A Study on NMR and GC/MS Spectra of the Isomers of Linear Hexyl Naphthalene

The GC/MS and NMR analysis of the reaction products of naphthalene with 1-bromohexane were reported. The products obtained were suggested to have six isomers of linear hexylnaphthalene and the structure of each isomer was determined by GC/MS and NMR spectra. For the first time, the unique chemical shift data were obtained. The content of each isomer calculated by ¹H NMR and ¹³C NMR spectra was consistent with that by GC/MS spectra, which confirmed the accuracy of NMR data.     

线性调制抗噪声性能的提高方法

本文主要是在线性解调系统中,利用信道中加性高斯白噪声正交分量(nc与Ns)两者正交性与其中之一(ns)经相移之后形成线性相关性使噪声本身消除噪声,以达到提高信噪比的目的,从而提高抗噪声性能.     

On Ultra-Fine Leak Detection of Hermetic Wafer Level Packages

Theoretical and practical ranges of leak rates measurable by the helium mass spectrometer are characterized. The effect of noise due to: 1) background helium present in the spectrometer and 2) desorption of helium that attaches itself to the specimen surface during bombing is quantified experimentally. The results guide a framework to extract the true leak rate from the measured leak rate profile. An optical interferometry based hermeticity measurement technique for ultra-fine leaks is proposed. The setup to implement the technique is described and a preliminary experimental result is reported.     

Investigation of Mechanical and Electrical Characteristics for Cracked Conductive Particle in Anisotropic Conductive Adhesive (ACA) Assembly

In an anisotropic conductive adhesive (ACA) assembly, the electrical conduction is usually achieved with the conductive particles between the bumps of integrated circuit (IC) and corresponding conductive tracks on the glass substrate. Fully understanding of the mechanical and electrical characteristics of ACA particles can help to optimize the assembly process and improve the reliability of ACA interconnection. Most conductive particles used in the ACA assembly are with cracks in the metal coating of the particles after the ACA bonding. This paper introduced the fracture analysis by applying the cohesive elements in the numerical model of the nickel-coated polymer particle and further simulating the cracks initiation and propagation in the nickel coating during the ACA bonding. The simulation results showed that the stress distribution on the nickel-coated particle with cracks was significantly different from that on the nickel-coated particle without crack, indicating that the stress analysis by taking the crack into consideration is very important for the reliability assessment of the ACA interconnection. The stress analysis of cohesive elements indicated that the cracks initiated at the central area of the nickel coating and propagated to the polar area. Furthermore, by the introduction of a new parameter of the virtual resistance, a mathematical model was established to describe the electrical characteristics of the nickel-coated particle with cracks. The particle resistance of the nickel-coated particle with cracks was found to be much higher than that of the particle without crack in the optimized bonding pressure range, indicating that it is necessary to take the crack into consideration for the particle conduction analysis as well. Therefore, the fracture analysis on the conductive particle by taking the crack into consideration could accurately evaluate the reliability of ACA interconnection and avoid serious reliability issues.     

Effects of Y and Ce on Microstructures and Properties of Nb-Si System Composites

The effects of yttrium and cerium on microstructures and properties of Nb-Si system composites were investigated by scanning electron microscopy( SEM), energy dispersive spectrum(EDS), X-ray diffraction(XRD) and high temperature oxidation experiments.It is found that the coarse primary silicide phase became finer and more homogeneous with Y and Ce addition.The results of high temperature oxidation experiments show that the oxidation rates of NbSi system composites with an appropriate amount of Y and Ce decrease compared with those of alloys without Y or Ce addition, and oxidation products mainly distribute along the phase boundaries between the Nb solid solution and silicide.     

分置式牛津型斯特林制冷机的数值分析与实验验证

对分置式牛津型斯特林制冷机进行了数值计算 ,介绍了计算模型考虑到的众多不可逆因素。通过对计算结果与实验结果的对比 ,验证了本文数值计算的准确性 ,说明本文计算模型与数值处理方法是切实可行的     

Reduction of optical beat interference using gain-saturated RSOA in upstream WDM/SCM optical links

A new scheme for reducing optical beat interference (OBI) noise in optical network units is proposed for subcarrier multiplexing-based access network applications. The optical spectrum of the transmit lasers is broadened by using a radio frequency (RF) clipping tone with a modulation depth greater than one. This reduces the impact of the OBI noise. The distortions caused by an RF clipping tone are also suppressed by introducing a gain-saturated reflective optical amplifier, which shows the characteristics of high-pass filter. The proposed scheme has been verified by measuring the error vector magnitude of 16QAM signal with 20 Mbps. Error-free transmission has been achieved even when the light of OBI-noise-causing lasers is stronger than that of the signal laser by 7 dB     

Cu—Zn—Al系合金热弹性马氏体相变的热滞

本文通过热处理工艺及添加第四组元研究了Cu－Zn－Al系记忆合金的相变热滞。结果表明，淬火冷却速度影响合金的相变热滞大小，随着母相时效时间的延长，马氏体相变热滞变大．Mn元素的加入可以减小CU－Zn－Al合金相变热滞．     

肝癌碘油栓塞后肝区平片所见碘油沉积量与疗效关系

本文分析了90例肝癌肝动脉灌注化疗碘油栓塞后,肝区平片所见碘油沉积量和疗效的关系。碘油沉积分为多,中,少三组,从ATP下降,肿瘤缩小率及一年生存率三方面比较。结果沉积多的与中等组三项都有显著差别;沉积中等的与少的组差别不明显。说明碘油沉积要达到一定的量后,疗效才会显著提高。同时分析了影响碘油沉积的几个因素。