Facile synthesis of ordered nanocrystalline alumina thin films with tunable mesopore structures

Mesoporous alumina layers have attracted attention for their potential use in ultrafiltration of salts, as a heterogeneous catalyst support, an adsorbent in environmental cleanup, and in petroleum refinement. The ability to control the fast hydrolysis rate of the inorganic precursors using simple and inexpensive routes is important for that potential to be realized. Herein, we introduce a novel and facile route to synthesize mesoporous alumina thin films from the combination of inexpensive and commercially available copolymer with aluminum chloride or nitrate (salts) in an EtOH–surfactant–NH₃ · H₂O–salts (EsNs) system through the evaporation-induced self-assembly (EISA) method. Mesoporous alumina layers obtained utilizing the EsNs system have ordered and tunable pore structures. The ability to easily control the mesophases of the alumina layers within a short time provides distinct advantages over previously reported synthesis procedures. Most importantly, we demonstrate that the binding of surfactant and NH₃ · H₂O for the formation of hydrogen bond between them in the EsNs system controls the fast hydrolysis rate of the inorganic species. This allows for the synthesis of nanocrystalline alumina layers via the aluminum oxo-clusters’ assembly with the surfactant. Such simple route may be applied in the synthesis of other non-silica mesostructured oxides.     

一种基于循环小波累积量的谐波恢复方法

循环统计量是乘性和加性噪声中谐波恢复问题的主要分析工具之一。本文在其基础上提出了一种新的理论与方法——基于循环小波累积量的谐波恢复方法。首先,提出了循环小波累积量的定义。然后,建立了基于一阶、二阶、三阶循环小波累积量的谐波分量的频率和相位的估计方法。在此基础上,采用了一种可调参数的小波,通过调节其参数来改善传统方法中频率分辨率低的缺陷。最后给出了模拟实验结果。     

成像光谱技术发展的科学背景和现状

本文分析与阐述了成像光谱技术发展的科学背景与现状。     

Steady-state modeling of resistive-gate MOSFETs

The Pao-Sah model for the long-channel MOSFET is generalized to include MOSFETs with resistive-gate electrodes (RG-MOSFETs). The RG-MOdSFETs current-voltage characteristics are studied using this extended Pao-Sah model. The steady-state operation of the RG-MOSFET can be divided into three regimes, separated by the uniform channel condition and the pinch-off condition, respectively. The regions of operation are discussed, and a simple analytical I-V expression is given for the device     

Synthesis of large building blocks for dendritic polyethers

Summary Building blocks containing multi-aryl ethers linkage in larger size for rapid building larger dendrimers were prepared with 3,5-di(4-hydroxyphenoxy)benzyl alcohol (1) as branch monomer and 1,3,5-tri(4-hydroxyphenoxy)benzene (2) as core molecule. Two generation of dendritic polyethers (12 and 15) were obtained by Fréchet convergent approach with 3,5-diphenoxybenzyl bromide (3) as starting molecule. They were characterized firstly by ¹H-NMR, ¹³C-NMR, and MS.     

实时跟踪控制系统中的数字滤波技术

在高精度的实时跟踪控制系统中，由探测器等其他一些因素给系统带来的噪声将不容忽视，数字滤波将是滤除噪声的有效手段，，由于系统实时性和采样频率的要求，本文介绍几种时跟踪系统中常用的数字滤波方法，并对它们在实时跟踪系统中的作用进行了和比较。     

Interactions between normal and tumoral tissues at the boundary of human anterior pituitary adenomas. An immunohistochemical study

Previously, the species complex Oncomelania hupensis, individuals of which act as intermediate hosts for the human bloodfluke Schistosoma japonicum, has been characterised by morphological and isoenzyme criteria. We have examined genetic variation between and within three subspecies of Oncomelania hupensis, i.e. O. h. hupensis (China), O. h. quadrasi (Philippines) and O. h. nosophora (Japan), by direct means using a PCR-based RFLP method. The subspecies of O. hupensis were readily distinguished by their characteristic restriction patterns, supporting isoenzyme data which suggests these may warrant species-specific status. No genetic variation was observed between O. h. quadrasi from different islands within the Philippines. In contrast, geographical isolates of O. h. hupensis differed markedly by this method indicating several genetically distinct populations of O. h. hupensis occur in China.     

激光对抗技术发展动态

激光对抗主要包括激光侦察告警、激光无源干扰和有源干扰，以及激光防护几方面。本文概述了激光对抗技术的发展。     

大型离心复合球墨铸铁轧辊的生产

简述了我公司为舞阳铜厂试制４２００ｍｍ厚板轧机离心复合球墨铸铁轧辊的性能要求、内外层双重金属铸造工艺参数的选择及整个铸造生产工艺过程。