± 1.1°, in the composite scaffolds containing 0.01, 0.03, 0.05, and 0.07 M of Ag salts. The incubation in simulated body fluid at 37°C to induce mineralization on nanofiber scaffolds indicated Ca and P crystals' formation. The antibacterial activity showed significantly more toxicity toward E. coli (8.3 ± 0.9 mm) than S. aureus (1.2 ± 0.1 mm). Biocompatibility studies using MTT assay on the pre-osteoblasts showed that both TiO2 and Ag NPs present in the nanofibers are non-toxic to the bone-like cells. However, results show that a higher concentration of Ag NPs (i.e., 0.07 M) is toxic to cells growing. Finally, all the results suggest that the nanofiber scaffolds have considerable scope for future bone tissue engineering materials. 相似文献
10.
Adil Farooq Arfa Iqbal Nosheen Fatima Rana Misha Fatima Tuba Maryam Farhat Batool Zahra Rehman Farid Menaa Shabia Azhar Afrah Nawaz Faheem Amin Zuhair M. Mohammedsaleh Salma Saleh Alrdahe 《International journal of molecular sciences》2022,23(6)
Chronic liver disease (CLD) is a global threat to the human population, with manifestations resulting from alcohol-related liver disease (ALD) and non-alcohol fatty liver disease (NAFLD). NAFLD, if not treated, may progress to non-alcoholic steatohepatitis (NASH). Furthermore, inflammation leads to liver fibrosis, cirrhosis, and hepatocellular carcinoma. Vitexin, a natural flavonoid, has been recently reported for inhibiting NAFLD. It is a lipogenesis inhibitor and activates lipolysis and fatty acid oxidation. In addition, owing to its antioxidant properties, it appeared as a hepatoprotective candidate. However, it exhibits low bioavailability and low efficacy due to its hydrophobic nature. A novel rat model for liver cirrhosis was developed by CCL4/Urethane co-administration. Vitexin encapsulated liposomes were synthesized by the ‘thin-film hydration’ method. Polyethylene glycol (PEG) was coated on liposomes to enhance stability and stealth effect. The diseased rats were then treated with vitexin and PEGylated vitexin liposomes, administered intravenously and orally. Results ascertained the liposomal encapsulation of vitexin and subsequent PEG coating to be a substantial strategy for treating liver cirrhosis through oral drug delivery. 相似文献