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The infiltration of compacted cubic BN (cBN) with molten aluminum has been investigated as a potential route for a cheap and easy method of manufacturing cBN/metal composites. CBN compacts have been infiltrated with molten Al at a temperature between 670 and 800 °C and pressure of 15 MPa in vacuum. At these temperatures no pronounced interactions between hexagonal and cubic BN with Al was observed, allowing the complete infiltration of cBN with 12 μm mean grain size. After infiltration at 800 °C, the temperature was increased without pressure to convert aluminum into borides and AlN. The hardness of the resulting materials depends on the content of hexagonal, cubic BN and the rate of conversion of Al into borides and AlN. The infiltration height of less than 1 mm obtained from infiltrating the 3 μm cBN powder green compacts gave a hardness of 22.0 ± 0.6 GPa after heat treatment. 相似文献
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Joachim Schummer 《Scientometrics》2007,70(3):669-692
Based on bibliometric methods, this paper describes the global institutionalization of nanotechnology research from the mid-1980s
to 2006. Owing to an extremely strong dynamics, the institutionalization of nanotechnology is likely to surpass those of major
disciplines in only a few years. A breakdown of the relative institutionalizations strengths by the main geographical regions,
countries, research sectors, disciplines, and institutional types provides a very diverse picture over the time period because
of different national science policies. The results allow a critical assessment of the different science policies based on
the relative institutionalizations strengths as well as the conclusion that the institutionalization process has run out of
control of individual governments who once induced the development. 相似文献
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Reports an error in the original article by J. Krueger (American Psychologist, 2001, Vol 56[1], pp. 16-26). In Figure 2, on page 22, two of the curves are labeled "p(H0)=.9" and "p(H0)=.1." These labels should have been reversed. (The following abstract of this article originally appeared in record 2001-16601-002.) Null hypothesis significance testing (NHST) is the researcher's workhorse for making inductive inferences. This method has often been challenged, has occasionally been defended, and has persistently been used through most of the history of scientific psychology. This article reviews both the criticisms of NHST and the arguments brought to its defense. The review shows that the criticisms address the logical validity of inferences arising from NHST, whereas the defenses stress the pragmatic value of these inferences. The author suggests that both critics and apologists implicitly rely on Bayesian assumptions. When these assumptions are made explicit, the primary challenge for NHST--and any system of induction--can be confronted. The challenge is to find a solution to the question of replicability. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
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Crystallization of Polymer-Derived Silicon Carbonitride at 1873 K under Nitrogen Overpressure 总被引:1,自引:0,他引:1
Martin Friess Joachim Bill Jerzy Golczewski re Zimmermann Fritz Aldinger Ralf Riedel Rishi Raj 《Journal of the American Ceramic Society》2002,85(10):2587-2589
The chemical stability of an amorphous silicon carbonitride ceramic, having the composition 0.57SiC·0.43Si3 N4 ·0.49C is studied as a function of nitrogen overpressure at 1873 K. The ceramic suffers a weight loss at p N2 < 3.5 bar (1 bar = 100 kPa), does not show a weight change from 3.5 to 11 bar, and gains weight above 11 bar. The structure of the ceramic changes with pressure: it is crystalline from 1 to 6 bar, amorphous at ∼10 bar, and is crystalline above ∼10 bar. The weight-loss transition, at 3.5 bar, is in excellent agreement with the prediction from thermodynamic analysis when the activities of carbon, SiC, and Si3 N4 are set equal to those of the crystalline forms; this implies that the material crystallizes before decomposition. The amorphous to crystalline transition that occurs at ∼10 bar, and which is accompanied by weight gain, is likely to have taken place by a different mechanism. A nucleation and growth reaction with the atmospheric nitrogen is proposed as the likely mechanism. The supersaturation required to nucleate α-Si3 N4 crystals is calculated to be 30 kJ/mol. 相似文献
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J Barrette R Bellwied P Braun-Munzinger WE Cleland T Cormier G Dadusc G David J Dee O Dietzsch M Fatyga SV Greene JV Germani JR Hall TK Hemmick N Herrmann RW Hogue B Hong K Jayananda D Kraus BS Kumar R Lacasse D Lissauer WJ Llope TW Ludlam R Majka SK Mark JT Mitchell M Muthuswamy E O'Brien C Pruneau FS Rotondo da Silva NC J Simon-Gillo U Sonnadara J Stachel H Takai EM Takagui TG Throwe L Waters C Winter D Wolfe CL Woody N Xu Y Zhang Z Zhang C Zou 《Canadian Metallurgical Quarterly》1995,52(5):2679-2683
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A Aliverti L Piubelli G Zanetti T Lübberstedt RG Herrmann B Curti 《Canadian Metallurgical Quarterly》1993,32(25):6374-6380
To investigate the functional role of the cysteine residues present in the spinach ferredoxin-NADP+ oxidoreductase, we individually replaced each of the five cysteine residues with serine using site-directed mutagenesis. All of the mutant reductases were correctly assembled in Escherichia coli except for the C42S mutant protein. C114S and C137S mutant enzymes apparently showed structural and kinetic properties very similar to those of the wild-type reductase. However, C272S and C132S mutations yielded enzymes with a decreased catalytic activity in the ferredoxin-dependent reaction (14 and 31% of the wild type, respectively). Whereas the C132S was fully competent in the diaphorase reaction, the C272S mutant flavoprotein showed a 35-fold reduction in catalytic efficiency with respect to the wild-type enzyme (0.4 versus 14.28 microM-1 s-1) due to a substantial decrease of kcat. NADP+ binding by the C272S mutant enzyme was apparently quantitatively the same (Kd = 37 microM) but qualitatively different, as shown by the differential spectrum. Stopped-flow experiments showed that the enzyme-FAD reduction rate was considerably decreased in the C272S mutant reductase, along with a much lower yield of the charge-transfer transient species. It is inferred from these data that the charge transfer (FAD-NADPH) between the reductase and NADPH is required for hydride transfer from the pyridine nucleotide to flavin to occur with a rate compatible with catalysis. 相似文献
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