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The syntheses of polyenynes as model compounds for poly(diacetylene)s (PDAs) are described. Variation of properties (UV–VIS, Raman, NMR and bond geometries) as a function of the chain length was investigated. After extrapolation to infinite chain length these data were compared to those for PDAs. From UV–VIS spectra a value of λ = 551 nm (2.25 eV) was calculated corresponding to the electronic transition of a single polyenyne chain. This energy is located at the low energy end of a yellow PDA solution spectrum. From Raman scattering v(C?C) = 2108–2128 cm?1 and v(C?C) = 1505–1532 cm?1 were calculated after extrapolation. Similarly sp-C13C NMR data yielded a shift of δ = 100 ppm. These data are almost identical to data known for yellow PDA solutions. Bond geometries are almost identical to those of poly(diacetylene)s and theoretical data. 相似文献
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Works of adhesion at the carbon fiber-liquid interface determined using a modified wetting technique
Works of adhesion WSL between aqueous solutions with pH values in the range from 1 to 14 and carbon fibers from different sources, which were additionally treated in an inert atmosphere or in oxygen, were measured by use of a microbalance. These works of adhesion WSL were found to show distinct stepwise dependencies on the pH value. The works of adhesion WSL are attributed to dispersion interactions WSL1 and various acid-base interactions wslab—in the latter case between the acidic and basic surface groups of carbon and the various basic and acidic aqueous solutions. 相似文献
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Distributed Multirobot Exploration and Mapping 总被引:3,自引:0,他引:3
Fox D. Ko J. Konolige K. Limketkai B. Schulz D. Stewart B. 《Proceedings of the IEEE. Institute of Electrical and Electronics Engineers》2006,94(7):1325-1339
Efficient exploration of unknown environments is a fundamental problem in mobile robotics. We present an approach to distributed multirobot mapping and exploration. Our system enables teams of robots to efficiently explore environments from different, unknown locations. In order to ensure consistency when combining their data into shared maps, the robots actively seek to verify their relative locations. Using shared maps, they coordinate their exploration strategies to maximize the efficiency of exploration. This system was evaluated under extremely realistic real-world conditions. An outside evaluation team found the system to be highly efficient and robust. The maps generated by our approach are consistently more accurate than those generated by manually measuring the locations and extensions of rooms and objects. 相似文献
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Schulz Laura E.; Bonawitz Elizabeth Baraff; Griffiths Thomas L. 《Canadian Metallurgical Quarterly》2007,43(5):1124
Causal learning requires integrating constraints provided by domain-specific theories with domain-general statistical learning. In order to investigate the interaction between these factors, the authors presented preschoolers with stories pitting their existing theories against statistical evidence. Each child heard 2 stories in which 2 candidate causes co-occurred with an effect. Evidence was presented in the form: AB→E; CA→E; AD→E; and so forth. In 1 story, all variables came from the same domain; in the other, the recurring candidate cause, A, came from a different domain (A was a psychological cause of a biological effect). After receiving this statistical evidence, children were asked to identify the cause of the effect on a new trial. Consistent with the predictions of a Bayesian model, all children were more likely to identify A as the cause within domains than across domains. Whereas 3.5-year-olds learned only from the within-domain evidence, 4- and 5-year-olds learned from the cross-domain evidence and were able to transfer their new expectations about psychosomatic causality to a novel task. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
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J.C. Schulz O.E.R. Heimdahl S.A. Finnegan 《International Journal of Impact Engineering》1987,5(1-4):577-584
A computational study to examine the effects of parameter variation on debris cloud formation and perforation behavior in a simple sphere-plate impact situation is described. The parameters varied were impact velocity, thickness: diameter ratio, projectile-target material combination and number of plates. In particular, effects associated with changes from strength-dominated to hydrodynamic behavior were considered. 相似文献
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M. Schulz 《Microelectronic Engineering》1998,40(3-4):113-130
The classical capacitance-voltage measurement methods and the conductance technique which are frequently used to analyze the SiO2---Si system, are briefly introduced and critically evaluated. These measurement techniques are based on macroscopic device structures, average structure parameters are determined. Transient and random telegraph signal measurements, and charge pumping are now available as new methods to study the SiO2---Si interface in sub-μm device structures. These techniques permit to analyze single, individual traps in the interface. Traps in small devices are isolated. The capture rates are thermally activated by the Coulomb energy. 相似文献