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排序方式: 共有4093条查询结果,搜索用时 15 毫秒
81.
Celso M. Ogawa Kurt Faltin Fernando A. Maeda Cristina L. F. Ortolani Renata O. Guar Cristiane A. B. Cardoso Andr L. F. Costa 《Microscopy research and technique》2020,83(8):928-936
This study was undertaken to assess in vivo the corrosion in two commercial nickel–titanium (NiTi) orthodontic archwires removed from the oral cavity of patients using fluoride mouthwashes. Five volunteers took part in this study on the corrosion behavior of two brands of NiTi archwires (3M and AO (brand of archwire)) during use of two mouthwashes with neutral sodium fluoride 1.1%, one with acidulated fluoride 1.1%, and one with placebo and a control group. Each patient used one mouthwash in three different periods of time for 1 min a day for 30 days. The archwires were assessed with scanning electron microscopy and atomic force microscopy for qualitative and quantitative analysis. The values obtained with atomic force microscopy (AFM) were submitted to normality test, two‐way analysis of variance, and Tukey's test at a significance level of 5%. The AFM images showed a gradual qualitative increase in the roughness of both types of wire between the treatments: control < placebo < neutral fluoride < acidulated fluoride. The arithmetic average of the roughness and root mean square of the roughness were similar. As for 3M archwires, only the acidulated fluoride group differed statistically from the others. As for AO archwires, the control and placebo groups did not differ from each other, but differed from the other fluoride treatments. The group using neutral fluoride also differed significantly from the acidulated fluoride group. 3M archwires were not affected by daily oral challenges. AO archwires were not affected by daily oral challenges either; their association with fluoride, either neutral or acidulated, increased their roughness. 相似文献
82.
Antônio Alisson Alencar Freitas Fernando Lessa Tofoli Edilson Mineiro Sá Junior Sergio Daher Fernando Luiz Marcelo Antunes 《International Journal of Electronics》2016,103(5):898-912
A high voltage step-up nonisolated DC–DC converter based on coupled inductors suitable to photovoltaic (PV) systems applications is proposed in this paper. Considering that numerous approaches exist to extend the voltage conversion ratio of DC–DC converters that do not use transformers, a detailed comparison is also presented among the proposed converter and other popular topologies such as the conventional boost converter and the quadratic boost converter. The qualitative analysis of the coupled-inductor-based topology is developed so that a design procedure can be obtained, from which an experimental prototype is implemented to validate the theoretical assumptions. 相似文献
83.
Matilde Ortiz-Gonzalez Ignacio Prez-Victoria Inmaculada Ramirez-Macias Nuria de Pedro Angel Linde-Rodriguez Víctor Gonzlez-Menndez Victoria Sanchez-Martin Jesús Martín Ana Soriano-Lerma Olga Genilloud Virginia Perez-Carrasco Francisca Vicente Jos Maceira Carlos A. Rodrígues-Poveda Jos María Navarro-Marí Fernando Reyes Miguel Soriano Jose A. Garcia-Salcedo 《International journal of molecular sciences》2022,23(11)
84.
Marina Paiva Abuafy Regina Celia Galvao Frem Giulia Polinario Fernando Rogerio Pavan Heng Zhao Angelika Mielcarek Cedric Boissiere Christian Serre Leila Aparecida Chiavacci 《International journal of molecular sciences》2022,23(14)
Nanoparticles of metal–organic frameworks (MOF NPs) are crystalline hybrid micro- or mesoporous nanomaterials that show great promise in biomedicine due to their significant drug loading ability and controlled release. Herein, we develop porous capsules from aggregate of nanoparticles of the iron carboxylate MIL-100(Fe) through a low-temperature spray-drying route. This enables the concomitant one-pot encapsulation of high loading of an antitumor drug, methotrexate, within the pores of the MOF NPs, and the collagenase enzyme (COL), inside the inter-particular mesoporous cavities, upon the formation of the capsule, enhancing tumor treatment. This association provides better control of the release of the active moieties, MTX and collagenase, in simulated body fluid conditions in comparison with the bare MOF NPs. In addition, the loaded MIL-100 capsules present, against the A-375 cancer cell line, selective toxicity nine times higher than for the normal HaCaT cells, suggesting that MTX@COL@MIL-100 capsules may have potential application in the selective treatment of cancer cells. We highlight that an appropriate level of collagenase activity remained after encapsulation using the spray dryer equipment. Therefore, this work describes a novel application of MOF-based capsules as a dual drug delivery system for cancer treatment. 相似文献
85.
Soroosh Sharifi‐Asl Fernando A. Soto Tara Foroozan Mohammad Asadi Yifei Yuan Ramasubramonian Deivanayagam Ramin Rojaee Boao Song Xuanxuan Bi Khalil Amine Jun Lu Amin Salehi‐khojin Perla B. Balbuena Reza Shahbazian‐Yassar 《Advanced functional materials》2019,29(23)
LiCoO2 is a prime example of widely used cathodes that suffer from the structural/thermal instability issues that lead to the release of their lattice oxygen under nonequilibrium conditions and safety concerns in Li‐ion batteries. Here, it is shown that an atomically thin layer of reduced graphene oxide can suppress oxygen release from LixCoO2 particles and improve their structural stability. Electrochemical cycling, differential electrochemical mass spectroscopy, differential scanning calorimetry, and in situ heating transmission electron microscopy are performed to characterize the effectiveness of the graphene‐coating on the abusive tolerance of LixCoO2. Electrochemical cycling mass spectroscopy results suggest that oxygen release is hindered at high cutoff voltage cycling when the cathode is coated with reduced graphene oxide. Thermal analysis, in situ heating transmission electron microscopy, and electron energy loss spectroscopy results show that the reduction of Co species from the graphene‐coated samples is delayed when compared with bare cathodes. Finally, density functional theory and ab initio molecular dynamics calculations show that the rGO layers could suppress O2 formation more effectively due to the strong C? Ocathode bond formation at the interface of rGO/LCO where low coordination oxygens exist. This investigation uncovers a reliable approach for hindering the oxygen release reaction and improving the thermal stability of battery cathodes. 相似文献
86.
87.
88.
Fernando Fraternali Matteo Negri Michael Ortiz 《International Journal of Fracture》2010,166(1-2):3-11
Free discontinuity problems arising in the variational theory for fracture mechanics are considered. A Γ -convergence proof for an r-adaptive 3D finite element discretization is given in the case of a brittle material. The optimal displacement field, crack pattern and mesh geometry are obtained through a variational procedure that encompasses both mechanical and configurational forces. Possible extensions to cohesive fracture and quasi-static evolutions are discussed. 相似文献
89.
Alexandre Antunes Ribeiro Rodrigo Fernando Costa Marques Antônio Carlos Guastaldi João Sinézio de Carvalho Campos 《Journal of Materials Science》2009,44(15):4056-4061
Many techniques have been used to coat metallic substrate with bioceramics. The aim of this study was to study the physical-chemical
characteristics of polyvinylidene fluoride (α-PVDF)/hydroxyapatite (HA) composite coating, obtained by casting method, on
commercially pure titanium (α-CP Ti) substrate surface modified by laser beam irradiation. The preparation of coating was
done for mixing α-PVDF pellets shape dissolved in dimethylacetamide (DMA) with HA/DMA emulsion. The mixture was poured onto
the α-CP Ti sample and left to dry in an oven. CP Ti plates were coated with α-PVDF/HA composite film, in proportions of 100/00
and 60/40 in weight, and characterized by particle size analysis, scanning electron microscopy, energy dispersive spectroscopy
(EDS), X-ray diffractometry, thickness measurement and contact angle. Uniform coating with a small thickness variation along
the coated surface was successfully obtained. 相似文献
90.
Oil‐spill cleanup: The influence of acetylated curaua fibers on the oil‐removal capability of magnetic composites 下载免费PDF全文
Eldho Elias Raphael Costa Fernanda Marques Geiza Oliveira Qipeng Guo Sabu Thomas Fernando G. Souza Jr 《应用聚合物科学杂志》2015,132(13)
A magnetic resin based on cardanol, furfural, and curaua fibers was prepared and characterized. The material could be used in oil‐spill cleanup processes, because of its aromatic/aliphatic balance. The resin was prepared through bulk polycondensation of cardanol and furfural in the presence of curaua fibers and maghemite nanoparticles. Hydrophobicity of the curaua fibers was improved by acetylation, increasing the oil‐absorbing capability of the composites. The obtained magnetic composites were studied by Fourier‐transform infrared spectroscopy, X‐ray diffraction, and thermogravimetric analysis. Degree of cure, magnetic force, and oil‐removal capability tests were also performed. The results show that the composites possess an elevated cure degree in addition to a considerable magnetic force. The materials exhibit a good oil removal capability in the presence of a magnetic field, which is improved by the use of acetylated curaua. In the best case, the composite filled with maghemite and curaua can remove 12 parts of oil from water. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 41732. 相似文献