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31.
32.
Recently, the interest in olive leaf has increased due to its high phenolic content. It has a high potential for industrial exploitation in food industry and the main process in olive leaf treatment is drying. Drying affects the product quality and is an energy-intensive process, so the use of heat pumps in drying processes that have low operating cost has attracted the attention of the investigators. In this study, response surface methodology was used to optimize operating conditions of drying of olive leaves in a pilot-scale heat pump conveyor dryer. The independent variables were air temperature, air velocity, and process time, and the responses were total phenolic content and antioxidant activity loss, final moisture content, and exergetic efficiency. Optimum operating conditions were found to be temperature of 53.43°C, air velocity of 0.64 m/s, process time of 288.32 min. At this optimum point, total phenolic content loss, total antioxidant activity loss, final moisture content, and exergetic efficiency were found to be 9.77%, 44.25%, 6.0% (w.b.), and 69.55%, respectively. 相似文献
33.
Extraction of Ti(IV) from its aqueous hydrochloric acid solutions into organic Alamine 336-m-xylene systems was investigated. Extraction experiments were conducted with three different initial metal concentrations of 1, 3, and 6 mg/mL, each at three acidic molarities of 1, 5, and 10 M. It was observed that the extractability of Ti(IV) increases with increasing acidic molarities. Alamine 336 diluted with m-xylene was found to be a suitable extractant for Ti(IV) across this acidic range. In parallel, a mathematical model was developed to correlate metal extractability and Alamine 336 volume content. Optimal Alamine 336 contents were estimated for single-stage extraction. 相似文献
34.
Fatma Nur Arslan Huseyin Kara Hamide Filiz Ayyildiz Mustafa Topkafa Ismail Tarhan Adnan Kenar 《Journal of the American Oil Chemists' Society》2013,90(8):1179-1193
The main goal of the present study was (i) to determine the formation of degradation products in cottonseed oil (CSO) blends during deep frying process by adsorption and high performance size exclusion chromatography techniques and (ii) to evaluate the impacts of food additives on total polar (TPC) and polymeric compound (PTAG) formation using a chemometric approach. In order to prepare the frying CSO blends; ascorbic palmitate, mixed tocopherols, dimethylpolysiloxane, lecithin and sesame oils were used as additives. To determine the real impacts of additives, a quarter-fraction factorial experimental design with two levels and five factors was used. The changes in TPC and PTAG data were carefully evaluated during 10 h of frying at 170 ± 5 °C with normal distribution (ND) graphs and analyzed using a one-way analysis of variance (ANOVA), followed by Tukey’s Post-hoc test (α = 0.05). The results indicated that the increasing values for TPC and PTAG during the frying processes for all blends, TPC and PTAG contents reached maximum levels of 16.37 and 6.01 % respectively, which are below the limit values stated by official authorities for the quality assessment of frying oils. The ANOVA test results were in good agreement with ND graphs and data indicated that the impact of mixed tocopherols was significant for TPC formation, meanwhile the impact of lecithin and ascorbic palmitate × dimethylpolysiloxane were significant for PTAG formation. Thus, the present study should be considered to be a very useful guide for developing new frying oil formulations based on CSO by using food additives. 相似文献
35.
Macroscopic (continuum) and microscopic models, used for simulation of material behaviors under different loading conditions, contain a large number of material parameters and determination of these parameters is an important and difficult issue in the modeling. The aim of this work essentially deals with parameter determination procedure of any viscoplasticity model. In this study, genetic algorithm (GA) parameter optimization procedure has been proposed to determine material parameters of viscoplastic models. Parameter determination capability of the GA optimization method was tested by using VBO model which one of the viscoplasticity theory with no yield surface and loading–unloading conditions. Fourteen material parameters of VBO model are determined using uniaxial loading–unloading stress strain curves of high density polyethylene (HDPE). Using these material parameters, creep and relaxation behaviors of HDPE are simulated. A good match with experimental results is obtained. Apart from many existing studies in the literature, GA optimization procedure is applied to determine material parameters instead of trial and error procedure. This method can also be used to determine materials parameters of other viscoplasticity theories for all kinds of materials. 相似文献
36.
Aykut Özgülsün Filiz Karaosmanôglu Melek Tüter 《Journal of the American Oil Chemists' Society》2000,77(1):105-109
In this study, the esterification of oleic acid with a fraction of fusel oil was investigated. The variables that affect ester
yield, such as temperature, molar ratio of oleic acid to alcohol, and amount of catalyst, were determined. Powdered silica
gel was chosen to remove water instead of granular silica gel, magnesium sulfate, or benzene. The behavior of amyl alcohols
and the fusel oil fraction was compared. The esterification reaction was carried out under the reaction conditions selected
as optimal, and the ester conversion of the reaction was 97.3%. The product mixture compressed products, excess reactants,
catalyst, and desiccant. Oleate ester and oleic acid (2.7%) were obtained using the refinement steps of filtration, evaportation,
washing with distilled water, and drying over sodium sulfate. 相似文献
37.
Filiz Yasar Mahlicli Sacide Alsoy Altinkaya 《Journal of materials science. Materials in medicine》2013,24(2):533-546
This study intends to improve blood compatibility of polysulfone (PSF) membranes by generating a nonthrombogenic surface through heparin immobilization. To achieve this task, the support membrane prepared from a blend of PSF and sulfonated polysulfone (SPSF) was modified with layer by layer (LBL) deposition of polyethyleneimine (PEI) and alginate (ALG) and heparin blended with ALG was immobilized only on the outermost surface of the LBL assembly. The results have shown that the adsorption of human plasma proteins and platelet activation on the LBL modified membranes decreased significantly compared with the unmodified PSF and PSF-SPSF blend membranes. Furthermore, blending ALG with a small amount of heparin remarkably prolonged the APTT values of heparin free PEI/ALG coated membranes. It is envisaged that the use of a blend of HEP and ALG only in the terminating layer of the LBL assembly can be an economical and alternative modification technique to create nonthrombogenic surfaces. 相似文献
38.
Yolcu Gozde Oztel Ismail Kazan Serap Oz Cemil Palaniappan Kannappan Lever Teresa E. Bunyak Filiz 《Multimedia Tools and Applications》2019,78(22):31581-31603
Multimedia Tools and Applications - Facial expressions are a significant part of non-verbal communication. Recognizing facial expressions of people with neurological disorders is essential because... 相似文献
39.
40.
In this work, we investigated the effect of electrodeposition of polypyrrole (PPy) films on two different self-assembled monolayers (SAMs) modified gold electrode for the electrochemical construction of ultramicroelectrode (UME). In order to obtain SAM modified surfaces, 4-mercapto-1-butanol and 11-mercaptoundecanoic acid were used. The effect of these two chains on pyrrole electropolymerization was compared. Electropolymerization of pyrrole on SAM modified Au electrode was carried out by using cyclic voltammetry (CV) and constant potential electrolysis. To investigate the UME formation, the obtained surfaces were tested in Fe(CN)63−/4− redox system. UMEs were characterized using scanning electron microscopy energy-dispersive X-ray spectroscopy, attenuated total reflectance fourier transform infrared spectroscopy and electrochemical impedance spectroscopy. The designed UME was applied as an immobilization matrix to entrap a redox protein, Hemoglobin (Hb), as a model. Direct electron transfer between this protein and the fabricated thiol modified PPy based UME was achieved, which is very challenging on bare electrode surfaces. With this study, a simple, low-cost and reproducible UME production way has been successfully accomplished and Hb modified UME is promising for different bioanalytical applications, for instance; cellular hydrogen peroxide or nitrite sensing. 相似文献