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81.
The master curve (MC) approach as standardised in the ASTM Standard Test Method E1921 was applied to weld metal of the reactor pressure vessel (RPV) beltline welding seam of Greifswald unit 8 RPV. Charpy size SE(B) specimens from 13 locations equally spaced over the thickness of the welding seam were tested. The orientation of the specimens within the welding seam is TL and TS according to ASTM E399. 相似文献
82.
Versuche zur Ermittlung der Schwefelaktivität in Kalk-Kieselsäure-Schlacken bei 1560°C bei Gleichgewicht zwischen Proben unterschiedlichen Basengrades und einer schwefelhaltigen Bleidampfphase. Abhängigkeit zwischen dem Einsatz von Eisensulfid in der Bleischmelze und dem im Tiegelraum entwickelten Schwefeldampfdruck. Nachweis der Homogenität der Schlackenproben. Feststellung der erforderlichen Reaktionsdauer bis zu Gleichgewichtseinstellung. Angabe von Gleichungen zur Berechnung der Schwefelaktivität in der Schlacke. 相似文献
83.
84.
Hellwig M Parala H Cybinksa J Barreca D Gasparotto A Niermann B Becker HW Rogalla D Feydt J Irsen S Mudring AV Winter J Fischer RA Devi A 《Journal of nanoscience and nanotechnology》2011,11(9):8094-8100
In2O3 thin films were grown by atomic vapor deposition (AVD) on Si(100) and glass substrates from a tris-guanidinate complex of indium [In(N(i)Pr2guanid)3] under an oxygen atmosphere. The effects of the growth temperature on the structure, morphology and composition of In2O3 films were investigated. X-ray diffraction (XRD) measurements revealed that In2O3 films deposited in the temperature range 450-700 degreesC crystallised in the cubic phase. The film morphology, studied by scanning electron microscopy (SEM) and atomic force microscopy (AFM), was strongly dependent on the substrate temperature. Stoichiometric In2O3 films were formed under optimised processing conditions as was confirmed by X-ray photoelectron and X-ray excited Auger electron spectroscopies (XPS, XE-AES), as well as by Rutherford backscattering spectrometry (RBS). Finally, optical properties were investigated by photoluminescence (PL) measurements, spectroscopic ellipsometry (SE) and optical absorption. In2O3 films grown on glass exhibited excellent transparency (approximately 90%) in the Visible (Vis) spectral region. 相似文献
85.
Bauer WA Neuber C Ober CK Schmidt HW 《Advanced materials (Deerfield Beach, Fla.)》2011,23(45):5404-5408
Electron beam lithography is a powerful technique for the production of nanostructures but pattern quality depends on numerous interacting process variables. Orthogonal gradients of resist composition, baking temperatures, and development time as well as dose variations inside writing fields are used to prepare ternary combinatorial libraries for an efficient stepwise optimization of a molecular glass negative tone resist system. 相似文献
86.
Polymer gradient materials (PGMs) are known to reduce stress concentrations and to increase fracture toughness. The first system we reported for the preparation of longitudinal PGMs was based on poly(dimethyl siloxanes), covering a relatively low Young's modulus range. In this study, we used two photochemically and one thermally curing polyaddition systems, enabling us to cover a much larger modulus range up to 1300 MPa. Three different gradient structures, hard-soft, hard-soft-hard, and soft-hard-soft, were realized and confirmed by position-dependent UV/Vis absorbance measurements. Tensile testing in dependency on the gradient structure was performed. A comparison with non-gradient samples with discrete composition revealed a significant improvement, specifically in the case of hard-soft-hard gradients. Hence, PGMs are a promising approach for the development of materials with a special mechanical property profile particularly at different temperatures, leading to novel thermoresponsive materials. 相似文献
87.
Grimm S Giesa R Sklarek K Langner A Gösele U Schmidt HW Steinhart M 《Nano letters》2008,8(7):1954-1959
Ordered nanofiber arrays are a promising material platform for artificial adhesive structures, tissue engineering, wound dressing, sensor arrays, and self-cleaning surfaces. Their production via self-ordered porous alumina hard templates serving as shape-defining molds is well-established. However, their release requires the destruction of the hard templates, the fabrication of which is costly and time-consuming, by wet-chemical etching steps with acids or bases. We report the nondestructive mechanical extraction of arrays of cross-linked polyacrylate nanofibers from thus recyclable self-ordered nanoporous alumina hard templates. Silica replicas of the latter were synthesized using the extricated nanofiber arrays as secondary molds that could be mechanically detached from the molded material. The approach reported here, which can be combined with microstructuring, may pave the way for the high-throughput production of both functional nanofiber arrays and ordered nanoporous membranes consisting of a broad range of material systems. 相似文献