A110－1－H／A110－1型氨合成催化剂在双筐并流合成塔中的使用

在双筐并流氨合成塔中使用了Ａ１１０－１－Ｈ／Ａ１１０－１型氨合成催化剂，使用寿命达１７４０天，累计产氨４３８３７８ｔ．该催化剂组合具有低温活性好、易还原、高催化活性、高抗毒能力、良好的热稳定性与破碎强度等优点．     

Study of thermally poled and corona charged poly(vinylidene fluoride) films

The effect of thermal poling and corona charging on the structure and characteristics of poly(vinylidene fluoride) films (PVDF) was investigated. The structure and chemical change of PVDF films with different polarizing treatments was examined using Fourier transform infrared spectroscopy and X‐ray photoelectron spectroscopy, respectively. The characteristics including piezoelectric coefficients, ferroelectric hysteresis, and leakage current were measured. It was found that both polarized methods contribute to dramatic improvement on the piezoelectricity and ferroelectricity of PVDF films, while thermal poling leads to structure change with the generation of new carbon composition. The reason to cause leakage current was also analyzed. POLYM. ENG. SCI., 47:1344–1350, 2007. © 2007 Society of Plastics Engineers     

Dynamic response of Ti3SiC2 under shock compression up to 112 GPa

Ti₃SiC₂ is of interest due to its unique dual nature reminiscent of both brittle ceramics and ductile metals at ambient conditions. In this work, plate-impact experiments have been performed to study the dynamic behavior of Ti₃SiC₂ under shock compression up to 112 GPa by using laser velocity interferometer and electric pin techniques. Hugoniot elastic limits (HEL), spall strength, and Hugoniot equations of state have been obtained based on measured particle velocity profiles and shock wave velocities. The ratio of spall strength to HEL for Ti₃SiC₂ is larger than brittle ceramics but smaller than metals. This result indicates that the dual nature of Ti₃SiC₂ remains at least up to 10 GPa. On the other hand, the linearity of the Hugoniot equation of state, $D=6.9\text{0}1(22)+1.153(53)u_{\text{p}}$, suggests that the initial structure of Ti₃SiC₂ should be stable up to 112 GPa, in contrast to the result reported by Jordan et al. [J. Appl. Phys., 93 (2003) 9639].     

不同炭化压力下沥青炭结构特性的研究

将高温煤沥青和浸渍剂沥青在不同压力下炭化，在2500℃下对所得沥青炭进行石墨化处理；测试了所得沥青炭的体积密度、开孔率；利用扫描电子显微镜（SEM）观察了所得沥青炭的显微结构；利用XRD检测了不同炭化压力所得沥青炭石墨化处理后的石墨化度。结果表明：随着炭化压力的增大．沥青炭的体积密度增大而开孔率减小；随着炭化压力的增大沥青炭显微结构有从流线型向镶嵌型和域型转变的趋势：流线型结构沥青炭石墨化度较高；沥青中QI组分也会影响沥青炭的显微结构。     

Preparation and Catalytic Performance of Mesostructured Aluminosilicate Nano-particles with Wormhole-Like Framework Structure

A facile two-step sol–gel method has been developed for the preparation of mesostructured aluminosilicate nano-particles (Si/Al = 7.5) with wormhole-like but uniform pore structures and highly catalytic activities towards bulky hydrocarbon cracking. It is desirable that, as this synthesis takes place in the absence of alkali cations, the mesoporous nano-particulate material is directly obtained in the acid form, making a subsequent ion-exchange and calcination treatment superfluous.     

铁路盐酸槽车衬胶与维修

简要介绍了铁路盐酸槽车衬胶工艺和衬胶层维修及其后期维修     

粉煤灰空心砖裂纹的成因及防治

介绍粉煤灰空心砖裂纹产生的原因及消除方法。     

聚合物纳米复合材料的研究进展

介绍了聚合物基纳米复合材料的种类及制备方法，详细介绍了聚合物／层状硅酸盐纳米复合材料的研究，包括聚合物／层状硅酸盐纳米复合材料的种类、性能及研究的新进展。     

提高100%无烟煤煅烧熟料早期强度的探索

1997年投产的国内首条100%燃无烟煤生产线——龙岩三德2000t/d熟料线的熟料3d强度一直偏低,平均仅为25.5MPa(新标准)。通过对3d强度因素及其相关性分析,排序为w(C2S)>熟料KH值>生料细度>入窑生料的w(Al2O3)。在此基础上,提出了调整配比,提高煤粉和生料细度质量指标以及提高石灰石和燃煤质量等一系列技术措施。