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51.
Writing with Fluid: Structuring Hydrogels with Micrometer Precision by AFM in Combination with Nanofluidics 下载免费PDF全文
Nicolas Helfricht Andreas Mark Marina Behr Andreas Bernet Hans‐Werner Schmidt Georg Papastavrou 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(31)
Hydrogels have many applications in biomedical surface modification and tissue engineering. However, the structuring of hydrogels after their formation represents still a major challenge, in particular due to their softness. Here, a novel approach is presented that is based on the combination of atomic force microscopy (AFM) and nanofluidics, also referred to as FluidFM technology. Its applicability is demonstrated for supramolecular hydrogel films that are prepared from low‐molecular weight hydrogelators, such as derivates of 1,3,5‐benzene tricarboxamides (BTAs). BTA films can be dissolved selectively by ejecting alkaline solution through the aperture of a hollow AFM‐cantilever connected to a nanofluidic controller. The AFM‐based force control is essential in preventing mechanical destruction of the hydrogels. The resulting “chemical writing” process is studied in detail and the influence of various parameters, such as applied pressure and time, is validated. It is demonstrated that the achievable structuring precision is primarily limited by diffusion and the aperture dimensions. Recently, various additive techniques have been presented to pattern hydrogels. The here‐presented subtractive approach can not only be applied to structure hydrogels from the large class of reversibly formed gels with superior resolution but would also allow for the selective loading of the hydrogels with active substances or nanoparticles. 相似文献
52.
Andreas Nägelein Matthias Steidl Stefan Korte Bert Voigtländer Werner Prost Peter Kleinschmidt Thomas Hannappel 《Nano Research》2018,11(11):5924-5934
Profiling of the electrical properties of nanowires (NWs) and NW heterocontacts with high spatial resolution is a challenge for any application and advanced NW device development. For appropriate NW analysis, we have established a four-point prober, which is combined in vacuo with a state-of-the-art vapor-liquid-solid preparation, enabling contamination-free NW characterization with high spatial resolution. With this ultrahigh-vacuum-based multi-tip scanning tunneling microscopy (MT-STM), we obtained the resistance and doping profiles of freestanding NWs, along with surface-sensitive information. Our in-system 4-probe STM approach decreased the detection limit for low dopant concentrations to the depleted case in upright standing NWs, while increasing the spatial resolution and considering radial depletion regions, which may originate from surface changes. Accordingly, the surface potential of oxide-free GaAs NW {112} facets has been estimated to be lower than 20 mV, indicating a NW surface with very low surface state density. 相似文献
53.
Jürgen R. Reichenbach Marco Essig E. Mark Haacke Benjamin C. Lee Christian Przetak Werner A. Kaiser Lothar R. Schad 《Magma (New York, N.Y.)》1998,6(1):62-69
The purpose of this study was to evaluate a non-flow related magnetic resonance imaging method to visualize small veins independent of arteries in the human brain. A long TE, high-resolution 3D gradient echo MR acquisition was used to highlight venous information. The method is based on the paramagnetic property of deoxyhemoglobin and the resulting phase difference between veins and brain parenchyma at long echo times. The MR magnitude images were masked with a phase mask filter to enhance small structure visibility.. Venous information down to sub-pixel vessel diameters of several hundred microns is visible. Venous data are displayed in an angiographic manner using a minimum intensity projection algorithm. Both superficial veins and deep white matter veins are visible. The method has been successfully applied in volunteers. Preliminary results in patients with cerebral arteriovenous malformations indicate its potential in clinical applications. The proposed method is easy to implement and does not require administration of a contrast agent or application of specially designed rf pulses to highlight the veins. Rather it exploits the intrinsic magnetic properties (BOLD-effect) and the prolonged T 2* of venous blood. The method may be of diagnostic potential in the assessment of arteriovenous malformations or other vascular venous lesions. © 1998 Elsevier Science B.V. All rights reserved. 相似文献
54.
G. Sparn F. Laube A. Link F. Steglich M. Baenitz K. Lüders H. Werner R. Schlögl 《Journal of Low Temperature Physics》1996,105(5-6):1703-1708
In BaxC60 superconductivity (sc) at Tc=(6.8±0.2) K is associated with the x=4 phase. Here we present pressure studies of Tc of a BaxC60 sample (dTc/dp= –1.9 K/GPa) which exhibits a large volume fraction of the x=4 phase. In the alkali-fullerides K60C60 and Rb3C60 Tc is governed by the electronic density of states N(EF) (Tc
exp{–1/N(EF)V}). The dependence of N(EF) on volume can be approximated by N(EF)=N0
d
eff
3, where deff is the surface to surface distance of neighboured C60-molecules. This relationship is corroborated by (TC,d)-data of various compounds of the form A3–xBxC60 (A: K, Rb; B: K, Rb, Cs; x2). Strong deviation from this behavior is found for the alkaline-fulleride superconductor Ba4C60. This deviation is attributed to the hybridization of alkaline-metal s-, d-states and C60 -states. 相似文献
55.
Franz Baader Werner Nutt 《Applicable Algebra in Engineering, Communication and Computing》1996,7(4):309-337
We study the class of theories for which solving unification problems is equivalent to solving systems of linear equations over a semiring. It encompasses important examples like the theories of Abelian monoids, idempotent Abelian monoids, and Abelian groups. This class has been introduced by the authors independently of each other as commutative theories (Baader) and monoidal theories (Nutt).We show that commutative theories and monoidal theories indeed define the same class (modulo a translation of the signature), and we prove that it is undecidable whether a given theory belongs to it. In the remainder of the paper we investigate combinations of commutative/monoidal theories with other theories. We show that finitary commutative/monoidal theories always satisfy the requirements for applying general methods developed for the combination of unification algorithms for disjoint equational theories.Then we study the adjunction of monoids of homomorphisms to commutative/monoidal theories. This is a special case of a non-disjoint combination, which has an algebraic counterpart in the corresponding semiring. By studying equations over this semiring, we identify a large subclass of commutative/monoidal theories that are of unification type zero. We also show with methods from linear algebra that unitary and finitary commutative/monoidal theories do not change their unification type when they are augmented by a finite monoid of homomor-phisms, and how algorithms for the extended theory can be obtained from algorithms for the basic theory. 相似文献
56.
The basic scheduling problem we are dealing with is the following. There are n jobs, each requiring an identical execution time. All jobs have to be processed on a set of parallel machines. Preemptions
can be either allowed or forbidden. The aim is to construct a feasible schedule such that a given criterion is minimized.
In this paper, we survey existing approaches for the problem class considered. 相似文献
57.
Schultz Thomas Theisel Holger Seidel Hans-Peter 《IEEE transactions on visualization and computer graphics》2010,16(1):109-119
Crease surfaces are two-dimensional manifolds along which a scalar field assumes a local maximum (ridge) or a local minimum (valley) in a constrained space. Unlike isosurfaces, they are able to capture extremal structures in the data. Creases have a long tradition in image processing and computer vision, and have recently become a popular tool for visualization. When extracting crease surfaces, degeneracies of the Hessian (i.e., lines along which two eigenvalues are equal) have so far been ignored. We show that these loci, however, have two important consequences for the topology of crease surfaces: First, creases are bounded not only by a side constraint on eigenvalue sign, but also by Hessian degeneracies. Second, crease surfaces are not, in general, orientable. We describe an efficient algorithm for the extraction of crease surfaces which takes these insights into account and demonstrate that it produces more accurate results than previous approaches. Finally, we show that diffusion tensor magnetic resonance imaging (DT-MRI) stream surfaces, which were previously used for the analysis of planar regions in diffusion tensor MRI data, are mathematically ill-defined. As an example application of our method, creases in a measure of planarity are presented as a viable substitute. 相似文献
58.
Nils Hasler Carsten Stoll Bodo Rosenhahn Thorsten Thormhlen Hans-Peter Seidel 《Computers & Graphics》2009,33(3):211
The paper presents a method to estimate the detailed 3D body shape of a person even if heavy or loose clothing is worn. The approach is based on a space of human shapes, learned from a large database of registered body scans. Together with this database we use as input a 3D scan or model of the person wearing clothes and apply a fitting method, based on ICP (iterated closest point) registration and Laplacian mesh deformation. The statistical model of human body shapes enforces that the model stays within the space of human shapes. The method therefore allows us to compute the most likely shape and pose of the subject, even if it is heavily occluded or body parts are not visible. Several experiments demonstrate the applicability and accuracy of our approach to recover occluded or missing body parts from 3D laser scans. 相似文献
59.
We propose a system that allows the user to design a continuous flow animation starting from a still fluid image. The basic idea is to apply the fluid motion extracted from a video example to the target image. The system first decomposes the video example into three components, an average image, a flow field and residuals. The user then specifies equivalent information over the target image. The user manually paints the rough flow field, and the system automatically refines it using the estimated gradients of the target image. The user semi-automatically transfers the residuals onto the target image. The system then approximates the average image and synthesizes an animation on the target image by adding the transferred residuals and warping them according to the user-specified flow field. Finally, the system adjusts the appearance of the resulting animation by applying histogram matching. We designed animations of various pictures, such as rivers, waterfalls, fires, and smoke. 相似文献
60.
Lutz Hofmann Tobias Fischer Thomas Werner Franz Selbmann Michael Rennau Ramona Ecke Stefan E. Schulz Thomas Geßner 《Microsystem Technologies》2016,22(7):1665-1677
This paper discusses approaches for the isolation of deep high aspect ratio through silicon vias (TSV) with respect to a Via Last approach for micro-electro-mechanical systems (MEMS). Selected TSV samples have depths in the range of 170…270 µm and a diameter of 50 µm. The investigations comprise the deposition of different layer stacks by means of subatmospheric and plasma enhanced chemical vapour deposition (PECVD) of tetraethyl orthosilicate; Si(OC2H5)4 (TEOS). Moreover, an etch-back approach and the selective deposition on SiN were also included in the investigations. With respect to the Via Last approach, the contact opening at the TSV bottom by means of a specific spacer-etching method have been addressed within this paper. Step coverage values of up to 74 % were achieved for the best of those approaches. As an alternative to the SiO2-isolation liners a polymer coating based on the CVD of Parylene F was investigated, which yields even higher step coverage in the range of 80 % at the lower TSV sidewall for a surface film thickness of about 1000 nm. Leakage current measurements were performed and values below 0.1 nA/cm2 at 10 kV/cm were determined for the Parylene F films which represents a promising result for the aspired application to Via Last MEMS-TSV. 相似文献