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81.
82.
The physicochemical and electrochemical properties of three 1-alkyl-2,3,5-trimethylpyrazolium cation-based room-temperature ionic liquids with various alkyl chain lengths were investigated. The temperature dependences of density, viscosity, and ionic conductivity were obtained by precise measurements. Electrolyte properties of these room-temperature ionic liquids were also examined from the viewpoint of their uses in lithium secondary batteries ([LiCoO2 positive electrode|electrolyte|lithium metal negative electrode]). It was found that the alkyl chain length affects the charge–discharge performances of cells.  相似文献   
83.
A new reactor concept of innovative water reactor for flexible fuel cycle (FLWR) is under development at Japan Atomic Energy Agency in cooperation with Japanese reactor suppliers. A design of 1,356 MWe high conversion boiling water reactor-type FLWR core, which has an instantaneous conversion ratio of 1.04, negative void coefficient, high burnup of 65 GWd/t, and 15-month operational cycle length, has been constructed. So far, studies on thermal-hydraulic characteristics have been performed for tight lattice core. Evaluation methods for the critical power and the pressure drop under both the steady and the transient states have been established, and a modified TRAC-BF1 code has been developed for the thermal-hydraulic design of the FLWR. In this paper, the thermal feasibility of the designed 1356MWe FLWR core is analyzed by using the modified TRAC-BF1 code. The analysis is first carried out for the current core design. It is confirmed that no boiling transition (BT) occurs under the steady state. However, the minimum critical power ratio (MCPR) is only about 1.08, and the BT is confirmed occurring under the postulated abnormal transient processes. Therefore, concretizations of the conditions that ensure the thermal feasibility of a natural circulation-type FLWR and a forced circulation-type FLWR are performed. As for the results, for a forced circulation-type FLWR, the operation-limited MCPR (OLMCPR) is 1.32, and the necessary minimum core coolant flow rate is 640 kg/(m2s). For a natural circulation-type FLWR, the OLMCPR is 1.19, and the necessary minimum core coolant flow rate is 560 kg/(m2s).  相似文献   
84.
85.
It has been confirmed, from observations with an electron microscope after staining negatively with aqueous uranyl acetate solutions and using a flourescent microscope, that sucrose fatty acid esters form closed vesicles. The range of particle size of the vesicle, consisting of chromatographically fractionated sucrose dilaurate, was apparently 70–700 nm in the longer diameter of individual vesicles based on the transmission electron microscopic (TEM) observation. The weight-average particle size was 424 nm as shown by means of the photon-correlation method. The amounts of 6-carboxyfluorescein trapped in the vesicles of sucrose fatty acid esters were determined, and it was ascertained that the volumes of the central water phase depended upon the acyl chain lengths of fatty acid residues. Further, the effect of the additives [cholesterol and dicetyl phosphate (DCP) was examined. As an example, the vesicle of sucrose stearate had a central water phase of 1.7 one water/mol ester, and showed a slow release of 6-carboxyfluorescein from the central water phase after preparation of the vesicle.  相似文献   
86.
Amorphous carbon materials for lithium ion battery anodes which contain a small amount of Li2CO3 were prepared by three methods. The obtained materials were characterized using X-ray diffraction (XRD) analysis, Raman spectroscopy and CO2 adsorption experiments. Although the XRD profiles and Raman spectra of these materials were similar to those of carbon materials synthesized with no addition, the amount of CO2 adsorbed was largely decreased by Li2CO3 addition. These results suggest that the micropores in these materials were plugged and/or filled with Li2 CO3. Galvanostatic lithium charging and discharging experiments showed that the irreversible capacity of the material can be significantly decreased by Li2CO3 addition, which is thought to be due to the plugging of the pore inlets by Li2CO3. Moreover, it was also found that the reversible capacities of the materials can be increased by adjusting both the amount of Li2CO3 addition and carbonization temperature.  相似文献   
87.
Results from double directional ultrawideband (UWB) channel sounding in a wooden house are described. The double directional channel sounder estimates directional information at both ends of the link, so that we can separate antenna directivity from the channel sounding results. We investigated the dominant propagation mechanisms by introducing cluster analyses. The detected propagation paths from the channel sounding were first classified into clusters in the angular-delay domain, and then properties of the clusters such as standard deviation of path positions, dynamic range of path power, and power distribution of clusters were derived. From the results, we discussed the similarities and differences between the measurement environment and the physical propagation phenomena. Finally, different types of scattering losses of the propagation paths were derived and modeled. The results from sounding and analysis contribute in the development of UWB propagation models and can be used in UWB propagation simulations  相似文献   
88.
Commercial zinc oxide nanoparticles (20–30 nm) were coated by aminopropyltriethoxysilane (APTES) under varying environments. Three different processes, acidic, basic and toluene were used. The effects of coating conditions (acidic, basic and toluene) on the grafting, structural and optical properties of these nanoparticles were studied. In the three cases, it was possible to control the coating and according to X-ray diffraction, BET, TEM and SEM results, it is clear that the APTES coating plays a role of growth inhibitor even at 800 °C. From diffuse reflectance measurements, one can notice that the grafting process did not modify the transmittance spectra of ZnO.  相似文献   
89.
This article deals with preparations of fine particles of metallocene copolymers by emulsifierfree emulsion polymerization of vinylferrocene (VFc), ferrocenylmethyl methacrylate (FMMA), 1-ferrocenylethyl methacrylate (1-FEMA), 2-ferrocenylethyl methacrylate (2-FEMA), and 1-ruthenocenylethyl methacrylate (1-REMA) with acrylonitrile (AN), styrene (St), and methyl methacrylate (MMA) in water/ethanol medium. As a result, spherical copolymer particles containing metallocene derivatives have been successfully synthesized in the particle size of ca. 120 to 600 nm. The contents of ferrocenyl or ruthenocenyl groups in copolymer particles increased with increasing concentration of charged metallocene derivatives, while the amounts of metallocene derivatives incorporated into particles are much lower than the charged ratio. © 1994 John Wiley & Sons, Inc.  相似文献   
90.
Food processing environments are suspected to be the primary source of Listeria monocytogenes contamination of foods. We investigated the survival of L. monocytogenes on stainless steel that was soiled with food components (minced tuna, ground pork, and cabbage) followed by dehydration. Stainless steel coupons were inoculated with 107 CFU/coupon and stored up to 30 days. In comparison with Staphylococcus aureus and Salmonella Typhimurium, L. monocytogenes demonstrated the highest survivability where about 3 log CFU/coupon remained at the end of the experimental period. While survival during the early storage period was markedly affected by both food-component attachment and food type, a long dehydration period diminished the effect of those.  相似文献   
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