甲氧胺盐酸盐的含量测定方法

提出了以酚酞为指示剂，氢氧化钠为滴定剂测定甲氧胺盐酸盐含量的方法。测定了甲氧胺盐酸盐的离解常数Ka，考察了干扰因素对测定的影响。结果表明，干扰物质NH4Cl在样品中的含量小于5％不影响测定。该方法具有简便、快速，准确等特点,测定了数批样品结果较满意。     

混炼硅橡胶的配合技术(四)

介绍了几种胶辊用混炼硅橡胶的配制,包括低硬度胶辊用混炼硅橡胶、低环硅氧烷含量的胶辊用混炼硅橡胶、送纸胶辊用混炼硅橡胶及工业胶辊用混炼硅橡胶的配制。     

促进我国硫铁矿制酸的发展

我国硫磺制酸原料主要依赖进口,大量进口硫磺已经影响到世界硫磺的供需关系,硫磺价格居高不下.硫铁矿是我国自有资源,可保证长期、稳定的供应,对我国硫酸工业的稳定和安全具有重要作用,我国发展硫铁矿制酸有其必要性.硫铁矿制酸实现大型化;采用高品位硫铁矿制酸,有效利用铁资源和热能;实现清洁生产,减少废水排放、尾气二氧化硫排放及综合利用废热,是发展方向.抓住硫酸需求增加的机遇,采用先进技术发展硫铁矿制酸,硫铁矿制酸一定会有良好的发展前景.     

辣椒疫病菌对氟吗啉的抗药性研究

为了评估氟吗啉的未来抗性风险，以辣椒疫病菌为靶标，通过室内抗性菌株的驯化、筛选，以及紫外线诱变等方法，初步探索了辣椒疫病菌对氟吗啉的抗性情况。结果表明：抗性菌株对氟吗啉的抗性倍数较低，在3.45～11．33，生长速率明显低于野生敏感菌株。由此可见辣椒疫病菌对氟吗啉的抗性风险可能较低。     

悬浮液进样-火焰原子吸收光谱法测定茶叶中的微量铬

将茶叶悬浮于琼脂胶体中制成悬浮液 ,直接喷入空气 -乙炔火焰 ,用火焰原子吸收光谱法测定茶叶中的微量铬 ,方法简便、快速、灵敏度和精密度高、测定结果与用灰化法处理样品一致 ,检验表明 ,两种样品前处理方法之间无显著性差异。相对标准偏差为 3.4 %～ 6 .1% ,加标回收率为 95 .7%～ 10 3.8 %。     

对叔丁基苄胺的合成研究

摘要选择Delepine反应法的路线合成对叔丁基苄胺，并对反应投料比、反应温度及酸化后的反应时间进行了优化试验，得到了较好的反应条件：反应温度为40℃，对叔丁基苄氯与乌洛托品投料比为1：1；加入酸和醇后的保温时间为2h，从而使反应收率稳定在90％以上，含量达到95％。     

Preparation of micro-patterned surfaces of Si-N-O films and their influence on adhesion behavior of endothelial cells

Microgrooves were prepared on Si(100) surface by photolithography and wet etching.Subsequently,Si-N-O films were deposited on the microgrooves by unbalanced magnetron sputtering(UBMS) and micro-patterned surfaces of Si-N-O films were obtained.The size of the micropatterns was measured by surface profilometer.The chemical composition of Si-N-O films were characterized by X-ray photoelectron spectrometry(XPS) and the wettability of the micropatterned surfaces was evaluated by contact angle measurement.The beh...     

Preparation,characterization and salt-resistance of a coal based super absorbent composite

Potassium humate was extracted from brown coal.A novel super absorbent composite,poly (acrylic acid-co-acrylamide)/potassium humate (PAA-AM/KHA),was prepared by graft polymerization of acrylic acid,acrylamide and coal based potassium humate using N,N'-methylenebisacrylamide as a crosslinker and potassium peroxydisulfate as an initiator.The effects of reaction temperature,degree of neutralization of the poly (acrylic acid) and the amounts of crosslinker,initiator and potassium humate were investigated.Salt resistance tests were also carried out.The composite prepared under optimal conditions had a potassium humate content of 10% and exhibited a water absorption of 770 g/g in distilled water,and 349,286 and 41 g/g in 0.5 mol/L KC1,MgCl2 and AlCl3 solutions respectively.The results indicate that the salt resistance of PAA-AM/KHA was superior to that of poly (acrylic acid-co-acrylamide) because of the collaborative effect of functional groups of the coal based potassium humate.The PAA-AM/KHA micro powder was characterized by IR spectroscopy and the micrographic surface was characterized by scanning electron microscopy.Introduction of potassium humate into the poly (acrylic acid-co-acrylamide) structure creates a composite more suitable for use as a water-managing material in the renewal of arid and desert environments.The salt resisting property of the composite is improved,production costs are reduced and the growth stimulant effect is still present.     

基于Java3D的虚拟雕塑系统的设计与实现

针对雕塑作品构思和设计阶段的需求,开发了一个基于Java3D中索引曲面造型方法的虚拟雕塑系统.可以用简单的交互操作,模仿雕塑的手工过程,修改形体几何信息.通过对变形结果的展现、比较和修改,优化设计效果,给出修改形体拓扑结构的实现方法,丰富了虚拟雕塑操作的种类,提高了模型的变形能力.该系统操作方便,对用户使用的技术水平要求低,与专业雕塑人员习惯操作比较吻合,并可推广到工艺品、玩具、景观的方案设计等多个领域.     

基于Morlet小波变换和改进遗传算法的动态识别

如何合理地识别大型复杂结构的动力参数一直是工程领域关心的问题.为此,以Morlet小波变换和采用单亲遗传算子的改进遗传算法为基础,构造一结构动态参数识别模型.并且以C++为平台,通过计算机内部命令调用ANSYS等软件,实现识别模型的程序化.通过模拟算例计算,计算结果与理论值一致.同时,结合一水电站厂房现场振动试验,对该大型结构进行动态参数识别,识别结果与工程经验值基本吻合.