550 MPa级中厚板矫直过程中表面凹坑缺陷的成因与对策

针对550 MPa级高强中厚板在矫直过程中极易出现氧化铁皮压入凹坑缺陷的问题，根据现场矫直工艺，研究了在不同温度下进行热变形时试样表面和横截面的形貌，钢基体与氧化铁皮界面处平直度的变化规律。结果表明，热变形温度为450 ℃时，表面氧化铁皮开始出现裂纹，且随着变形温度的降低，裂纹的数量逐渐增加；此外，氧化铁皮与钢基体之间的界面长度随变形温度的降低而呈直线增加，表明氧化铁皮与钢基体界面平直度随着热变形温度的降低越发粗糙、易脱落而形成凹坑缺陷。为此，应适当提高终轧温度以确保矫直时钢板表面温度大于450 ℃，同时提高钢板的运行速率，防止氧化铁皮在低温变形发生破碎和脱落的同时降低氧化铁皮厚度，从而减小因氧化铁皮脱落而造成凹坑缺陷的发生几率。     

压入深度与膜厚对薄膜与基体复合硬度及弹性模量的影响

根据高华建的复合弹性模量模型，提出了用一个测点的载荷-位移曲线计算整个压入深度内薄膜和基体复合硬度分布的方法，探讨了压入深度与膜厚对硬度与弹性模量测量值的影响，指出可由膜-基复合性能反推膜本身的性能。     

双金属盘式制动器的试制与研究

汽车工业的发展对刹车系统的关键零部件——刹车盘的抗冲击韧性提出了更高的要求。研究结果表明，把灰铸铁(HT250)与用优质碳素结构钢25Mn预先冲压成型的钢件镶铸在一起制成的1种新型刹车盘，既具有灰铸铁良好的抗磨、减震、尺寸稳定等性能，又具有较高的抗冲击韧性，能够满足汽车工业高速化、轻量化对刹车盘的综合要求。     

Al-Pb-Si-Sn-Cu轴瓦合金的微观结构及特征

采用机械合金化、冷压与热挤压法制备了Al-15％Pb-4％Si—1％Sn—1．5％Cu(质量分数，％)轴瓦合金。试验结果表明，块体材料的组织分布很均匀。Pb粒子细小均匀弥散分布在Al基体上，呈纳米晶粒。Al基体晶粒大小约1．2μm，在其晶界和晶粒内都有粒子析出。在Al基体上还分布着由非晶和亚微米晶粒构成的混合相。研究表明，该工艺是制备Al-Pb系列轴瓦合金的较佳方法；并为制备室温不互溶、高温存在很宽固溶间隙、有较大密度差异的合金组元且组织均匀的合金奠定了工艺基础。     

磁性塑料注射成型机设计原理

磁性塑料作为一种重要的基础材料近年来得到了不断发展和广泛应用,而注射成型是磁性塑料的一种新的成型或加工工艺,其核心技术就是磁性塑料注射成型机.分析了磁性塑料注射成型机的工作原理,提出了磁性塑料注射成型机的设计原则,给出了磁性塑料注射成型机的设计方案、主要技术参数及主要部件的设计简图,并重点讨论了磁性塑料注射成型机的主要部件--塑化和充磁系统的设计,可为塑料注射成型机的推广应用以及系列化开发提供指导和帮助.     

Effect of miscibility and forced compatibility on damping properties of CIIR/PAc blend

In this study, a kind of novel damping materials was prepared based on the blend of chlorinated butyl rubber (CIIR) and polyacrylate (PAc) synthesized by different molar ratio of butyl methacrylate and ethyl acrylate. Research results from experiments and analyses by employing DMA, TEM, and FTIR show that whether at a cocured system or noncocured system, it can be achieved to shift a loss peak of CIIR towards a higher temperature region and to keep the damping value from markedlly decreasing, which broadens the effective damping function area of CIIR to the vicinity of ambient temperature. In the former system, the thermodynamical miscibility of CIIR and PAc, to some extent, is predominated by the molecular design of PAc, while in the latter system, covulcanized networks play a more significant role in improving compatibility and abating the peak split, though the suppression effect of thermal stress on the transition of CIIR T_ll transition still can not be neglected. Furthermore, transition state derived from the cocuring CIIR and PAc cannot make the phase separation completely take place, and consequently results in the deformation of phase morphology of the cocured CIIR/PAc blend. It is the influence of thermodynamics miscibility and forced compatibility in different size that makes the suppression effect of foreign PAc on CIIR T_ll transition be controllable. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3127–3133, 2006     

高效液相色谱法测定稻·噁乳油含量

采用高效液相色谱法,在同一色谱条件下对稻·噁乳油中所含有效成分稻瘟灵和噁霉灵同时进行含量测定。色谱条件为:使用Nova-PaK C18250mm×4.6mm(i.d)不锈钢色谱柱,流动相v(甲醇)∶v(水)=70∶30,流速1mL/min,检测波长为220nm。测定方法中稻瘟灵和噁霉灵的回收率分别在98.8%～100.3%和98.6%～100.0%之间,变异系数分别为0.54%和0.52%,证明本方法快速、准确、可靠。     

基于全网能量均衡的WirelessHART图路由算法

如何均衡使用网络节点能量并生成高可靠路由是WirelessHART网络研究的一个难题,为此提出了一种GRAEB（graph routing algorithm based on energy balancing）图路由算法。首先,网络被初始化为连通的图结构,能够提高丰富的冗余路径。网络管理器根据全网节点剩余能量、通信周期、链路分布等因子生成节点鲁棒系数矩阵,节点通过比较邻居的鲁棒系数来选择最优路径。另外,规定了邻居节点数的上限阈值,每次路由更新只保留鲁棒系数最优的邻居。仿真结果表明GRAEB不仅提高了网络可靠性,而且延长了网络寿命。     

基于表面等离子体共振传感器的尿微量白蛋白检测

检测尿微量白蛋白(MAU)可对轻微肾脏损害进行早期诊断,也可对高血压患者可能发生的心脑血管事件进行预测。实验将抗体通过巯基自组装固定于Au膜表面,研制了一种快速检测MAU的表面等离子体共振(SPR)生物传感器。结果表明:直接检测法可以检测到0.3μg/L的MAU,而纳米Au放大法检测限可以低至0.03μg/L。     

CaCO3/natural rubber latex nanometer composite and its properties

Calcium carbonate/natural rubber (NR) latex nanometer composites were prepared by adding nanometer CaCO₃ whose surface had been treated to natural rubber latex (NRL) before sulfuration. The physical, thermooxidative aging, and thermal degradation properties and the ultra‐microstructure were analyzed with a multipurpose material testing meter, a thermal analysis meter and a Philips XL‐30 SEM, respectively. The results showed that the structures and properties of nanometer composites could be clearly improved by NRL mixed with surface‐treated nanometer CaCO₃. The physical properties of the nanometer composites were best when the content of surface treatment agent was 2.5% (to nanometer CaCO₃), the nanometer CaCO₃/NRL content was 3:100, and the stirring time for treating the surface of the nanometer CaCO₃ was 20 min. Simultaneously, the thermooxidative aging resistance of the nanometer composites also was significantly improved. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3442–3447, 2006